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The amidation and esterification of different cyclic anhydride s with aniline and phenol gave different major products,and the routes were optimized.

结果表明,环酐的分子结构直接影响反应结果,当酸酐分子存在共轭结构时以N-芳基内酰胺为主要产物。

A series of new style crude oil pour point depressants were synthesized by aminate of acrylic alkyl ester and maleic anhydried bipolymer.

通过丙烯酸高碳酯与马来酸酐二元共聚进行胺解反应得到一系列新型高凝原油降凝剂,并进行筛选,从中选出丙烯酰高碳胺与共聚物结合后的降凝剂降凝效果最好,凝点降幅大于10℃;进一步回归出加剂和未加剂原油的全粘温方程,方程呈对数关系。

In connection with the character of Boc L-Glutamic Acid and aminoacetic acid structures, the reaction of aminoacetic acid acylated via Boc Anhydride has been studied on the condition of CH3OH in the paper. The yield of the derivatives is characterized by the melting point, the content of carboxylgroup and the product purity. The results showed that the best experiment condition is followed.

本论文以甲醇作为均相反应介质,Boc酸酐与谷氨酸为原料,在碱性条件下,以产物的熔点,羧基含量以及产物纯度作为产物质量确定的指标,最终得出N-Boc-谷氨酸的合成最优条件。

Aminoacetic acid;Boc- Glutamic;synthesize;optimize

Boc酸酐;谷氨酸;合成;方法优化

Poly-[N-(2-hydroxyethyl)-L-glutamine] was then obtained by aminolysis of PBLG with 2-aminoethanol.

以L -谷氨酸为单体,经r -羧基的苄基保护,与光气/甲苯液反应制备L-谷氨酸苄酯的羧酸酐,均聚得L -谷氨酸苄酯,然后经由 2 -氨基乙醇胺解得聚 [N -( 2 -羟乙基)-L -谷酰胺 ] 。

Retrospective analysis of the previous ascitic fluid showed high creatinine levels, confirming the ascitic fluid to be urine.

回溯分析原来的腹水发现,有高浓度的肌酸酐,证实这腹水就是尿夜。

IR analysis indicated that both of the results were accorded with their standards IR spectrum and that the products of alkylation and animation were polyisobutylene succinic anhydride and ashless dispersant TEPA.

通过烃化产物和胺化产物的红外光谱分析,并分别与其标准谱图对照比较,看出产物红外谱图与标准谱图相符,可以确认烃化产物和胺化产物即为聚异丁烯丁二酸酐和聚异丁烯丁二酰亚胺无灰分散剂。

To improve water solubility of betulin, two acyl groups were introduced at C-3 and C-28 hydroxy groups of betulin. 3, 28-di-O-glutaryl-betulin was synthesized with pyridine as solvent and DMAP as catalyst from betulin and glutaryl anhydride.

为了增强桦木醇的亲水性,对桦木醇的C-3位、C-28位羟基进行修饰,在吡啶作溶剂、二甲基氨基吡啶作催化剂的条件下,与戊二酸酐反应合成桦木醇戊二酸酯。

Cloud point curves from light scattering experiment verify the calculation results;The agreement between the cloud point curve s and the binodal is quite well.

用浊点测定、傅里叶变换红外光谱和微差扫描热分析等方法研究了苯乙烯-顺丁烯二酸酐共聚物与苯乙烯-丙烯腈共聚物共混物的相容性。

The para-/ortho- product isomer ratio is 6.2 for the nitration of chlorobenzene at 18℃ for 8h with n/n(NH4NO3)=5. The para-/ortho- product isomer ratio is 14.0 for the nitration of bromobenzene at 0℃ for 8h with n/n(NH4NO3)=5. The pars-product, p-nitrobromobenzene, from the nitration of bromobenzene in [HSO4] under 0℃ precipitates with 98% purity, which facilitates the separation of the pure isomert.

其中氯苯在18℃下反应8h,三氟乙酸酐/硝酸铵为4时产物的对邻比达到6.2,而溴苯在0℃下反应8h,TFAA/硝酸铵为5时产物的对邻比可达到14.0,并且生成的对硝基溴苯可以从反应液中析出,得到对硝基溴苯含量为98%的产物。

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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面,更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。

You rap, you know we are not so good at rapping, huh?

你唱吧,你也知道我们并不那么擅长说唱,对吧?