酸基

Part two: Using chloroformic ester reacted with potassuim thiocyanate to get thiocyanic esters. Then reacted with biological substituted pyrimidinamine to synthesize forty two thiourea compounds, thirty eight of them are new compounds. Their structures have been charactered by IR, 1H NMR and elemental analysis.

第二部分：先以氯甲酸酯和硫氰酸钾为原料合成异硫氰酸酯，再与有生物活性的取代氨基嘧啶反应，合成了一系列新的取代嘧啶基硫脲类化合物，合成的42个化合物中有38个为首次合成的新化合物，结构经元素分析、IR及~1H NMR得到确证。

RESULTS AND CONCLUSION: The seeded cells had chondrogenesis in scaffolds under certain conditions.

结果与结论：种子细胞在三维支架中特定条件下有成软骨效应，骨髓间充质干细胞在含20%透明质酸的胶原/透明质酸支架扩增少于3代有成软骨效应，软骨细胞传代数更高仍然有成软骨效应，但脂肪源性成熟基质细胞成软骨效应能力较弱。

Synthesis technology of cinnamyl methyl fumarate containing α,β-unsaturated carbonyl group and its antimicrobial activity was studied.

以α，β-不饱和羰基结构为母体设计合成反丁烯二酸桂醇甲酯，并对反丁烯二酸桂醇甲酯的抗菌活性进行了研究。

The results of magnesium and calcium ions tolerance test indicated that the modified SPS, synthesized from the above two methods,has good chelation with magnesium and calcium ions for the crablike carboxyl and ester group and increase the reaction weight with magnesium and calcium ions for addition of hydrophilic group.Both of the two modified petroleum sulfonates could produce ultra-low interfacial tension at calcium and magnesium ions concentration lower than 600 mg/L,whereas the general petroleum sulfonates could only produce ultra-low value below 300 mg/L.

耐钙镁离子能力测试结果，以大庆炼化公司两种渣油为原料，采用上述两种合成方法制备的改性石油磺酸钠，由于产物中引入蟹爪状羧酯基，对钙镁离子有较强的螯合作用，同时增加了亲水基，增大了表面活性剂分子与钙镁离子的反应量，因而在600mg/L的钙镁离子溶液中获得10-3级的超低界面张力；而普通石油磺酸钠仅能在300mg/L的钙镁离子溶液中获得超低界面张力。

Condensation of cinnamaldehyde with methyl crotonate in the presence of alcohol-flee potassium methoxide gives,after hydrolysis,p-phenyl-benzoic acid in low yield.Its structure has been ascertained by direct comparison with an au- thentic sample.

桂皮醛与α-丁烯酸甲酯在催化剂去醇的甲氧基钾影响下进行反应，得到低产率的对-苯基-苯甲酸，共结构经用已知方法所得同样的酸直接加以比较而确定。

Experiments for deacidification of cyclohexanecarboxylic acid on MgO catalyst were carried out in a fixed bed unit and the effects of temperature, space velocity and the size of catalyst on the catalytic deacidifcation were investigated.

在固定床评价装置上对MgO进行了环己基甲酸脱酸试验，考察了温度、空速和催化剂颗粒尺寸对MgO催化脱酸反应的影响。

A small molecule core (TMP-SK3)with three terminal carboxyl groups was synthesized successfully by the reaction of 1,1,1-trihydroxymethylpropane with the excessive sebacic acid diacetic anhydride.

以1，1，1-三羟甲基丙烷与过量癸二酸二乙酸酐反应，制得了端羧基的三官能度小分子核三癸二酸三羟甲基丙烷酯（TMP-SK3）。

In the third part of this paper, a facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

对肼基苯磺酸是由对氨基苯磺酸经亚硝酸钠重氮化得到的重氮盐用亚硫酸氢钠还原、水解、硫酸酸化制得，本文经多次实验确定了反应原料、用量及反应条件，得到的产品纯度好，产率高。

The spectra of X-ray diffract revealed that its crystal is B type and the value is about 18%, far lower than that of ordinary maize starch. With the method of chemistry modification, we modified the amylose starch with acetates. The result showed that the best reaction condition was at the ratio of 1:5.3 (glucose: acerbity), with MSA 1.5% catalyzer, at 75℃ for 3 h.

利用化学改性法对高直链玉米淀粉进行醋酸酯化改性，最佳反应条件为，淀粉葡萄糖基与酸的质量比1：5.3、催化剂甲磺酸用量为体系的1.5%、反应温度75℃、反应时间3 h，在此条件下可制备取代度为2.84的醋酸酯淀粉，比普通玉米淀粉高0.78。

The organic modification of nano-scale TiO_2 and the effect factors were studied by using dodecanoic acid and hexadecanoic acid as modifier.

本文选用月桂酸和棕榈酸作为改性剂，让羧基与TiO2的羟基以化学吸附的形式连接起来，使纳米TiO2表面改性为亲油性。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。