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We have used GC to follow up the formation of epoxy acid and established the acidify condition; we have done series of parallel experiments to better the pivotal condensation reaction between acid and amine; In the cyclization step, we use cheap and available reagent-Lithium amide , rather than expensive LiHMDS, to proceed the reaction; and at last, we introduced green reagent-ozone to clear the phenyl group of nitrogen to avoid using heavy metal reagent-CAN. The total yield for this method is 29.8%.

通过GC监测,确定环氧酸的最佳酸化条件;对关键的酸和胺的缩合步骤,平行试验了多种条件;在环合一步,用价廉易得的氨基锂及催化量的HMDS代替昂贵的LiHMDS进行反应;氮上苯基的脱除采用臭氧,避免了重金属试剂-硝酸铈铵的使用,总收率为29.8%。

A continous flow equipment operation results show that on the hydrolysis acidulation,organic acid rates is 10%,organic compound removal rates is 25% or so,when the HRT of hydrolysic acidulation is about 6~10 hours, and penicillin wastewater dilute with the third water supply, the CODcr and Total Nitrogen removal rate would reach about 90% and 60%.

小试研究表明,青霉素废水在不同稀释倍数时,水解酸化反应水力停留时间为6~10h时,总有机酸酸化率达到10%左右,CODcr去除率20%左右;膜生物反应器的CODcr运行负荷达到8kg/m3·d,去除率90%左右;系统CODcr和总氮去除率可稳定在90%和60%以上。

aim to study the efficaciousness of wuling cap-sules for hepatic fibrosis in rats.methods rat models with hepatic fibrosis were induced by ccl4 compound factors and then treated with wuling capsules.pathology of liver sections,hyaluronic acid and procollagencontents in rat liver and serum were examined respectively.results pathological examinations showed that the liver cells of mod-el rats were injured seriously.collagen fibers proliferated and dissected hepatic lobules in model rats.wuling capsules could protect liver cells and reduce degrees of hepatic fibro-sis.the best effects were achieved at3.0g?

目的 研究五灵胶囊对大鼠肝纤维化的作用。方法采用以四氯化碳为主的复合因素致大鼠肝纤维化,观察五灵胶囊对肝组织病理学、肝组织和血清中羟脯氨酸、ⅰ,ⅲ型前胶原含量的影响。结果病理学检查显示,模型组大鼠肝细胞损伤严重,胶原纤维大量增生,形成假小叶。五灵胶囊组大鼠肝细胞结构破坏不明显,肝纤维化程度轻,在3.0g?kg-1 时治疗效果最好。

Effects of the different accelerants(La and Ce nitrate,Na nitrate and Na molybdate) on phosphatization were discussed.

提出在表面生成磷化膜以提高不锈钢的耐磨与耐蚀性能的工艺方法,讨论了各种促进剂(亚硝酸钠、钼酸钠、硝酸铈和硝酸镧)对磷化膜形成的影响,探讨了稀土对磷化的影响机理。

Study on Phosphatization and Passivation Two in One Treatment Process;2. Effects of the different accelerants(La and Ce nitrate,Na nitrate and Na molybdate) on phosphatization were discussed.

提出在表面生成磷化膜以提高不锈钢的耐磨与耐蚀性能的工艺方法,讨论了各种促进剂(亚硝酸钠、钼酸钠、硝酸铈和硝酸镧)对磷化膜形成的影响,探讨了稀土对磷化的影响机理。

A comparison has been made between the sensitometric results obtained from sulphur-sensitized cubic silver bromide emulsions which are latensified and hypersensitized with a gold thiocyanate solution, respectively, and those obtained from sulphur-plus-gold sensitized emulsions.

本文采用硫氰酸金溶液对硫敏化的立方体溴化银乳剂分别进行潜影加强和过敏化处理,并与硫加金敏化的乳剂进行感光性能的比较。

(1)PAL is better entrapped by PAG with a T∶C ratio of 8∶30.(2)PAL immobilized by glutaric dialdehyde on Bio-Gel P-300 is better than by CDC.(3)The best one is the dehydration and redehydration method.(4)Immobilized and permeated PAL active yeast cells are resistant to trypsin digestion and retain its PAL activity.

(1)固定化酶活性采用T∶C比为8∶30明显高于8∶19;(2)以戊二醛将PAL固定于Bio-GelP300优于用DCD固定化的酶;(3)质脂体包被中以脱水再加水法对酶活性影响较少,脂类组成以磷脂酰胆碱:胆固醇:磷脂酰丝氨酸比值7∶2∶1最好;(4)固定化PAL活性酵母细胞能较好地抵抗人工肠液中胰蛋白酶的水解作用,亦能明显降低苯丙氨酸的浓度。

However, phosphotyrosine protein and Stat3 are subsequently activa ted through phosphorylation. In scar tissues, although EGFR has an intrinsic ty rosine kinase activity when activated by EGFR correlated ligand, phosphorylation of Stat3 showed no significant changes.

早期不同的配体刺激造成EGFR表达差异,随后导致酪氨酸蛋白磷酸化的不同,在正常的皮肤中Stat3磷酸化继续引起下游信号的表达,而瘢痕组织中Stat3磷酸化与正常情况无显著差别,造成信号不匹配。

According to the content of sulfated bile acid s in urine the function of hepatobiliary can be judged whether normality.

肝胆系统有疾患,会导致尿中磺酸化胆汁酸浓度的增加。

The functions of acetic acid in the acid treatment of sand stones are systematically analyzed in several aspects such as retardation,stability of ferric ions,corrosion inhibition,acid sludge resistence and buffering property etc.

从缓速性、铁离子稳定性、缓蚀性、抗酸渣性及缓冲性几个方面系统分析了乙酸在砂岩酸化中的功能。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。