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The direct incorporation of U-13C glucose was estimated by the intensity increase of m/z to F(F was parent fragment, and n was the carbon number in the fragment), while the total isotope incorporation from the added 13C could be calculated according to the abundance ratio increment summation from m/z (Fa+1) through (Fa was the fragment containing all original skeleton carbons, and T was the carbon number in the amino acid molecule). The 13C enrichment in the target compound was expressed as atom percentage excess, and that of D-amino acid needed to be corrected by the coefficient of hydrolysis-induced racemization. The 13C enrichment reflected the carbon turnover velocity of individual amino acid enantiomers, and was powerful to investigate the dynamics of soil amino acids.

外加葡萄糖直接合成氨基酸的比例可利用质谱碎片的相对强度变化来评价(n为质谱碎片F中含有的碳原子数目);而源于葡萄糖的13C同位素在氨基酸分子中的富集程度是所有同位素峰相对强度变化的总和。13C在目标化合物中的富集比例用原子百分超评价,D氨-基酸的APE还需进一步利用水解诱导的外消旋化系数校正。13C在目标化合物中的富集程度可反映各氨基酸手性异构体的碳循环速率大小,是研究土壤氨基酸动态变化的有力工具。

To obtain new functional aromatic polymer material, the reaction of acenaphthene with nitrobenzene under high active catalyst of AlCl3 was investigated at room temperature and ambient atmosphere.

为制备更多新型功能高分子中间体,研究了高活性lewis酸AlCl3催化作用下,苊与硝基苯在温和条件常温常压下的反应。

A novel family of ester acetal molecular glass materials has been created by the reaction between monocarboxylic acid and divinyl ether s.

通过一元羧酸和二乙烯基醚的反应,我们得到了一种新颖的酯缩醛结构分子玻璃。

The results of clinical assessment showed that levosimendan was safe and effective which could improve the prognosis of the patients and kept normal blood kinetics. By improving the reported synthetic route, levosimendan was synthesized from acetanilide via eight steps of reaction.

本论文探索了左西孟旦的合成路线,对文献报道的合成工艺进行了合理有效的改进,以乙酰苯胺为原料,最终经Friedel-Crafts反应,羰基α-位溴代,丙二酸二乙酯缩合,水解,脱羧,环合,拆分及重氮化加成等八步反应合成了左西孟旦。

Ellagic acid helps reduce free radical damage and protect the nuclei of cell DNA against damage.

柔花酸能有效对抗游离基,更深层保护细胞中的DNA。

They have been widely used in aerospace structures, aircrafts, dielectrics, some other government issues and civil industry products in recent years.

作为一种20世纪70年代发展起来的优异热固性树脂,氰酸酯树脂是目前树脂基复合材料研究领域的重点和热点基体材料之一。

The ten target compounds from alkyl substituent to aryl substituent that have not yet been reported,which was obtained by dehydration, Subsequently treated with sodium nitrite resulting nitroso compounds and then reduced.

本论文以2-羟基-3-萘酸和邻巯基苯胺为原料,通过分子脱水、亚硝化、还原等反应合成了10个不同取代基团的4-苯并噻唑基-[1,2-d]萘并噁唑衍生物,并优化了合成的工艺条件。

As support, Agarose can benot only used in normal condition, but also in denaturalization (for example, 6 mol/Lhydrochloric acid carbamidine or 8 mol/L urea). Herein, the preparation of IMACmatrixes were conducted using agarose as support, carboxymethylated aspartate as chelating ligand and Co~(2+) and Ni~(2+) as chelating center ions.

本实验用琼脂糖作为基质,选用四配位,与金属离子有较强作用力的羧甲基天冬氨酸为配基,以Co~(2+)、Ni~(2+)作为螯合金属离子,合成了一系列金属螯合亲和色谱填料,并对其蛋白质分离性能进行了研究。

BACKGROUND: Based on documents abroad and home, both alginic acid and carbomer are used to prepare gel matrix of lithium carbonate tablets; furthermore, hydroxypropyl methyl cellulose, a kind of water-soluble skeletal material, can be used as controlled release matrix of lithium carbonate tablets.

摘要背景:目前国内外文献报道的碳酸锂缓释片多采用海藻酸、卡波姆等制备凝胶型骨架片,同样作为水溶性骨架材料的羟丙基甲基纤维素,也可作为碳酸锂的缓释基质。

We synthesized polynitrobenzenes by oxidation of polynitroanilines by peroxysulfuric acid (hydrogen peroxide dissolved in sulfuric acid, it is also known as Caro's acid) several years ago.

我们曾在若干年前用过硫酸(过氧化氢溶于硫酸中,亦称卡洛氏酸)氧化多硝基苯胺而合成了多硝基苯类(硝基数3至6)。

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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。

This is not paper type of business,it's people business,with such huge money involved.

这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。