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The invention discloses an InP quantum point preparing method, comprising the steps of:(1) mixing InCl3 with trioctylphosphine oxide, and preserving heat at 90-110DEG C to prepare a solution whose In content is 0.1-0.3mol/L;(2) raising temperature to 130-180DEG C, and charging argon gas;(3) injecting PSi(CH333 into InCl3-TOPO compound in the molar ratio of 1 to 1-1 to 2;(4) when the solution color turns into transparent red or orange, raising temperature to 260-270DEG C and preserving heat;(5) lowering temperature to 90-110DEG C and injecting dodecyl amine, decyl amine or mercaptan;(6) dissolving reacting mixture in nonpolar solvent to form transparent colloidal solution, then adding in polar solution until the colloidal solution is muddy, and centrifugally separating and obtaining deposits and supernatant; and (7) centrifugally separating the supernatant, where the above steps (1)-(5) are performed.

本发明公开了一种InP量子点的制备方法,其步骤为:①将InCl 3 与三辛基氧膦混合,在90~110℃保温制得In含量为0.1~0.3mol/L的溶液;②升温到130~180℃,通入氩气;③将PSi(CH 3 3 3 注射入InCl 3 -TOPO复合物中,其摩尔比为1∶1~1∶2;④待溶液颜色变为透明的红色或橙红色,将升温260~270℃保温;⑤降温到90~110℃,注入十二胺、癸胺或硫醇;⑥将反应混合物溶于非极性溶剂,形成透明的胶体溶液,然后加入极性溶剂,直至胶体溶液出现混浊状,然后离心分离获得沉积物和上层清液;⑦取上层清液进行离心分离。上述步骤①~⑤在保护气氛下进行。

Chirata, and they were identified as β-sitosterol and swerchirin by spectral method. These two compounds were got firstly from the petrolelum ether fraction of S. chirata.

结论]2种化合物β-谷甾醇与1,8-二羟基-3,5二甲氧基山酮均为首次从印度獐芽菜乙醇提取物的石油醚部位分离得到。

And the content of chromate and polyvinyl alcohol also affect the bonding force between the coating and matrix.

涂液中铬酐和聚乙烯醇的含量还影响涂层与基体之间的结合力,必须适当控制。

As well as activity was exhibited. Theaddition of cinchonidine led to a remarkable increase in the reaction rate, as confirmed bythe IR study that the modifier activates the carbonyl groups of the reactant through itsquinuclidine nitrogen. On the contrary,〓 exerted a strong inhibition effect on theenantioselective hydrogenation. Chapter 3 Finely dispersed polyvinylpyrrolidone-stabilized iridium andbimetallic clusters were prepared by the alcohol-water reduction method.

第三章 采用醇水还原的方法制备了聚乙烯基吡咯烷酮稳定的铱纳米簇及双金属纳米簇,对丙酮酸甲酯的催化氢化表明,在铱金属簇催化体系中,辛可尼定不仅诱导了一定的对映选择性,同时对反应活性有明显的促进作用,平均反应速率可提高2-6倍。

By the theories of cavitations and free volume, it analyses the factors on lubricant low-temperature property in view of molecule structure, brings up effective ways to improve the low-temperature properties, conducts plenty of testing with even designs, and then investigates and tests the lubricant's low-temperature properties with computerized system; it analyses the data by regressi on method and optimizes the solving, and studies on the base oil of environment friendly lubricants and selects the composition of colza oil, esters and PAO2, and discusses on low-temperature flowability of vegetable-base lubricants.

应用空穴理论及自由体积理论,从分子结构角度分析了影响润滑油低温性能的因素,提出了改善对润滑油低温性能的有效途径,组织了大量试验,通过润滑油的计算机检测系统对润滑油的低温性能进行了分析检测,采用均匀设计来组织实验;用逐步回归对数据进行分析并且进行最优化求解,对环境兼容润滑油的基础油进行了分析研究,选择菜籽油、季戊四醇酯和聚α-烯烃作为基础油,并从理论上对植物基润滑油的低温流动性进行了探讨。

By the theories of cavitations and free volume, it analyses the factors on lubricant low-temperature property in view of molecule structure, brings up effective ways to improve the low-temperature properties, conducts plenty of testing with even designs, and then investigates and tests the lubricants low-temperature properties with computerized system; it analyses the data by regression method and optimizes the solving, and studies on the base oil of environment friendly lubricants and selects the composition of colza oil, esters and PAO2, and discusses on low-temperature flowability of vegetable-base lubricants.

