醇胺

Seven compounds have been isolated from hard coral Acropora pulchra. These compounds are:pentadecoic acid, heptadecyl ester;(2)n-cetanol;(3)batyl alcohol;(4) N- [ 1 --2-hydroxyl--3,7-heptad-ecadienal] -hexadecanamide;(5)1 -0-hexanoyl-glycerol ester;(6)thymine;(7)uracil. Their structures were determined by IR, MS, HNMR, 13CNMR analysis.

从北海佳丽鹿角珊瑚Acropora pulchra乙醇提取液的乙酸乙酯部分分离出七个化合物，经IR、MS、~1HNMR、~(13)CNMR等波谱方法鉴定，其结构分别为：(1)十五酸十七酯，(2)正十六碳醇，(3)鲨肝醇，(4)N-1-羟基甲基-2-羟基—-3，7-十七碳二烯基十六酸酰胺，(5)1-正十六酸甘油酯，(6)胸腺嘧啶，(7)尿嘧啶。

Synthesis and liquid crystalline behavior of three recently reported mesogenic block-molecules, namely polyhydroxy 1-benzoylaminopropane-2,3-diols I、star-shaped pentaerythritol tetrabenzoates II and calamitic bolaamphiphiles with lateral chains III which are constituted of anisometric block, amphiphilic block and alkyl or perfluorinated chains with different topologies are reviewed in this article.

本文对近来报道的三类嵌段液晶分子：多羟基1－苯甲酰胺－2，3－丙二醇两亲性分子I，星状季戊四醇苯甲酸酯II及带侧链的波拉化合物III的合成及自组装行为作了综述。

The results showed that precursor feeding (phenylanine, sodium acetate and benzamide) and mixed sugar as production medium resulted in significant increase of taxol production not only in the one-liquid-phase cultures of Taxus chinensis var. mairei but also in the two-liquid-phase cultures. And the integrated function of precursor feeding and mixed sugar in the two-liquid-phase cultures gave more significant increase of taxol production significant increase of taxol production, which was four times more than that of the control (the one-liquid-phase culture without precursors and mixed sugar).

结果表明前体饲喂（苯丙氨酸，醋酸钠和苯甲酰胺）和蔗糖与麦芽糖配伍作为生产培养基糖源不仅对红豆杉细胞悬浮培养，而且对其两液相培养的紫杉醇产量提高均有明显的促进作用，与对照组相比，在南方红豆杉细胞两液相培养中，采用前体饲喂和蔗糖与麦芽糖配伍作为生产培养基糖源，紫杉醇产量提高4倍多。

Thermodynamic properties of PSf - DMAc - alcohols ternary systems are studied, the binodal is calculated. Cloud point curves from light scattering experiment verify the calculation results; The agreement between the cloud point curves and the binodal is quite well.

文章摘要：对聚砜-二甲基乙酰胺-醇类非溶剂构成的制膜体系的热力学特性进行了研究，计算出这些体系的双结点线，并用这些醇类非溶剂通过光散射法进行浊点滴定实验，浊点曲线与双结点线基本重合，验证了双结点线的计算结果。

Undecanedioic acid, dodecanedioic acid, brassylic acid, tetradecanedioic acid, pentadecanedioic acid, nylon 1212 resin, nylon 1212 salt, nylon 1212 powder, pa 1212 adhesives and sealants, zirconium dioxide, zirconium dioxide powder, zirconium oxychloride, 1,10-decanediol, 1,12-dodecanediol, dimethyl sebacate, dodecanedioic acid dimethyl ester, dodecane diamine etc.

十一碳二元酸，十二碳二元酸，十三碳二元酸，十四碳二元酸，十五碳二元酸，十二碳二元胺，十二碳二元醇，癸二醇，癸二酸二甲酯，十二碳二酸二甲酯，PA尼龙1212型高档热熔胶；以及二氧化锆，氧氯化锆等。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先，以巴豆醛与乙硫醇为原料，在三乙胺的催化作用下高收率制得3-乙硫基丁醛；然后从乙酰乙酸甲酯出发，通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮，接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环，再通过皂化和脱羧反应生成中间体5-[2-丙基]-1，3-环己二酮；再与丙酸酐反应丙酰化，最后与0-3-氯-2-丙烯基羟胺肟化，得到目标化合物烯草酮。

A novel planar chiral diferrocenylimine-diols 6 was synthesized by the condensation of R, S(subscript p-1-(2-diphenyl hydroxyl methyl) ferrocenylethylamine [R, S(subscript p-4] with phthaldehyde in anhydrous ethanol, and was crystallographically characterized.

通过R，S(下标 p-1-（2-二苯基羟甲基）二茂铁乙胺[R，S(下标 p-4]和对苯二甲醛在无水乙醇中的缩合反应合成了一种新型平面手性双二茂铁亚胺二醇化合物6，并经X-射线衍射分析它的晶体结构。

The preparation of grafted derivant of tertiary amine: it is prepared by the reacting of above (1) product and (2) product heated in water bath at 40℃ within 10min.

聚环氧氯丙烷乙二醇哌啶接支衍生物的制备：将上面制备的聚环氧氯丙烷乙二醇与0.25mol环氧丙基哌啶叔胺于40℃水浴条件下进行接支反应。

The results show that the foamable MAA/MAN copolymers were prepared at 40-60℃ by polymerizing the mixture of 50phr MAA, 50phr MAN, 1-5phr magnesium oxide, 2-8phr butanol and tert-butanol, 0.2-0.3 phr dibenzoyl peroxide and tert-butyl perbenzoate and 0.1-0.2phr DMF. Then the resulting copolymers were expanded at 200-220℃ for 2-3h, subsequently treated at 160℃ for 5-6h, generating PMI foams with excellent mechanical properties and heat-resistance.

研究结果表明：将50份MAA、50份MAN、1~5份氧化镁、2~8份正丁醇、叔丁醇的混合物、0.2~0.3份过氧化二苯甲酰和过氧化苯甲酸叔丁酯和0.1~0.2份的甲酰胺，混合均匀后在40~60℃聚合为可发泡的MAA/MAN共聚物，该共聚物在200~220℃下发泡2~3h，在160℃下热处理5~6h，制得PMI泡沫塑料，其力学性能和耐热性能优异。

The results showed that dihydric alcohol as the solvent with diethanolamine as the catalyst under 150~190℃ was useful in the glycolysis of the liquefied woody material-based PU foams.

以液化生质物为基质之PU发泡体利用二醇类为溶剂，二乙醇胺为催化剂，在150~190℃加热温度下可快速进行醇解反应。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。