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Results show that the best value of w is 7~10% and 5~7%, i is 0.08~0.2 A/cm^2 and 0.03~0.05 A/cm^2 respectively, during the electrolysis fluorination of pyridine and tributylamine; the addition of N-butyl mercaptan into the organic mixture can stabilize electrolysis process with its mass fraction 15~20% at best; impulse current polarization work status of low load is helpful to the electrolysis process and reduces corrosion rate of anode; electrolysis temperature is suitable at 0~20℃; electrobath can use electrolyte inner circulation structure, exterior circulation structure or blending structure.

结果表明:吡啶和N-三丁胺电解氟化的最佳值w分别为7%~10%和5%~7%,i分别为0.08~0.2A/平方公分和0.03~0.05A/平方公分;有机混合物中添加N-丁基硫醇可稳定电解过程,其质量分数最佳为15%~20%;采用低负荷的脉冲电流极化工况有利电解过程,降低阳极的腐蚀速度;电解温度0~20℃为宜;电解槽可采用电解液内循环、外循环结构,或其混合结构。

Results The ethanol extracts 0.48 gkg^(-1, macroporous resin eluate of aqua 0.3 gkg^(-1 and the further purification 0.1, 0.3 gkg^(-1 could hasten gastric emptying in mice. Furthermore, they restrained the inhibition of dopamine on gastric emptying in mice. They had no effect on the inhibition of atropine.

结果 醇提物0.48gkg^(-1、大孔树脂水洗脱物0.3gkg^(-1及继续纯化物01、0.3gkg^(-1对正常小鼠的胃排空有促进作用,并可拮抗多巴胺引起的小鼠胃排空的抑制作用,而对阿托品引起的小鼠胃排空抑制作用无影响。

In another direction, the radical cyclization of thioimide with acylsilane produced simple cyclization product in low yield without expected enol silyl ether compound.

对於硫醯亚胺与矽基酮的自由基反应,则是得到低产率的简单环化产物,而不是预期的烯醇矽醚化合物。

METHODS: Eighty guinea pigs were randomized into control group, model group, salbutamol treated group and Maxin liquid treated group. Asthma model s were established by ovalhumin. The changes of eosinophile in bronchoalveolar lavage fluid, thromboxane B2 and 6-Keto-prostaglandin F1a in blood, the airway resistance and the pulmonary compliance were observed by Pap staining, radio-immunity , and pulmonary function test instrument of MIL type specially for experimental animal.

实验设正常对照组、模型对照组、复方麻辛组、沙丁胺醇组,选用豚鼠共80只,采用清蛋白造模,并运用巴氏染色法、放射免疫法、MIL型实验动物肺功能测量仪,分别检测肺泡灌洗液中嗜酸粒细胞数、血浆凝血恶烷(TXB2)、6-酮-前列腺素(6-K-PGF1a)以及清蛋白激发后气道阻力和肺顺应性。

Solasodine, which was known to inhibit the synthesis of ergosterol, had a close clustering position with ketoconazole and clotrimazole group.

另外已知澳洲茄胺抑制的是细胞膜上麦角固醇的合成,聚类分析表明它与酮康唑,克霉唑的聚类很靠近。

The phosphoric acid in turn is esterified to another moiety, such as choline, ethanolamine, or inositol.

此磷酸本身又与另一部分如胆碱、乙醇胺或肌醇分子酯化结合。磷酸甘油酯的命名法和甘油三酸酯的命名法相同。

BIO-BEAUTE commits to selecting only 100%pure natural extracts: no silicone, no PEG, no petrochemical derivatives, no genetically modified organisms, no artificial coloring agents, no parabens, no EDTA, no formaldehyde, no products with ethoxyl derivatives, no phenoxyethanol.

BIO-BEAUTE 保证选择100%的纯净天然提取物:无硅胶、无聚乙二醇、无石油化学衍生物、无转基因有机体、无人工着色剂、无苯甲酸酯类、无乙二胺四乙酸、无甲醛、无羟乙基衍生产品,无无苯氧乙醇。

Effects on the reaction of factors such as reactant ratio, reaction time, and reaction temperature were investigated, and optimum reaction conditions were determined as follows: mole ratio of cyanuric chloride to ethylamine to sodium hydroxide to sodium methyl mercaptide was 1:2.1:2.0:1.7, and the temperature and time of the first, second, and third substitution reactions were -2, 0, and 82℃ and 30, 60, and 180 min, respectively.

讨论了原料配比、反应时间和反应温度等因素对反应的影响,获得了较佳的反应条件。较佳反应条件为三聚氯氰:乙胺:氢氧化钠:甲硫醇钠=l:2.1:2.0:1.7,第一、第二、第三取代反应的反应温度和反应时间分别为-2℃、0℃、82℃和30、60、180min。

Simetryne is synthesized from cyanuric chloride, ethylamine and sodium methyl mercaptide in solution of the trichloroethylene.

以三聚氯氰、乙胺和甲硫醇钠为原料,以三氯乙烯为溶剂制备了西草净。

The appropriate conditions are that the mole ratio of cyanuric chloride to ethylamine, sodium hydroxide, sodium methyl mercaptide is 1:2.1:2.1:4.0, the temperature and time of first, second, third substitution reaction is respectively 0℃, 20℃, 78℃ and 10min, 30min, 480min.

适宜反应条件为三聚氯氰:乙胺:氢氧化钠:甲硫醇钠=1:2.1:2.1:4,第一、第二、第三取代反应的反应温度和反应时间分别为0,20,78℃和10,30,480min。

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