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In the fifth chapter, a series of betulin derivatives including 28-acetoxybetulin, 28-tritylbetulin, 28-benzoylbetulin, 3-0-P-D-glucopyranoside of betulin and some betulinic acid conjugate containing amino acid were synthesized and confirmed by MS and NMR.

第五章分别合成得到了乙酰化白桦酯醇、28-苯甲酰化白桦酯醇、28-三苯甲基化白桦酯醇、3-O-β-D-glucopyranoside of betulin和一系列的白桦酯酸苷氨酸的衍生物,并分别对其进行了结构鉴定。

In the fifth chapter, a series of betulin derivatives including 28-acetoxybetulin, 28-tritylbetulin, 28-benzoylbetulin, 3-O-β-D-glucopyranoside of betulin and some betulinic acid conjugate containing amino acid were synthesized and confirmed by MS and NMR.

第五章分别合成得到了乙酰化白桦酯醇、28-苯甲酰化白桦酯醇、28-三苯甲基化白桦酯醇、3-O-β-D-glucopyranoside of betulin和一系列的白桦酯酸苷氨酸的衍生物,并分别对其进行了结构鉴定。

Since 2002, Institute of Coal Chemistry, Chinese Academy of Sciences has been developing a new technology to prepare high-purity glyoxylic acid by maleic anhydride ozonation, which has been completed, and now the research of the downstream products of glyoxylic acid including vanillin, heliotropin and the substituted mandelic acid is underway.

中科院山西煤化所从2002年开始进行研究,完成顺酐臭氧化法制备高纯乙醛酸新技术工艺的开发,现正进行乙醛酸下游产品香兰素、洋茉莉醛、取代扁桃酸的技术研究。

Factors were reviewed, and optimum conditions was obtained,these experiments provide effective data for industrial manufacture.On the condition of using fatty acids of cottonseed oil as raw material,85% acetic acid as solvent,this paper prepared azelaic acid and pelargonic acid by ozonolysis, oxidation decomposition , extracted by boiling water,active carbon absorpting etc.

以棉油酸为原料、85%醋酸水溶液为溶剂,经臭氧化、氧化分解、沸水萃取、活性炭吸附脱色等过程制备壬二酸的最佳反应条件为:m:m(85%醋酸)=1:4,臭氧化温度20-25℃;氧化分解温度90-95℃,催化剂醋酸锰/醋酸铜用量为原料棉油酸质量的0.15%,氧化分解4h,壬二酸收率为57.4%,壬酸收率为51.6%。

Results Fluoridated milk had significant effects of remineralization,anti-deminer alization and anti-caries.

结果 氟化牛奶有明显的再矿化、抗酸脱矿及抗龋作用,而氟水有一定的抗酸脱矿及抗龋作用,无再矿化作用。

Ornithine decarboxylase, a rate-determining enzyme of the polyamine biosynthetic pathway, is involved in the control of cell cycle, differentiation, cell growth and apoptosis. Previous studies described that protein kinase Cd regulates ODC activity. In this thesis, human leukemia cell line, HL60 cell, was used for the treatment with a specific PKCd inhibitor, rottlerin, to measure the effects on cell growth.

鸟胺酸去羧化(ornithine decarboxylase,ODC)为多胺酸起始与决定反应速率的酵素,对细胞周期、细胞生长、分化及细胞凋亡扮演一重要角色;在寻找肿瘤治疗及预防药物研究中,纯化植物天然物质是其中来源之一,研究者筛选药物时,测定对鸟胺酸去羧化活性是否具抑制效果是一个重要的试验。

At thenormal production condition sulphonate-barium content variety in the 13.69~19.45%,the shallow sulphonation refining oil of sulphonate-barium content was 15.47%among the normal data.

在正常工业生产中,磺酸钡含量在13.69~19.45%之间变化,浅度磺化试制的石油磺酸钡含量为15.74%,介于正常生产数据之间,这表明采用浅度磺化工艺完全可以生产出合格的石油磺酸钡添加剂。

Pit corrosion is a main kind of localized corrosion. The process of forming pit corrosion includes three stages-formation of pit source, development of pit cave and forming occluded corrosion cell. Molybdate series inhibitors can be inhibitive, for it can control three stages of pit development. First, there is apparent synergistic effect between molybdate and phosphate, which can suppress formation of pit source. Second, there is apparent passivation of molybdate inhibitor according to electrochemistry analysis, which let oxidation film in unoccluded cave repassivate.

首先,钼酸盐与磷酸盐或硅酸盐复配的缓蚀剂具有较理想的缓蚀性能,并且有明显的协同作用,从而能抑制部分点蚀核的产生;其次,钼酸盐复配缓蚀剂的使用,从电化学的角度分析,具有明显的钝化性能,且钝化区间较宽、维钝电流密度较小,从而能使未封闭的蚀孔或点蚀核附近的氧化膜再钝化,得到有效的修复;最后,对于还有部分蚀孔发展成为闭塞腐蚀电池的情况,钼酸盐、磷酸盐能进入蚀孔内部并且在酸性条件下生成铁钼磷酸盐,从而有效地减缓了点蚀的恶化,抑制了腐蚀的发展。

The mechanism of carbonization process of aluminate solution was analyzed thermodynamically. The results show that the internal reason of precipitation of Al3 in the process is its spontaneous nucleation caused by supersaturation of aluminate solution. The behaviors of SiO2 in the process are in accordance with that from published experiment, which implies that the content of product SiO2 from carbonization depends on its solubility but is not the result of absorption. The thermodynamic calculation for forming Na2O·Al2O3·2CO2· n H2O was achieved.

摘 要:为对高浓度铝酸钠溶液碳酸化分解过程中产品杂质含量的控制提供理论依据,分析了铝酸钠溶液碳酸化分解过程的热力学,认为该过程中Al3析出的真正机理是过饱和铝酸钠溶液的自发结晶;而基于分解过程中平衡浓度的热力学计算表明,在碳酸化分解过程中SiO2的变化规律与公认的三段变化规律一致,说明该过程产品中SiO2的含量取决于它在溶液中的平衡浓度,而非吸附所致;同时还分析了丝钠铝石的形成热力学。

Simultaneously, the activity and coding gene expression of ribulose 1, 5-bisphosphate carboxylase, phosphoenolpyruvate carboxylase, and glycollic oxidase all decrease in two rice accessions under low potassium supply while significant decrease in non-allelopathic rice "Lemont".

水稻光合作用相关酶的分析结果表明,低钾条件下核酮糖-1,5-二磷酸羧化酶、磷酸烯醇式丙酮酸羧化酶和乙醇酸氧化酶的活性及其基因表达强度均降低,但化感水稻&PI312777&的下降幅度显著小于非化感水稻&Lemont&。

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