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Water,butylene glycol,cyclomethicone,VP/VA copolymer,glyceryl stearate,glycerin,ppg-15 stearyl ether,titanium dioxide,propylene glycol,cetyl alcohol,citrus aurantium dulcisfruit extract,saccharide isomerate,biosaccharide gum-1,ethoxydiglycol,peg-40 stearate,glycyrrhiza glabraroot extract,morus bombycis root extract,potassium cetyl phosphate,phenoxyethanol,c12-20 acid peg-8 ester,triethanolamine,prunus amygdalus dulcis oil,carbomer,caprylyl glycol,caffeine,disodium edta,methylparaben,chondrus crispus,butylparaben,iris germanica root extract,pentadecalactone,sodium polyacrylate,ethylparaben,sodium hyaluronate,peg-8,propylparaben,citric acid,chlorhexidine digluconate,tocopherol,ascorbyl palmitate,ascorbic acid

水,丁烯二醇,环甲硅脂,VP/VA共聚物,甘油基硬脂酸,甘油,ppg-15 stearyl ether,二氧化钛,丙二醇,十六烷基醇,橙子萃取物,天然异构寡糖, biosaccharde gum-1,乙基氧基乙二醇,聚乙二醇- 40硬脂酸,甘草根提取物,桑白皮根萃取,钾十六烷基磷酸盐,苯氧乙醇,c12-20 acid peg-8 ester,三乙醇胺,甜杏仁油,高分子胶,辛乙二醇,咖啡因,乙二胺四乙酸二钠,对羟基苯甲酸甲酯,卡拉胶,对羟基苯甲酸丁酯,鸢尾花根萃取, pentadecalactone ,聚丙烯酸钠,羟苯乙酯,透明质酸钠,聚乙二醇- 8,羟苯丙酯,柠檬酸,洗必泰葡萄糖酸盐,维生素E,维生素C棕榈酸酯,抗坏血酸

Purified water, octyl palmitate, castor oil phosphate, triethoxycaprylylsilane, glyceryl stearate, peg-100 stearate, isopropyl palmitate, cetearyl alcohol, vegetable glycerin, phenoxyethanol, benzyl alcohol, potassium sorbate, tocopherol, stearic acid, certified organic aloe barbadensis extract, certified organic lavandula angustifolia extract, avena sativa kernal flour, certified organic helianthus annuus seed oil, panthenol (vitamin B5), certified organic simmondsia chinensis seed oil, polysorbate 60, allantoin, certified organic chamomilla recutita flower extract, potassium cetyl phosphate, and xanthan gum.

纯水、辛基棕榈酸酯、蓖麻油磷酸盐、triethoxycaprylylsilane、硬脂酸锌,异丙酯、peg-100棕榈酸、cetearyl酒精、蔬菜甘油、萃取物、苯甲醇、山梨酸钾、生育酚、硬脂酸、有机认证索芦荟精华、有机认证此提取物、淡紫色沙枣阿韦纳处理(燕麦粉、有机认证的核心annuus的向日葵籽油、维他命原B5、泛醇经认证的有机simmondsia羊(霍霍巴籽油、polysorbate 60、尿囊素、有机认证chamomilla recutita洋甘菊三叶草萃取物、钾cetyl磷酸盐、黄原胶。

In this paper, the applications of the environmental friendly solid acid catalysts for esterification were studied and the activities of these catalysts were discussed, by which the solid acid ferric sulfate x-hydrate was used first as catalyst in the synthesis of dimethyl fumarate and ethyl chloroacetate and solid super acid SO42-/Fe2O3 was used first as catalyst in the synthesis of ethyl p-nitrobenzoate.

本文研究了对环境友好的固体酸催化剂在酯化反应中的应用,首次以固体酸Fe_2(SO_4)_3·xH_2O为催化剂合成了新型防霉剂富马酸二甲酯和化工原料氯乙酸乙酯,以固体超强酸5O_4~(2-)/Fe_2O_3为催化剂合成了医药中间体对硝基苯甲酸乙酯,并探讨了这些催化剂的催化活性。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2,6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐,然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基,而擅转乙酰,氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂,加氯。

Metabolites, including 1 phenolic diterpene, 2 phenolic acids (rosmarinic acid and caffeic acid), 2 flavonoids (6-methoxyluteolin-7-glucoside and homoplantaginin) and 1 coumaric acid ( cis-4-glucosyloxycinnamic acid), were successfully identified from two rosemary extracts with chloroform-methanol ( v / v , 3/1) and 50% aqueous methanol on the basis of HPLC, UV, NMR and MS data.

基于高效液相色谱、紫外吸收、核磁共振波谱及质谱数据,具有代表性的6个迷迭香代谢物的结构得到了确定,它们分别为1个酚类二萜、2个酚酸、2个黄酮(6-甲氧基木樨草素-7-葡萄糖苷和高车前甙)和1个香豆酸(顺-4-香豆酸葡萄糖苷)。

For systematically studying the quantitative structure-property relationships for electrolytes, the thesis chapter 6, 7 and 8 systematically studied molecular structure and quantitative structure-property relationships, including the relationship between molecular structure and conductivity, anions structure and electrochemistry stability, on anions of 1,2-Dihydroxycyclo-pentenetrione (croconic acid, H_2C_5O_5) and the whole series of dicyanomethylene derivatives, anions of 1,2-dihydroxycyclobuten- 3,4-dione (squaric acid, H_2C_4O_4) and the whole series of dicyanomethylene derivatives, and anions of 1,2-Dihydroxy-cyclobuten- 3,4-dione (squaric acid, H_2C_4O_4) and the whole series of dicyanomethylene derivatives.

