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The dyes were extracted from textiles composed of natural or chemical fibers by methanol under ultrasounication, and then eluted with gradient by acetonitrile and 5 mmol/L ammonium acetate from an RP-C18 column with two segments in effluents. The first effluents accommodated Acid Red 26, Direct Blue 6, Direct Black 38 and Direct Red 28 with negative ionization mode, while the second accommodated Basic Red 9, Basic Violet 14, Disperse Blue 1, Disperse Orange 11 and Disperse Yellow 3 with positive ionization mode. Thus the investigated compounds could be identified simultaneously with single-run analysis no matter which type of the fibre the sample was and no matter which category of the dye the analyte was.

用甲醇超声同时提取天然纤维和化学纤维上的染料,以5 mmol/L乙酸铵和乙腈为流动相在C18柱上于前段洗脱酸性红26、直接蓝6、直接黑38和直接红28(采用电喷雾质谱负离子模式检测),于后段洗脱碱性红9、碱性紫14、分散蓝1、分散橙11和分散黄3(采用电喷雾质谱正离子模式检测),实现了对不同种类纤维织品中分属4类性质不同染料的一次提取和一次分析检测。

The research presented here is aimed at exploring the effect of DTT on the in vitro fibril formation of hen egg-white lysozymes with four disulfide bonds. In this work, we specifically addressed the effect of DTT concentration under different incubation temperatures on the hen lysozyme structure and fibril formation, the effect of addition of DTT at later time points on the amyloid fibrillization of hen lysozymes, and the effect of concentration ratio between reduced and oxidized forms of DTT on the fibril formation of lysozymes.

本研究以具有四对双硫键的母鸡蛋白溶菌酶为蛋白质模式系统,在含盐类之酸性溶液环境下诱导生成类淀粉纤维,再配合二硫代苏糖醇破坏溶菌酶中的双硫键,探讨:(1)不同温度下加入不同DTT浓度对溶菌酶类淀粉纤维形成之影响,(2)不同生长时期加入DTT对溶菌酶类淀粉纤维形成之影响,(3)不同比例之DTT和氧化态DTT浓度对溶菌酶类淀粉纤维形成之影响。

According to the results of the former study in our laboratory, trans-1, 2-cyclohexanediol is produced with a lot of acids and water, for extraction of trans-1, 2-cyclohexanediol from the solution, ethyl acetate and butyl acetate were used as extraction reagents, the solubility data of the trans-1, 2-cyclohexanediol in corresponding mixed solvents of some sorts of acetates and water are needed.

根据本实验室前期研究结果可知,反式-1,2-环己二醇是在酸性和大量水存在的条件下得到的,为了把反式-1,2-环己二醇从反应液中萃取出来,本工艺所采用的萃取剂是乙酸乙酯和乙酸丁酯,需要获得反式-1,2-环己二醇在这些酯类与水混合溶剂中的溶解度数据,因而对反式-1,2-环己二醇进行相关固液相平衡的研究是非常迫切和必要的。

In the second part, we studied the reactions of tonghaosu analogs with mercaptans alcohols and organic metallic reagent under acid condition. Moreover, we synthesized and determined a natural compound by using this kind of reaction.

第二部分研究了茼蒿素类似物在酸性条件下与硫醇、醇、有机金属试剂发生亲核取代反应,同时通过这类反应合成了一天然产物。

Sample matrix are discharged by the pre-column. The mobile phases applied consisted of 0.1% HOAc (pH3.0) acetonitrile-water on extraction column with UV detection at 225nm. Then, coupled-column liquid chromatographic methods for the direct analysis of atrazine and simazine in urine was established. As a result, the system showed good chromatographic property in the on-line analysis of atrazine and simazine in urine.

使用该系统对尿中的莠去净和西玛津残留进行了分离分析,以含有0.1%乙酸的酸性水缓冲液对加标尿液中莠去净类化合物保留在预柱上,干扰分析的大分子被排阻而无保留通过,其它干扰分子保留小而通过,再切换六通阀,以乙腈和0.1%乙酸水溶液进行梯度洗脱,进而在下一级ODS分析柱上进行分离(紫外检测225nm),两种除草剂的分离分析取得了良好的定性定量结果

The electrochemical behavior on tetramethylquinone in n-butylpyridini-um chloride-aluminum chloride, a room temperature molten salt , is dependent on theacidity of this melt.

四甲基苯醌在氯化正丁基吡啶-AlCl_3室温熔盐中的电化学行为,和室温熔盐的酸碱度有关,在碱性熔盐中,四甲基苯醌以不络合的形式存在,电极上的还原过程是一个ECE过程;在酸性熔盐中,形成络合物TQ(AlCl_3)_m,络合数m为1,2,3,随熔盐酸度变化,此外,醌类物质芳香环上的取代基,也影响其电化学性质。

The rocks of early Proterozoic and Archaean contain the lower potassium feldspar and lead number in potassium feldspar is lower than 10% of lead in the whole rocks.

中文摘要:在中-酸性岩浆岩、碱性岩浆岩、片麻岩及混合岩等岩石类型中,钾长石是含铅最高的造岩矿物,其铅含量是全岩铅含量的2~10倍,云母类矿物铅含量的3~16倍,石英铅含量的6~32倍。

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推荐网络例句

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。

This is not paper type of business,it's people business,with such huge money involved.

这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。