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In this research, we used Trifluoroacetic anhydride as a derivatizing agent to esterify the trace glycerol in biodiesel, followed by the determination of trace glycerol using microwave assisted headspace SPME extraction technique combined with GC-ECD.

本研究利用三氟醋酸酐与生质柴油中的微量甘油进行酯化反应,反应后的衍生物以本实验室开发的微波辅助顶空固相微萃取装置采样,并以气相层析仪搭配电子捕捉侦测器作分析。

Supersonic wave disperse research indicated, ethanediol as the disperse medium, it could got suspending liquid about for firve days, but relatively large in grain size. However, combined use of lauryl sodium sulfate and maleic anhydride as disperse medium, the disperse result among water was better than the former, and it would be steady for two days.

超声分散研究表明,使用聚乙二醇作为分散介质,可得到分散五天左右的悬浮液,但分散后粒度较大,使用十二烷基硫酸钠和顺丁烯二酸酐混合作为分散介质在水中分散效果较好,可稳定两天左右。

Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5:1)中和-2,6-二羟基甲苯环合得1,3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

The low phosphate scale and corrosion inhibitor consists of hydroxyl ethylidene bisphosphoric acid in 0.5-1 mg/l, hydrolyzed polymaleic anhydride in 0.5-2 mg/l and polyasparic acid in 1-2 mg/l, with the total concentration being 3 mg/l.

还含有0.5~2mg/L的水解聚马来酸酐和1~2mg/L的聚天冬氨酸,低磷阻垢缓蚀剂的总质量分数之和为3mg/L。

They were unaware of the extrarenal and renal factors separate from GFR that might influence BUN and reported that serum creatinine concentration was not a reliable indicator of kidney damage.22 Morris subsequently developed, produced, and sold a reduced-protein diet, KD, for dogs with renal failure.

没有被注意到的肾外和肾脏因素被肾丝球体过滤率做分离,其有可能影响血中尿素氮,报告也指出血清肌酸酐浓度并不是一个可靠测量肾脏损害的指标。22 Morris随后为了肾衰竭的狗开发出降低蛋白质的饮食、进而生产、分装做销售。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&(One—pot Synthesis),由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4,4\'—二氨基二苯醚、3,4\'—二氨基二苯醚、2,2—双[4—(4—氨基苯氧基苯基]丙烷和2,2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&O(来源:88AB57C论文网www.abclunwen.comne—pot Synthesis,由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4,4\'—二氨基二苯醚、3,4\'—二氨基二苯醚、2,2—双[4—(4—氨基苯氧基苯基]丙烷和2,2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

The process comprises the subsequent steps a through e: a reacting phthalic anhydride with fluorobenzene or a derivative thereof in appropriate reaction conditions; b over reducing the product obtained in step a at the ketone moiety; c reducing the product obtained in step b with sodium dihydro-bis (2- 15 methoxyethoxy) aluminate to the corresponding alcohol ; d chlorinat ing the alcohol obtained in step c ; e inserting CO into the product obtained in step d through an appropriate Pd-containing catalytic system.

该方法包括以下步骤a~e:a使邻苯二甲酸酐与氟苯或者其衍生物在适当的反应条件中反应;b完全还原步骤a中获得的产品的酮部分;c用二氢-二(2-甲氧基乙氧基)铝酸钠将步骤b中获得的产品还原成相应的醇;d对步骤c中获得的醇进行氯化;e通过适当的含Pd的催化剂体系,将CO插入到步骤d中获得的产品中。

In recent years, photochromism has great development in basic study and application. Especially heteraryl fulgide family compound attracts more attentions of scientists and engineers.

近年来,有机光致变色学在基础研究和应用开发两个方面都获得了重大进展,其中芳杂环取代俘精酸酐家族化合物是最引人注目的热点之一。

For 5-selenazolyl fulgide. In steady state, the Z and E photoisomerization is easily observed only by the change of absorption spectra.

在稳态条件下,5-硒唑俘精酸酐只能观察到Z和E之间的光异构化,而不能观察到它们的光环合产物。

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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面,更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。

You rap, you know we are not so good at rapping, huh?

你唱吧,你也知道我们并不那么擅长说唱,对吧?