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In this work, isobutyl isobutyrate was prepared by the condensation of two molecular isobutyraldehyde in the presence of aluminium isobutoxide catalyst system.

依据间歇反应所得一系列数据,确定了异丁醛连续缩合反应工艺流程;考察了以异丁醛为原料,在 5~10℃,停留时间 1 5~ 2h ,在异丁氧基铝催化体系作用下,两分子异丁醛缩合成一分子异丁酸异丁酯;脱除催化剂后,粗产品精制得到纯度≥ 99 5 %的异丁酸异丁酯,异丁醛的转化率≥ 98 5 %,异丁酸异丁酯的选择性≥95 %。

At first, urea decomposed into isocyanic acid, which interacted with ZnO to form a relatively steady isocyanate species. Then propylene glycol reacted with isocyanate species to form hydroxypropyl carbamate, and the HPC lost ammonia to form PC.

结果表明,该反应是分步进行的,首先尿素分解生成氨气和异氰酸,异氰酸与ZnO作用形成异氰酸物种,在丙二醇的作用下生成中间产物羟丙基氨基甲酸酯,然后由HPC脱氨气生成PC。

Chinensis and Kuruma prawn M. japonicus increased at 12 and 48 hours post-inoculum, but decreased sharply after 36 and 72 hours post-inoculum respectively. LPS inducible NOS activity also decreased significantly with the time elapsed in WSSV infected shrimps. Results of WSSV detection with the Dig-DNA Probe dot blot hybridization test showed that WSSV of the two penaeid species couldn't be detected until iNOS started decreasing.

在此基础上,我们建立了对虾血细胞中诱导型一氧化氮合成酶的鉴定方法—硝基四氮唑蓝还原法和血细胞形态法以及酶活力的测定方法—L-瓜氨酸分析法和亚硝酸盐分析法并优化了鉴定和测量条件,结果显示:对虾血细胞在4℃下与L-精氨酸和LPS孵育8h以及当L-精氨酸浓度为2.5mmol l〓LPS浓度为100μg ml〓,Ca〓浓度为2.5mmol l〓时,iNOS活力的测定结果最佳。

Approximately 80% of the triacylglycerols in coconut oil are trisaturated, with lauric acid concentrated at the sn - 2 positions, octanoic acids at the sn - 3, and myristic and palmitic at the sn - 1 positions.

在椰子油中约80%三酰基甘油是三饱和的,月桂酸集中分布在sn-2位,辛酸位于sn-3位,肉豆蔻酸和棕榈酸位于sn-l位。

BHD. Production of fatty acids (such as stearic acid, lauric acid, myristic acid, palmitic acid, oleic acid, etc.), glycerin, soap, EBS, 6501 chemical products such as oils and fats.

生产的脂肪酸(如硬脂酸、月桂酸、肉豆蔻酸、棕榈酸、油酸等)、甘油、皂基、EBS、6501等油脂化工产品。

Myristic monoethanolamide ammonium sulfatewas synthesized from myristic acid and monoethanolamide with sulfamic acid as sulfating agent .

在芳烃类溶剂与羰基化合物催化剂存在下,以肉豆蔻酸和乙醇胺为原料,氨基磺酸作硫酸化剂,制备了肉豆蔻酸单乙醇酰胺硫酸酯铵盐。

Commodities subject to export quota license are: corn, rice, wheat, cotton, wood products, live ox, live pig, live chicken, natural silk and its products, coal, coke, crude oil, finished oil, rare-earth metal, antimony oxide ore, antimony and antimony products, antimony oxide, tungsten ore, Ammonium Paratungstate, Ammonium metatungstate, Tungsten Trioxide and Blue Tungsten Oxide, Tungstic acid and salt, tungsten powder and its products, Zinc ores, Tin ores, tin and tin-base alloy, and white silver.

实行出口配额许可证管理的货物是:玉米、大米、小麦、棉花、锯材、活牛、活猪、活鸡、蚕丝类、煤炭、焦炭、原油、成品油、稀土、锑砂、锑及锑制品、氧化锑、钨砂、仲钨酸铵及偏钨酸铵、三氧化钨及蓝色氧化钨、钨酸及其盐类、钨粉及其制品、锌矿砂、锡矿砂、锡及锡基合金、白银。

In order to check the corresponding compound at 31P NMR –45.4 ppm, stable pentacoordinate spirobicyclic 2-phenoxy-1,3-phenylene-dioxo-1,3,2-iminoacetoxyphosphoranes were synthesized through a new and efficient method whereby phosphorus pentachloride was displaced stepwise by catechol, N,O-bisamino acid and phenol, or catechol, phenol and N,O-bisamino acid, their 31P NMR chemical shifts are at about 31P NMR –45.0 ppm, the results showed that the compound 4 at 31P NMR –45.4 ppm was pentacoordinate phosphorane containing amino acid residue.

采用磷谱跟踪来研究上述成肽反应机理。例如在氮气保护下,0.1mmol O,O-亚苯基磷酰氯(1)和0.15mmol N,O-二苯丙氨酸(2)苯溶液加入0.6ml核磁管中,混合均匀,反应过程用磷谱检测。反应1分钟后,起始原料1(δp=19ppm)很快转变成N-磷酰苯丙氨酸的三甲基硅基酯(3)(δp=19.8ppm),在8分钟内,3完全转变成苯丙氨酸磷烷4(δp =-45.4ppm),同时出现环磷三酯(6)(δp=3.5ppm)。随着反应的进行,对应于化合物4的峰逐渐变小,而6逐渐变大。

The combination of chemicals includes a catalyst, such as, dibutyl tin dilaurate; carboxylic or sulfonic acid; and an extender compound, such as 2,4 pentanedione.

该化学试剂混合物包括催化剂,如二月桂酸二丁基锡;羧酸或磺酸;和增量化合物,如2,4-戊二酮。

Synthesis of PPA are intermediate ester methoxy-pyrimidine main raw material; for quinoline acid synthesis; are prepared quinolones (such as: Pipemidic, Ciprofloxacin quinolinic acid, such as containing the quinolone drugs) of raw materials; also are manufacturing and other chemical products dyes intermediates.

是合成PPA的中间体甲氧基嘧啶酯的主要原料;用于喹啉酮酸的合成;是制备喹诺酮类药物(如:吡哌酸、环丙氟哌酸等含喹啉酮酸的喹诺类药物)的原料;亦是制造染料及其他化工产品的中间体。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

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Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。