醇溶胶

A novel platinum immunosensor modified with hepatitis B surface antibody on colloidal gold and polyvinyl butyral has been fabricated to detect hepatitis B surface antigen.

报道了一种基于聚乙烯醇缩丁醛和金溶胶，把乙型肝炎表面抗体固定在铂金电极上，用来检测乙型肝炎表面抗原的一种新型电位型免疫传感器。

Chapter 4 comprises two part. Part reports on the manufacture and characterization of glucose oxidase -silver sol-polyvinyl butyral modified platinum electrodes with naphthol green B as an electron transfer mediator in the glucose solution.

将纳米Ag溶胶与聚乙烯醇缩丁醛构成复合固酶膜基质，采用溶胶-凝胶法固定GOD修饰铂丝电极，并以葡萄糖溶液中的萘酚绿B为电子媒介体组成葡萄糖生物传感器。

Part two describes the manufacture and characterization of glucose oxidase -silver sol-polyvinyl butyral modified platinum electrodes with tris(2,2-bipyridyl)cobalt perchlorate as an electron transfer mediator in the glucose solution.

用纳米Ag溶胶固定GOD，采用聚乙烯醇缩丁醛为辅助固酶膜基质修饰铂丝电极，并以葡萄糖溶液中的CO恤pyh（CIO4）3为电子媒介体组成葡萄糖氧化酶生物传感器。

The preparation technics are optimized. The power reunite can be decreased from adding glycol into the solution, and the Sol-Gel is a efficiency method to prepare the power of cobaltite.

优化了制备工艺，乙二醇的加入可以缓解粉末团聚现象的发生，溶胶-凝胶方法是制备钴酸盐粉体材料的有效方法。

The method comprises:(1) weighing lead acetate hexahydrate and thioacetamide, and preparing aqueous solutions respectively, so that the concentration ratio of Pd2+ to S is 1:(1-4);(2) adding acetic acid into thioacetamide solution to adjust the pH value to 2-4;(3) adding poly surfactant into lead acetate solution, ultrasonicating to mix uniformly and obtain a colorless and transparent sol;(4) mixing the sol and thioacetamide solution;(5) placing the mixed solution in a sealed container, irradiating by 2.5 MeV and 40 mA electron accelerator with irradiation dose of 25-40 Mrad;(6) washing the product, centrifuging for separation, and drying to obtain black PdS nanoparticles.

本发明方法的工艺过程如下：首先称取一定量的六水合醋酸铅和硫代乙酰胺，各自配制成水溶液，其浓度比为使其中的铅离子浓度与硫原子浓度的比例为1∶1～1∶4；在硫代乙酰胺溶液中加入适量醋酸调节其pH值至2～4；醋酸铅溶液中加入少量表面活性剂聚乙烯醇，然后超声振荡，混合均匀，制成无色透明溶胶；随后将溶胶与上述的硫代乙酰胺溶液混合；将该混合液置于密闭容器中，并将其放置于2.5MeV、40mA的电子加速器产生的电子束辐照下进行辐照处理，其辐照剂量为25～40Mrad；然后将反应生成物清洗，并用高速离心机离心分离，然后干燥，最终得到黑色纳米硫化铅颗粒。

The porous TiO2 anatase nanometer thin films were prepared from alkoxide solutions containing polyethylene glycol by sol-gel method.

锐钛矿型多孔TiO2纳米薄膜可以从含聚乙二醇的钛酸盐溶胶前驱体中通过溶胶-凝胶法制备。

Ni-P-mCMC/mCS bipolar membrane was prepared from carboxymethyl cellulose modified with phosphorylated agent as a cation exchange layer and chitosan modified with glutaraldehyde as an anion exchange layer. The electrolysis cell was constituted by Ni-P-mCMC/mCS BPM as a septum for electrogenerating furfural alcohol and furoic acid.

以磷酸化试剂改性羧甲基纤维素钠制备了阳膜层，以戊二醛改性壳聚糖制备了阴膜层溶胶，将阴膜层溶胶流延于阳膜层上，制备了P-mCMC/mCS双极膜，而后以化学镀方法在阳膜层表面镀镍，制备了Ni-P-mCMC/mCS双极膜，并应用于成对电合成糠醇、糠酸。

The sol gel materials are prepared through the hydrolysis and polycondensation of tetramethoxy silicane.

溶胶 凝胶技术是将金属醇盐等原料配制成均质溶液，在饱和条件下经水解缩聚等化学反应，生成物聚集成溶胶，再经蒸发、干燥转变为凝胶，这是一项在低温下制备纳米粉末或多孔玻璃的技术[1] 。

Using ethylene glycol as solvent, all the three source materials were takingpart in polyreaction of gel. The solubility of bismuth subnitrate in ethyleneglycol was accelerated greatly due to the production of nitrate ester during thepolymerization of precursors.

SBT粉体的溶胶—凝胶制备过程表明：在以乙二醇为溶剂时，三种原材料都参与了聚合反应，前驱物聚合反应过程中有硝酸酯产生，因而促进了硝酸氧铋在乙二醇溶液中的溶解性能。

In contrast, Al2TiO5 can not be synthesized at low temperatures using methanol or tert-butyl alcohol as oxygen donor due to their high chemical reactivity resulting in hydrolysis reaction.

以TiCl4和无水AlCl3为原料，以无水低碳醇为氧供体通过非水解溶胶-凝胶法低温合成了钛酸铝，研究了无水低碳醇种类及用量对钛酸铝合成反应的影响。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。