为了系统地研究锂盐的分子结构与电解质的关系,论文第六、七、八三章系统地从理论上研究了方酸及其氰基亚氨基衍生物、方酸及其二氰亚甲基衍生物、克酮酸及其二氰亚甲基衍生物等各系列电解质分子结构、分子结构与电导率、阴离子结构与电化学稳定性的关系。

The protic- or Lewis acid catalyzed ring-closure of divinyl ketones (and their acid-labile precursors) pentadienylic cations is known as the via Nazarov cyclization.

质子酸或路易斯酸通过戊二烯基阳离子催化二乙烯酮的环闭合(以及它们的酸不稳定前体)这个反应被称为Nazarov环化。

Specifically, itcontains 8 chapters.In chapter 1, the formation, structures, properties and the futureprospect of liposome were thoroughly reviewed;In chapter 2, the stibility and permeability of phopholipid -eleostericacid liposome were studied together with the effect of polymerizationof eleostearic acid. This membrane system was very sensitive to 〓,the effect of 〓 was clarified to increase the aggregation/fusion ofliposomes and made the permeability of mixed liposomes much higher;In chapter 3, two polymerizable conjugated diyne bolaamphiphiles were synthesized. They could form very stable mixed liposome, andthe diyne could be polymerized by UV light in bilayer liposomes, as aresult, the stability of mixed liposome against solvent or surfactantafter polymerization were enhanced. In chapter 4, two kinds of amphiphilic amino acids were synthesized andstable liposomes were formed therefrom After the condensationpolymerization of amino acid in bilayer liposomes, stable polypeptide liposomes were obtained, which had lower phase transition temperatureand higher permeability.In chapter 5, four kinds of glycolipids were synthesized and theiraggregation behavior in water was comparied. When incorporated intophospholipid bilayer membranes, they could increase the phase transitiontemperatures and inhibit the aggregation and fusion of mixedliposomesat lower temperature.In chapter 6 and 7, three kinds of steroidal bolaamphiphiles withdifferent chain lengths were synthesized. Incorporation of steroidalmoiety to the center of lipid bilayer membrane obviously increased themobility of lipid membrane and shifted Tc to lower temperature side incomparasion with cholesterol. The bolaamphiphile which was shorter thanthe hosted lipid bilayer membrane thickness influenced the lipid packingmore obviously.

全文共分8章:第一章对脂质体的形成、结构、性质及展望进行了较为详细的文献综述;第二章研究了磷脂-桐酸脂质体的稳定性,通透能力及桐酸的聚合对这些性质的影响;磷脂-桐酸混合脂质体为一类对〓灵敏的脂质体,〓的作用首先是使脂质体集聚然后使脂质体融合,并加速内包荧光物的释放;第三章通过合成两种可聚合共轭双炔双极性双亲分子DDCA,DDOL,研究了共双炔分子在双分子层脂质体膜上的聚合及对脂质体性质的影响,聚合可以提高脂质体相对于溶剂及表面活性剂的稳定性;第四章合成了两类氨基酸为极性基团的双亲分子,它们均可以在超声下形成稳定的脂质体结构;氨基酸基团可以在脂质体上进行缩聚反应,若聚合后脂质体表面仍有足够的亲水能力,则可得到稳定的多肽型脂质体;聚合后脂质体的相变温度降低,通透能力增加;第五章合成了四种亲水基团为单糖基的双亲分子GL-l,GL-2,GL-3, GL-4,研究了它们在水中的分散情况、集合体形态与分子结构的关系;在DMPC双分子层膜中加入糖脂分子可以使脂质体的相变温度提高,阻止脂质体在低温放置时的集聚与融合;第六章-第七章合成了三种不同碳链长度的双极性含胆甾环双亲分子 CL-1,CL-2,CL-3;它们可以象胆固醇一样与磷脂混合形成稳定脂质体,胆甾环基团位于脂质体双分子层膜的中间;与胆固醇的作用相反,它们可以增加磷脂双分子层膜的流动性,降低混合脂质体的相变温度;三种分子的作用与其碳链长度和磷脂双分子层膜的厚度有关,比膜厚度短的分子影响最大。

ConclusionThe main components of essential oils are 2,4-bis(1,1-dimethylethyl) phenol (4.4%), tetradecanoic acid (6.96%), n-hexadecanoic acid (7.69%), 9,12-cctadecadienoic acid (6.37%), hexadecanoic acid-2-hydroxy-1- ethyl ester (4.79%) and octadecanoic acid-2-hydroxy-1- ethyl ester (4.77%), respectively.

结论阿给炭挥发油的主要成分为2,4-二树丁基苯酚(4.4%)、十四酸(6.96%)、n-十六酸(7.69%)、-9,12-十八碳二烯酸(6.37%)、软脂酸-2-羟基-1-羟甲基乙酯(4.79%)、硬脂酸-2-羟基-1-羟甲基乙酯(4.77%)。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

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此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

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