应用空穴理论及自由体积理论,从分子结构角度分析了影响润滑油低温性能的因素,提出了改善对润滑油低温性能的有效途径,组织了大量试验,通过润滑油的计算机检测系统对润滑油的低温性能进行了分析检测,采用均匀设计来组织实验;用逐步回归对数据进行分析并且进行最优化求解,对环境兼容润滑油的基础油进行了分析研究,选择菜籽油、季戊四醇酯和聚α-烯烃作为基础油,并从理论上对植物基润滑油的低温流动性进行了探讨。

By the theories of cavitations and free volume, it analyses the factors on lubricant low-temperature property in view of molecule structure, brings up effective ways to improve the low-temperature properties, conducts plenty of testing with even designs, and then investigates and tests the lubricant's low-temperature properties with computerized system; it analyses the data by regression method and optimizes the solving, and studies on the base oil of environment friendly lubricants and selects the composition of colza oil, esters and PA02, and discusses on low-temperature flowability of vegetable-base lubricants.

应用空穴理论及自由体积理论,从分子结构角度分析了影响润滑油低温性能的因素,提出了改善对润滑油低温性能的有效途径,组织了大量试验,通过润滑油的计算机检测系统对润滑油的低温性能进行了分析检测,采用均匀设计来组织实验;用逐步回归对数据进行分析并且进行最优化求解,对环境兼容润滑油的基础油进行了分析研究,选择菜籽油、季戊四醇酯和聚α-烯烃作为基础油,并从理论上对植物基润滑油的低温流动性进行了探讨。

The invention discloses a polyvinyl composite material with moisture absorption function and a method for preparing the same.

本发明公开了一种聚乙烯基吸湿功能复合材料及其制备方法,该材料的组分及其重量百分比含量为:低密度聚乙烯60~80%,相容剂2~8%,聚乙烯醇10~30%,助剂5~10%。

The present invention relates to a coating composition comprising; A at least one polyester oligomer prepared from reactants comprising a 20 60 wt.% of at least one polyol, b 5 30 wt.% of at least one polycarboxylic acid selected from the group of cyclic polycarboxylic acids, the esters or the anhydrides thereof, wherein the carboxyl groups are separated by 3 carbon atoms or less, and from the group of alpha , beta -saturated acyclic polycarboxylic acids, the esters or the anhydrides thereof, and c 20 60 wt % of at least one monocarboxylic acid, the sum of the wt.% indicated for the reactants,, and always being 100 wt.%, and the oligomer being a low-viscosity oligomer having a weight average molecular weight Mw of less than 5,000, and a hydroxyl number in the range of about 200 to about 400 mg KOH/g oligomer, and B at least one polyisocyanate.

本发明涉及一种包含如下组分的涂料组合物:A至少一种由包含如下成分的反应物制备的聚酯低聚物:a20-60wt%至少一种多元醇,b5-30wt%至少一种选自其中羧基被3个或更少碳原子隔开的环状多元羧酸、其酯或酸酐以及选自α,β-饱和的无环多元羧酸、其酯或酸酐的多元羧酸,以及c20-60wt%至少一种一元羧酸,其中反应物、和的wt%之和总是为100wt%,所述低聚物是重均分子量Mw低于5000且羟基值为约200-约400mg KOH/g低聚物的低粘度低聚物,以及B至少一种多异氰酸酯。

The waste acid was recovered from the raffinate with the active carbon as the decolorant at room temperature .

以正辛醇为萃取剂,通过三级萃取处理硝基C酸废水,萃余水相经过活性炭室温下脱色回收废酸。

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