醇基

The solubilities in some solvents were investigated and solubilization abilities of OCC for water-insoluble drugs were evaluated. The results show that the degree of substitution of carboxymethyl groups and octyl groups are determined to be 115.9% and 58.0%, respectively. OCC are insoluble in organic solvents while show a much better solubility in water and formed opalescence solutions, which increased the solubility of paclitaxel up to 500 folds in water. The drug loading and drug encapsulation efficiency of OCC are 34.6% and 89.9%, respectively.

所制备的OCC羧甲基取代度为115.9%，取代主要发生在6位羟基上；辛基取代度58.0%，取代主要发生在2位氨基上；与壳聚糖相比，OCC分子间／内氢键作用减弱；OCC在常用的有机溶剂中不溶，但在水中溶解度增加，能够形成具有淡蓝色乳光的纳米胶体溶液，对难溶性抗肿瘤药物紫杉醇具有优越的增溶能力，使紫杉醇在水中的溶解度提高近500倍，载药量34.6%，包封率为89.9%。

New Hawthorn Buccal Tablet mainly takes the effective element as its major material,plus sugar-free materials such as xylitol and Palatinitol,as well as pawpaw,plum , liquorice,mint and etc.

新"山楂含片"是以山楂有效成分提取物为主要原料，并用木糖醇、帕拉金糖醇等无糖原料为基料，配以木瓜、乌梅、甘草、薄荷等中药，经现代科学工艺精制而成的方便口含片。

Thereinto, the content of eucalyptus oil was the most with 27.20%, the next was Terpinen-4-OL (21.27%), N-methyl-laurotetanine (6.32%), Hepladecanoic acid (4.33%), Phytol (3.53%), Ether linoleic acid (3.45%), 2,6-dimethyl-2,6-octadiene (2.96%) and so on.

其中，含量最高的是桉油(27.20%)，其次是松油烯－4-醇(21.27%)、N甲基山鸡椒痉挛碱(6.32%)、十七烷酸(4.33%)、叶绿醇(3.53%)、乙醚基亚油酸(3.45%)、2，6－二甲基－2，6-辛二烯(2.96%)等。

In this paper poly and monomethoxypoly with different molecular weight were used as raw material.

本论文通过不同的合成方法，利用不同分子量的聚乙二醇和甲氧基聚乙二醇为原料，制备了不同类型的聚乙二醇衍生物。

The results indicated that the composite films exhibited much improved gas sensing performance.The phthalocyanine and its a-Fe2O3 embedded nano-particulate LB filmswere prepared by Langmuir-Blodgett technique. The films were characterized by AFM, UV-Vis and FT-IR spectra. The results indicated that the embedded LB films were composed of a-Fe2O3 nanoparticles and isopropoxyphthalocyanine molecules. The gas sensitivity of such prepared composite LB films was greatly improved. The film could detect 5ppm of propyl alcohol at room temperature. The composite films could be considered as gas-sensors for alcohols.

利用LB技术制各了异丙氧基酞菁铜LB膜和酞菁铜包埋球形α-Fe_2O_3纳米粒子的杂化LB薄膜，对其AFM、紫外和红外光谱的研究表明，利用LB技术可以实现酞菁与α-Fe_2O_3纳米粒子的有序组装，而且杂化薄膜对醇类气体的灵敏度有较大幅度提高，如对浓度为5ppm正丙醇的灵敏度为3.85，因此，杂化薄膜可以作为室温下醇类气体传感器进行开发研究。

The integrated analytical results show that the novel ligand coexists in ketoform and enolform structures under the measuring conditions, the ketoform structure may change into the enolform structure during the coordination and bonds with the central ion by two O atoms of the enolized hydroxyl group of pyrazolone ring and H2O and the N atom of the imine group and the N atom containing H of benzimidazole ring by losing the proton. And the coordination number of these complexes is four.

综合各种分析结果显示：配体在测试条件下以酮式和烯醇式结构共存，配位时酮式可能转化为烯醇式结构，按去质子的方式以吡唑啉酮环羟基和H2O上的两个O原子以及亚胺基上的N原子和苯并咪唑环上的含氢N原子与中心离子成键，配合物的配位数为4。

It has been demonstrated that the methods are successfully used for QSRR studies of quinazoline derivatives, alkypyridine, haloid alkane, ketone, alcohol, sulfur alcohol compounds.

本文成功地用该方法对喹唑啉类、烷基吡啶化合物、卤代烃、醇、羰基化合物和硫醇化合物的结构保留关系进行了探讨。

Free tryptophane, docosoic acid and methyl 14-methy pentadecanate were isolated and identified as monomeric compounds also for the first time from Panax plants. Malonyl-ginsenoside 〓, ginsenoside Ro,〓, Re,〓,〓,〓(8 saponins) and stigmasterol were isolated and identified for the first time from the fruits and molonyl- ginsenoside 〓 was also the first from the plant of panax quinquefolium.

游离色氨酸、二十二碳酸及14-甲基-十五碳酸甲酯是首次从人参属植物中分离鉴定的杂环α-氨基酸和脂肪羧酸类单体化合物；丙二酸单酰基人参皂甙〓、人参皂甙〓及豆甾醇是西洋参果中首次分离鉴定的8种单体皂甙和1种甾醇化合物，M-〓亦为西洋参中首次分离鉴定的皂甙化合物。

The results of the dissertation were concluded as follows:(1) It is essential to deposit a basic additive on the Mo-based catalysts for the synthesis of CH_3SH. The potassium-doped Mo-based catalysts exhibit the highest activity than that of the catalysts doped with the otherⅠA andⅡA group basic promoters. H_2-TPR and LRS characterizations suggest that the addition of a base leads to the transformation of octahedrally coordinated Mo to tetrahedrally coordinated Mo, thus leads to the split of low temperature reduction peaks. The interaction between the basic components and Mo lead to the formation of B-Mo interface phase, which are closely correlated with the formation of CH_3SH.(2) It has been found that Fe, Co, Ni and Te have evident promoting effects for the K-Mo/SiO_2 catalysts.

主要结果归纳如下：(1)在Mo基催化剂中，必须添加碱才具有可观的合成甲硫醇活性，在IA和IIA族元素中，K是最佳的碱促进剂，当K/Mo摩尔比为2，前驱体为K_2CO_3，采用共浸法制备的K-Mo催化剂活性最高。H_2-TPR和LRS表征显示，碱的加入导致表面八面体钼氧物种向四面体转化，催化剂的低温还原峰发生分裂，碱助剂与钼之间存在强相互作用形成了B-Mo"界面相"，该物种与合成甲硫醇密切相关。

A novel β-cyclodextrin graft copolymer was synthesized by immobilizing β-CD onto the linear chain of PVA through acetalization reaction.

利用缩醛化反应将醛基化β环糊精固载到聚乙烯醇大分子链上，合成出了聚乙烯醇固载β环糊精的线性环糊精高分子，其最佳反应条件是反应时间 2h ，温度 70℃，β CD 6 CHO与PVA的质量比小于等于 4∶1。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。