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醇胺

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The present invention relates to a process for rapid solution synthesis of a peptide, the process comprising repetitive cycles of steps-: a coupling step, using an excess of an activated carboxylic component to acylate an amino component, a quenching step in which a scavenger is used to remove residual activated carboxylic functions, wherein the scavenger may also be used for deprotection of the growing peptide, one or more aqueous extractions and optionally, a separate deprotection step, followed by one or more aqueous extractions, characterised in that the process comprises at least one step, referred to as step, in which an amine or a thiol comprising a free anion or a latent anion is used as a scavenger of residual activated carboxylic functions.

本发明涉及快速溶液合成肽的方法,该方法包括步骤-的重复循环:偶联步骤,使用过量的活化羧基成分酰化氨基成分,淬灭步骤,在该步骤中使用清除剂除去残余的活化羧基官能团,其中该清除剂还可以用于使生长中的肽去保护,一或多个水抽提和任选地,独立的去保护步骤,之后进行一或多次水抽提,其特征在于该方法包括至少一个步骤,称作步骤,在该步骤中包含自由阴离子或潜阴离子的胺或硫醇用作残余活化羧基官能团的清除剂。

The studies segmented polyester polyurethaneurea elastomers based on 4,4'-diphenylmethane diisocyanate, ethylene diamine and polybutylene adipate (M. W. 1975 and M. W. 1228) were studied by means of IR spectrascopy.

用红外光谱法对基於4,4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯(分子量分别为1975和1228)的嵌段聚脲氨酯弹性体进行了研究。

Hydrogen bonding in hard segment domains of segmented polyester polyurethaneurea based on 4,4'-diphenylmethane diisocyanate, ethylene diamine and polybutylene adipate(M. W. 1975 and M. W. 1228) was studied by means of IR spectroscopy.

用红外光谱法对基於4,4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯(分子量分别为1975和1228)的两系列嵌段聚酯型聚脲氨酯硬段微区中的氢键化进行了研究。

In this work, a series of layered silver-long chain alkylamine complex has been synthesized in the alcohol/water system for the first time, and such compound possesses the special sponge-like macroporous structure.

在本工作中,系列银-不同碳链长度的有机胺的配合物首次在醇-水体系中被合成获得,且该化合物具有特征性的海绵形貌中空结构。

Compared the homogeneous enthalpic interaction coefficients of glycine in aqueous potassium chloride solutions with that in aqueous sodium chloride solutions and discussed different cations influence on the interaction of glycine in aqueous solutions. The dilution enthalpies of DMF in aqueous ethylene glycol, glycerol, glucose and sucrose solutions of various molalities have been determined using CSC4400 flow microcalorimetry at

本文选择N,N—二甲基甲酰胺为模型化合物,用流动量热法测定了298.15K下DMF在不同浓度的乙二醇、甘油、蔗糖和葡萄糖水溶液中的稀释焓,根据McMillan-Mayer理论,计算了其在不同溶剂组成下的同系焓相互作用系数,得到水溶液中多羟基化合物与酰胺的相互作用规律。

Examples of suitable polar volatile liquid are amines ethers especially lower alkyl ethers organic acids esters ketones glycols alcohols amides ureas sulphoxides sulphones and water.

合适的极性挥发性液体的例子有胺,醚,尤其是低级烷基醚,有机酸,酯类,酮类,乙二醇,乙醇,酰胺,尿素,sulphoxides,砜和水。

In this work, salbutamol and sulphuric acids were used as reactants and isopropanol was used as a solvent.

以沙丁胺醇和硫酸为反应物,在异丙醇溶液中采用反应结晶法制备超细硫酸沙丁胺醇颗粒。

Ethambutol is a first-line drug used for antituberculosis therapy. It is often used in combination with isoniazid, rifampin, pyrazinamide, and streptomycin. The action of EMB in antituberculosis mechanism is the destruction of cell wall of tubercle bacilli via binding the target molecule -- arabinosyl transferases. These enzymes are involved in the polymerization of the cell wall arabinan. Inhibition of arabinan synthesis by EMB results in the accumulation of mycolic acids, leading to cell death.The EMB-resistance of MTB is involved with the mutation of emb operon or the over expression of emb operon.

乙胺丁醇是和异烟肼、利福平、链霉素、吡嗪酰胺联合治疗结核病的一线抗结核药物,EMB对结核分枝杆菌的作用机制与分枝杆菌胞壁结构破坏有关,主要作用于靶分子阿拉伯糖基转移酶,抑制了阿拉伯糖基聚合入阿拉伯半乳聚糖,从而影响细胞壁分枝菌酸-阿拉伯半乳聚糖-肽聚糖复合物的形成,导致菌细胞的死亡。

Determination of methyl ethyl ketone and sec-butanol by gas chromatography was reported.

丁酮在合成抗氧防胶剂N,N'-二仲丁基对苯二胺过程中是过量的,回收利用可以节省不少成本,但其可以加氢生成仲丁醇,有必要测定回收丁酮中仲丁醇的含量。

In this study, Japanese cedar, Ma bamboo and Makino bamboo were liquefied in polyethylene glycol/glycerol co-solvent with H2SO4 or HCl as catalyst. The liquefied woody materials were blended with PMDI (4,4'-Diphenylmethane diisocyanate;MDI) to prepare the PU foams. The effects of preparation conditions of PU resin on the properties of PU foams were investigated.

中文摘要本研究将柳杉(Cryptomeria japonica; Japanese cedar)、麻竹(Dendrocalamus latiflorus; Ma bamboo)及桂竹(Phyllostachys makinoi; Makino bamboo)等木质材料以聚乙二醇及丙三醇之混合液为溶剂,H2SO4及HCl为催化剂进行液化处理,并将其液化木质材料与4,4'-二苯甲烷二异氰酸酯反应制造聚胺基甲酸酯发泡体,探讨PU树脂调配条件对PU发泡体性质之影响。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

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