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Based on analyzing the generation mechanism and quality characteristics of reclaimed acid from benzol refining and comparing varies kinds of purification methods, the operation easily, the technical process simple extraction method is used to purify the reclaimed acid and the dosage of the extraction agent and extraction power are studied in detail.

对精苯再生酸的生成机理、质量特性进行了分析,通过比较各种再生酸净化方法的优缺点,选用操作简便、工艺简单的再生酸净化方法——萃取法对再生酸进行处理试验,并对萃取剂的用量、萃取能力等进行了详细的研究。

Purified GO could oxidize both glycolate and glyoxylate, and both activities highly depended on FMN. The activity of glyoxylate oxidation was weaker than that of glycolate. During purification or storage of purified GO, the ratio of glycolate to glyoxylate oxidation was progressively enhanced.

纯化的菜心叶片乙醇酸氧化酶对乙醇酸和乙醛酸均有氧化活性,且两者都强烈依赖于FMN,但对乙醛酸的氧化能力相对较弱;在酶的纯化及纯化酶的贮存过程中其两催化活性的比值均呈逐渐升高的趋势。

The article introduces the biological functions and producation of ornithine in the world, including of breeding of mutant, questing for fermentation condition and industrializating production.

介绍了L-鸟氨酸的生物功能及发酵法生产L-鸟氨酸的过程及研究状况,包括产L-鸟氨酸的菌种,发酵条件的摸索及优化和国外L-鸟氨酸的工业化生产情况。

We prepared the pyrethric acid II through four reactions: esterification, oxidation, decomposition, diesterification. And the original synthesis route of the pyrethric acidII was improved: the yield of oxidation of allyl rise through increasing the activity of Selenium dioxide; in the document, tert-butyl-trans -2, 2-dimethy1-3-(2"-methoxycarbony1-1"-propenyl)cyclopropanecarboxy late was synthesized from tert-butyl-trans-2,2-dimethyl-3-(2 -formyl-r -propenyl) cyclopropanecarboxylate with two steps, with low yield.

我们经过酯化,氧化,成双酯,热分解四步反应,成功地得到了第二菊酸,并改进了原第二菊酸的合成路线:通过改变二氧化硒的活性提高了烯丙甲基的氧化产率;将原路线中醛氧化成羧酸、羧酸酯化的两步反应改为醛和甲醇、二氧化锰等作用一步直接酯化的方法,减少了反应步骤,提高了总收率。

The optimum reaction conditions were as follows: rosin 5 g, m: in: m 1:2:2, palladium chloride 0.090 %, n: n1:10, hydrogen pressure 5 MPa, reaction temperature 160℃ reaction time 3 h, mass fraction of abietic acid could be under 1%, mass fraction of dehydroabietic acid was 5.6%, which conforms to the national standards. The regeneration of catalyst was investigated. After cycling five times, the product of hydrogenated rosin still conforms to the national standards without any treatment of catalyst.

在松香5g、m:m:m1:2:2、氯化钯0.090%、n:nl:10、氢气压力5MPa,反应温度160℃,反应时间3h的较佳工艺条件下,产物氢化松香中极酸的质量分数小于1%,去氢枞酸的质量分数5.6%,符合GB/T 14020-2006国家标准;并对催化剂的重复使用性能进行了考察,催化剂相不经过处理直接重复使用5次后,产品氢化松香仍然符合国家标准中关于枞酸和去氢枞酸的指标要求。

The isomerization of resin acid was studied by HCl catalysis method, high temperature catalysis method and microwave-assisted method. Separation of abietic acid was analyzed with recrystallization method and many organic amine salt methods; Using abietic acid separated from resin acid as raw materials, 6 compounds of abietic-type resin acid derivetives were synthesized.

从产率、纯度和成本等方面分析对比了改进的二戊胺盐法、A胺盐法、B胺盐法和文献报道的二戊胺盐法分离提纯枞酸;以得到的枞酸为原料,进行氧化合成,得到6种枞酸的氧化衍生物,通过柱分离得到2种枞酸氧化衍生物纯品,并测试了其抑菌和对家蝇的拒食活性。

Most sugars, organic acids, phenolic acids and most amino acids increased significantly with elevated CO_2. The treatment, 950±50μmol·mol-1 CO_2 enrichment for 6 h every day had more obvious effects than the treatment, 950±50μmol·mol-1 CO_2 enrichment for 3 h every day. Levan, sucrose, arginine, oxalic acid, alanine, malic acid, acetic acid, lactic acid cinnamic acid,ρ- hydroxybenzoic acid and benzoic acid increased significantly.

CO_2施肥黄瓜根系分泌有机酸、氨基酸、糖和酚酸的总量增加,上、下午均施肥的处理分泌数量最多;CO_2施肥显著促进了果聚糖、蔗糖、草酸、苹果酸、乙酸、乳酸、多数氨基酸、肉桂酸、对羟基苯甲酸和苯甲酸等组分的分泌;单位鲜重根系分泌糖和酚酸的数量增加,多数氨基酸保持不变或降低,但有机酸分泌规律不一致。

Results showed that amino acid cheleted iron was molecular coordination compounds in liquids and had low molar conductivity, Among them, methionine chelated iron and glycine chelated iron was stable in pH 2.0~6.0 solution, the histidine cheleted iron was stable in pH 2.0~8.0 solution .

为探索更有效的脱酸方法,实验研究了在固相体系中气流A脱酸的可行性,结果发现,气流A既能起到很好的脱酸效果,又能缓慢地引发螯合反应,维持反应体系温度的稳定,其脱酸率达到94.60%。

The results showed that the mixed-addenda heteropolyacids H6PM o9V3O40,H10PMo5V7O40and H11PMo4V8O40 c an improve the conversion of 2-octanol,selectivity for hexanoic acid and the r ate of production.When the amounts of heteropoly acid are 14%,10%and 14% of the weight of 2-octanol,co...

结果表明:H6PMo9V3O40、H10PMo5V7O40、H11PMo4V8O40等多元杂多酸均可提高仲辛醇的转化率、己酸产率和己酸选择性,并确定了这3种催化剂的最佳用量:当它们分别为仲辛醇质量的1 4%、1 0%、1 4%时,仲辛醇转化率可达98 3%、97 6%、100%;己酸的选择性可达85 7%、85 8%、78 8%;其性能明显优于钒催化剂。

Malate dehydrogenase is an essential enzyme in TCA cycle. And it can be used in the separation of D-malic acid, which is an important chiral 4-carbon dicarboxylic acid in pharmaceutical industry.

苹果酸脱氢酶(Malate dehydrogenase,MDH)是生物体三羧酸循环中的一种关键酶,在药物生产过程中利用其催化特性可实现DL-苹果酸的拆分,从而得到D-苹果酸这种重要的手性碳源,具有较高的经济价值。

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呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

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然而,要让一个真正的引用,你需要提供详细的个人和财务信息。