酸基

Firstly, synthetic racemates of β- amino acids were resolved into their enantiomers by ehiral ligand - exchange flash chromatography with L - hydroxyproline chemically bonded to irregular silica as the stationary phase and aqueous solution containing cupric ions as the mo

首先合成L-羟脯氨酸硅胶键合手性固定相，用于快速色谱中3-羟基-4-甲氧基-β-苯丙氨酸对映体的制备分离，考察了流动相中Cu^2＋浓度、样品体积等因素对分离的影响。

The premixing self-assembly solution of horseradish peroxide with poly(sodium 4-styrenesulfonate) is made by blending HRP and polyelectrolyte PSS,and the active.enzyme muhilayer biofilm is fabricated by altemate deposition of and PDDA on the surface of negative ionized PET.

以阳离子化的辣根过氧化物酶和阴离子聚苯乙烯磺酸钠的预混合溶液，与阳离子聚电解质聚二甲基二烯丙基氯化铵通过逐层组装，在阴离子化聚对苯二酸乙二酯表面构建了多层生物活性膜。

The results show that the degradation effectiveness of PVA was optimum when potassium ferrate and sodium hypochlorite were jointly used as the oxidative agent. The removal rate of PVA and COD was more than 98% and 40% under the conditions that the concentration of PVA was 3.0 g/L and the pH value was 7.2, the dosage of potassium ferrate and sodium hypo chlorite were 0.32 g/L and 3.92 g/L, and the reaction time was 50 min. In the process of united oxidative degradation, the chain of PVA was cut off and many low molecular weight compounds were formed. The main degradation products were carboxyl compounds.

结果表明，用高铁酸钾与次氯酸钠联合氧化PVA时，降解效果最佳；在3.0 g/L，pH值为7.2的PVA溶液中，当高铁酸钾与次氯酸钠的投加量分别为0.32 g/L、3.92 g/L，反应时间为50 min时，PVA的去除率大于98%，COD去除率大于40%；在联合氧化降解过程中，PVA断链成小分子物质，最终降解产物主要为羧基化合物。

In the solution,low concentration sulfate ions was determined by a direct titration with barium perchlorate as titrant and thorin as the indicator;the concentration of calcium ions was determined by a direct EDTA titration using Calcon carboxylic acid sodium salt as the indicator.

先用高氯酸将固体混合物溶解形成水溶液，然后以钍试剂为指示剂，用高氯酸钡溶液滴定溶液中的微量硫酸根，并用EDTA法以钙红为指示剂滴定溶液中的钙离子，从而可以计算出钙基脱硫剂的固硫率(表示为脱硫后固体混合物中的钙硫化)。

A method used to simutaniously analyze the residues of herbicides 2, 4-dichlorophenoxyacetic acid (2,4-D), 2-(2,4-dichiorophenoxy) propanoic acid (2,4-DP) and 2,4-dichiorophenoxybutyric acid (2,4-DB) in garlic was developed in our study.

本研究建立了一种应用基质固相分散－高效液相色谱法，同时测定大蒜中2，4-二氯苯氧乙酸、2，4-二氯苯氧丙酸及2，4-二氯苯氧丁酸等3种2，4-D类除草剂残留的方法。

The simple and fast determination method presented is based on initial chelation of Sn4+, Cu2+, Pb2+ and other metal ions with EDTA and its subsequent decomposition with trihydroxybenzoic acid, mercaptosuccinic acid and dithiocarbamic propanoic acid.

本文提出的简易、快速测定方法是用EDTA螯合锡、铜、铅和其它金属离子，然后分别用三羟基甲酸、巯基丁二酸和氨荒丙酸解蔽。

ABSTRACT: In the presence of sodium t-butoxide and DMSO,ethyl 2-oxocyclopentanecarboxylate was subjected to C-alkylation with 2-(4-bromomethylphenyl)propanoic acid with high regioselectivity to give 2-［4-(1-ethoxycarbonyl-2-oxo-1-cyclopentanylmethyl)phenyl］propanoic acid (4) which was followed by hydrolysis,decarboxylation and salt formation to afford loxoprofen sodium in about 72% overall yield.

在叔丁醇钠和二甲基亚砜的存在下，2-丙酸对2-乙氧羰基环戊酮进行C-烷基化，再经水解脱羧，成盐即得洛索洛芬钠，以2-丙酸计算，总收率为72%。

And then re-use the nitroso muscle strain mutagenesis, in order to collect acid analog of GABA as a selection factor has been a 18% increase in production of new strains 42,, this new high-yield flask under the conditions of strain in the process were studied.

然后又对该菌株再采用亚硝基肌诱变，以撷氨酸结构类似物氨基丁酸作为筛选因子又得到一株新的产量提高18%的菌株42，，对此新的高产菌株在摇瓶条件下的工艺进行了研究。

The experimental results show that the composite emulsion of nitrocellulose -alkyd resin acrylate, which is prepared by modifying the nitrocellulose with non -drying or alkyd resin, methyl methacrylate and butyl acrylate monomer under the optimized experimental conditions have good stability and excellent performance.

实验结果表明，以不干性油醇酸树脂、甲基丙烯酸甲酯和丙烯酸丁酯单体为主要原料，在优化的实验条件下对硝基纤维素进行改性，可制得稳定性好的硝化纤维素-醇酸树脂-丙烯酸酯复合乳液。

A process for making an electronic device which comprises applying a nonaqueous plate-resistant ink by ink jet printing to selected areas of a dielectric substrate, optionally laminated with an electrically conductive metal, exposing the plate resistant ink to actinic and/or particle beam radiation to effect polymerisation, adding one or more metal layers by electrolytic or electroless deposition, the upper layer of which is an etchresistant metal, removing the polymerised plate-resistant ink with alkali and finally removing the electrically conductive metal which are optionally directly laminated to the dielectric substrate and not protected by an upper layer of etch-resistant metal by chemical etching wherein the plate-resistant ink is substantially solvent-free and comprises: A 30 to 90 parts acrylate functional monomers free from acid groups comprising mono- or higher functionality wherein 5 to 95% by weight are mono-functional monomers; B 1 to 30 parts acrylate functional monomer containing one or more acid groups; C 0 to 20 parts polymer or prepolymer; D 0 to 20 parts radical initiator; E 0 to 5 parts colorant; F 0 to 5 parts surfactant; and where the ink has a viscosity of not greater than 30 cPs at 40 DEG C and all parts are by weight.

一种制备电子装置的方法，所述方法包括以下步骤：通过喷墨印刷在任选层压了一种或多种导电金属的介电底材的选定区域涂覆非水的阻沉积油墨，将所述阻沉积油墨暴露在光化辐射和/或微粒束辐射中以完成聚合，通过电解沉积或无电沉积增加一层或多层金属层，其中最上层的金属层为一种或多种阻蚀刻金属，用碱除去聚合的阻沉积油墨，最后通过化学蚀刻将任选直接层压在所述介电底材上并且不被一种或多种阻蚀刻金属的上层保护的导电金属除去，其中所述阻沉积油墨基本不含溶剂，并且包含以下组分：A30-90份不含酸基团的丙烯酸酯功能性单体，所述单体包括单官能或多官能单体，其中5-95％重量为单官能单体；B1-30份包含一个或多个酸基团的丙烯酸酯功能性单体；C0-20份聚合物或预聚物；D0-20份自由基引发剂；E0-5份着色剂；和F0-5份表面活性剂；其中所述油墨的粘度在40℃下不高于30cPs，并且所有的份数以重量计。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。