酸化的

Macroporous tributyl amine aminating strongly basic anion exchange resin-a phase transfer catalyst with high catalytic activity for nucleophilic substitution,which was screened out via combinatorial chemistry method –was used to catalyze the nucleophilic substitution reactions for synthesis of benzyl acetate,benzyl propionate,benzyl butyrate and benzyl valerate.

用组合化学方法筛选出的对无外加碱条件下的亲核取代催化活性最高的聚合物季铵盐–三丁胺胺化强碱性阴离子交换树脂为相转移催化剂，催化合成了乙酸苄酯、丙酸苄酯、丁酸苄酯、戊酸苄酯等羧酸苄酯。

Discussion Diphenylacetic acid can be prepared by the reduction of benzilic acid with hydriodic acid and red phosphorus,1 by carbonation of the reaction product of phenylsodium and diphenylmethane,2 and by hydrolysis of 1,1-dichloro-2,2-diphenylethylene.3

讨论 Diphenylacetic酸可编写的减少benzilic酸hydriodic酸和红磷， 1碳化反应产物phenylsodium和二苯基甲烷，第2和水解1，1 -二氯- 2 ，2 - diphenylethylene 0.3

Poly with sulfonic acid groups were readily synthesized with biphenol and 1,3-bis(4-fluorobenzoyl)benzene in the presence of excess potassium carbonate followed by sulfonation with chlorosulfonic acid.

以二氯二苯甲烷和2，6-二甲基苯酚为原料合成了含有阻碍基团的双酚单体，用此双酚单体和1，3-二(4-氟苯甲酰基苯)在无水碳酸钾存在的条件下反应制得聚芳醚酮，然后用氯磺酸磺化，控制反应条件，使磺酸基团恰好进入苯环对位，制得新型结构的磺化聚芳醚酮。

On the condition of using fatty acids of rapeseed oil as raw material,85% acetic acid as solvent, pelargonic acid as recrystalization solvent, this paper prepared azelaic acid and brassylic acid by ozonolysis ,oxidation decomposition ,recrystallization etc.

以蓖麻油酸为原料、85%醋酸水溶液为溶剂，经臭氧化、氧化分解、沸水萃取等过程制备壬二酸的最佳反应条件为：m：m(85%醋酸)=1：4，臭氧化温度20-25℃；氧化分解温度90-95℃，催化剂醋酸锰/醋酸铜用量为原料蓖麻油酸质量的0.09%，氧化分解4h，壬二酸的收率为62.5%。

The new surfactant was synthesized from the main starting materials such as lauric acid, p-cresol, chlorosulphonic acid and ethylene diamine, by 5 classic reactions which are acyl chlorination, esterification, Fries rearrangement, sulfonation and condensation, with total yield of 58%.

作者以十二酸、对甲酚、氯磺酸、乙二胺等为主要原料，共采取了酰氯化、酯化、Fries重排、磺化和缩合等5步经典的单元反应，合成了该表面活性剂，总收率为58％，并探讨了各步反应的条件对收率的影响。

Synthesis of dibutyrate nylon acids from nylon acids and butanol by the reaction of direct esterification and distillation under reduced pressure, using solid acid as catalyst.

尼龙酸在固体酸催化下，与丁醇直接酯化、减压蒸馏制得合格的尼龙酸二丁酯。

The volatile components were separated and identified using GC-MS technique. RESULTS Seven ingredients were. isolated: 2-ethyl-hexyl-adipate (66.5%), 1-methoxy-4-(1-propenyl)benzene (12.5%), isopropyl isothiocyanate (6%), isobutylisothiocyanate (6%), 6-methyl-5-heptene-2-one (3.5%), benzaldehyde (1.4%), phenylacetaldehyde (0.8%).

结果 分离出7个成分，采用峰面积归一化法确定了各成分的相对含量，分别为66.5%双－2-乙基己基－己二酸、12.5%1-甲氧基－4-（1-丙烯基）苯、6%异硫氰酸异丙酯6%、6%异硫氰酸异丁酯、3.5%6-甲基－5-庚烯－2-酮、1.4%苯甲醛、0.8%苯乙醛。

A traditional acidification method incorporated with an ether extraction technique was used to prepare silicotungstic acid and phosphotungstic acid with Keggin structure.

采用盐酸酸化-乙醚萃取法制备了Keggin型硅钨酸、磷钨酸，并分别以活性炭和硅胶为载体，采用不同的制备方法制备出一系列负载型杂多酸。

Four hemicyanine derivatives,-N-(4-sulfobutyl)-4-[2-(4-N,N-dimethylamino-phenyl) etheny1] pyridinium (P1),-N-(4-sulfobutyl)-4-[2-(4-N,N-dimethylaminophenyl)-1,3-buteny1] pyridinium (P2),-N-(4-sulfobutyl)-4-2-(4-N,N-dimethylaminophenyl) ethenyll quinolinium (Q1) and-N-(4-sulfobutyl)-4-

合成了具有不同共轭链长度的吡啶盐类及喹啉盐类半菁染料-N-（4-磺酸丁基）-4-[2-4-N，N-二甲基氨基苯基）乙烯基]吡啶鎓盐(P1、-N-（4-磺酸丁基）-4-[2-4-N，N-二甲基氨基苯基）丁二烯基]吡啶鎓盐(P2、-N-（4-磺酸丁基）-4-[2-(4-N，N-二甲基氨基苯基)乙烯基]哇琳鎓盐(Q1)以及-N-（4-磺酸丁基）-4-[2-4-N，N-二甲基氨基苯基丁二烯基]喹啉鎓盐(Q2)。研究了它们的光物理性质，并将它们用作TiO2纳米晶电极的光敏化剂引入光电化学电池。

The product structure, compositional information and spectral properties were carefully characterized by XRD, IR and DTA-TG, and the mineralization mechanism of mineralizer was studied during the process of calcium aluminates preparation.

借助于红外光谱、 X射线粉末衍射、差热-热重分析等手段对不同原料的铝酸钙粉的结构、组成及性能进行了表征和研究，并对矿化剂在合成铝酸钙中的矿化机理进行探讨。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。