酸基

In this report, the 59Tc labelling of Annexin V fragment modified with HYNIC (HYNIC-Anx13) using Tricine, EDDA or EDDA/Tricine as coligands was described. The effect of various factors on 99Tc labelling was investigated. Biodistribution studies in normal mice and gamma imaging of apoptosis in rats induced by cyclophosphamide were performed.

为探讨99Tc标记的HYNIC-Anx13用于细胞凋亡显像的可能性，分别以N-［三甲基］甘氨酸，乙二胺－N，N'-二乙酸和EDDA/Tricine为协同配体，对经6-肼基烟酰基修饰的膜联蛋白V片段(HYNIC-Anx13)的99Tc标记条件和主要影响因素进行了研究，并完成了HYNIC-Anx13的99Tc标记物在正常小鼠体内的生物分布和大鼠细胞凋亡模型的显像实验。

On the base of molecular structure design, the mechanism and technique of the synthesis of 2-(acryloyloxy ethyl trimethyl-ammonium chloride/2-acrylamido-2methylpropane sulfonic acid/acrylamide (AETMAC/AMPS/AM) amphoteric terpolymers by radical co-polymerization in aqueous solution was studied systematically.

依据分子结构设计理论，将2—丙烯酰氧乙基—三甲基氯化铵/2—丙烯酰胺基—2—甲基丙烷磺酸/丙烯酰胺(AETMAC/AMPS/AM)三种单体进行水溶液自由基共聚，合成了AP系列两性离子聚合物。

They were eucalyptol, bicyclo［2.2.1］heptan-2-one,1,7,7-trimethyl-,(1R)-, borneol, 1-methyl-2-(1-methyl ethenyl)-(1R-cis)-cyclobutaneethanol, limonene, 1-hydroxymethyl-7,7-dimethy lbicyclo［2.2.1］heptan-2-one,-spathulenol, 3,7,11,15-Tetramethyl-2-hexadecen-1-ol, isocitronellol,-9-Octadecenoic acid, heneicosane, respectively.

阿给中共有11个阿给炭没有检测出的成分，包括桉油精、D-樟脑、冰片、(1R-cis)- 1-甲基-2-(1-甲基乙烯基)环丁基乙醇、二戊烯、1-羟甲基-7，7-二甲基-双环［2.2.1］庚-2-酮、-匙叶桉油烯醇、3，7，11，15-四甲基-2-十六碳烯-1-醇、异香茅醇、-9-十八碳烯酸和廿一烷。

The fabrication of SiNW was used by "electroless etching" which was when (100) c-Si was immersed in the solution containing silver nitrate and hydrofluoric acid. Si was etched by fluoric ion and released electrons to combine with silver ion to form Ag particles.

制作矽奈米线阵列的方式为无电镀蚀刻法，系将一p-type(100)之矽基板置入氢氟酸与销酸银的混合蚀刻液中，当溶液中之氟离子与矽基板接触后，矽即被解离成矽离子并放出一颗电子。

Teflubenzuron was synthesized from 2,4-difluoronitrobenzene and 2,6-dichlobenil as starting reagent through six-step reaction with the yield of 75.3%.3,5-Dichloro-2,4-difluoroaniline was synthesized by chlorination,reduction reaction from 2,4-difluoronitrobenzene,the yield was 84.5%;2,6-difluorobenzamide with the yield of 87.7% was synthesized by fluoridation and hydrolysis from 2,6-dichlobenil.

以2，4-二氟硝基苯和2，6-二氯苯腈为起始原料，经过6步反应合成伏虫隆，总收率为75.3%。以2，4-二氟硝基苯为原料，经过氯化、还原反应合成3，5-二氯-2，4-二氟苯胺，产率为84.5%；以2，6-二氯苯腈为原料，经过氟化和水解，制得2，6-二氟苯甲酰胺，产率为87.7%；将Ⅱ与二碳酸酯酰化，合成2，6-二氟苯甲酰异氰酸酯，产率为91.3%；Ⅲ与Ⅰ加成，得到杀虫剂伏虫隆，产率为95%。

Isocyanic acid ; Hydrogen abstraction reaction ; ab initio ; Formyl radical ; Rate constant

异氰酸；氢转移反应； abinitio ；甲酰基自由基；速率常数

Then, N-for-aspartame was obtained from the reaction of 3-formyl-4-carboxymethyl-1,3-oxazolidine-5-one and L-phenylalanine methylester hydrochloric acid under sodium acetate anhydrous in ethyl acetate, and the target product was prepared after removing formyl in the mixture system of hydrochloric acid, methanol and water, the yield of aspartame reaches 89.2%.

最后，用3-甲酰-4-羰基口恶唑烷-5-酮乙酸与L-苯丙氨酸甲酯盐酸盐在溶剂中进行接肽反应，然后在甲醇/盐酸混合体系中进行脱甲酰保护基，从而得到最终目标产物，产率为89.2%。

A sequential extraction technique to fractionate P and the method proposed by Bremner to separate N in different fractions were used.

本试验利用Sui 和 Thompson (1999)序列萃取法，以不同强弱的萃取剂来划分土壤中的磷，将土壤磷划分为水萃取磷、碳酸氢钠萃取有机磷及无机磷、氢氧化钠萃取有机磷及无机磷、盐酸萃取磷及残余磷；利用 Bremner (1965)的土壤有机态氮划分法将土壤有机态氮划分为水解性全氮、水解性铵态氮、胺基醣态氮、胺基酸态氮及不可辨认的水解性氮。

Localization of Vps74p at the Golgi is not dependent on the N-terminal phosphorylation, but on its C-terminal domain.

Vps74p坐落在高基氏体是不需倚赖氮端被磷酸化，但是需要碳端的胺基酸序列。

In order to find high active pesticide containing heterocycle, six novel terephthaloyl bisthioureas containing 1, 3, 4-thiodiazole were synthesized by the reaction of 2-amino-5-alkyl-1, 3, 4-thiodiazoles with terephthaloyl diisothiocyanate.

摘 要：为寻找高活性的含杂环农药，由中间体5-烷基-2-氨基-1， 3， 4-噻二唑与对苯二甲酰基二异硫氰酸酯反应，合成6种新的含1， 3， 4-噻二唑环的对苯二甲酰基双硫脲化合物Ⅲaf。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。