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The influence factors such as molar ratio of hexyl alcohol to propionic acid,amount of catalyst, and reaction time on the yield of hexyl propionate were discussed.

以钨硅酸为催化剂,通过丙酸和己醇反应合成了丙酸己酯,探讨了醇酸物质的量比、催化剂用量及反应时间对酯化率的影响。

The title complex has been synthesized by the reaction of silicotungstic acid , 1,10-phenanthroline monohydrate and cupric acetate.

以钨硅酸为催化剂,通过丁酸和异丁醇反应合成了丁酸异丁酯,探讨醇酸物质的量比、催化剂用量及反应时间对酯化率的影响。

In the past we tannery waste water treatment process on the basis of the road, an increase of acid hydrolysis and the flotation of the , use of acid hydrolysis pretreatment of law and the method of combining so that the system can be stable and reliable operation, to achieve the requirements of emission standards .

我们在以往的制革废水处理工艺路线的基础上,增加了水解酸化与气浮的功能,采用水解酸化预处理与生物法相结合的方法,使处理系统可以稳定可靠地运行,达到排放标准的要求。

Namely, the fluid of swift water and tiny whirlpool come from kinetics of the process which make the mass transfer better; 2 Increase alkalinity to improve the capability of abirritation of the system and an optimal pH condition which fit to acidic bacterium come into being.

即通过动力学措施造成反应器内流体介质的湍动及形成微涡旋,利用涡流扩散和对流扩散来加速传质;2提高所处理的碱度,增强系统的缓冲能力,控制酸化菌生存的最佳pH值范围,以实现系统在酸化段有机去除能力的高效性。

The inhibitor for DNA methyltransferase, 5-azacytidine (5-azaC), can demethylate the methylated DNA and restore transcription of genes. High dose homocystine can mediat DNA methylation and suppress gene expression.

应用甲基转移酶抑制剂5-氮杂胞苷(5-azacytidine, 5-azaC)可以使甲基化的启动子去甲基化,启动基因重新转录;高浓度同型半胱氨酸(homocystine, Hcy)可以介导基因甲基化而抑制其表达。

Using hydrochloric acid as a cheap catalyst,perfume methyl furoate was synthesized from methanol and furoic acid prepared from furfural,and was characterized by GC,IR and 1H-NMR.

从糠醛出发,由制备的糠酸和甲醇反应,在盐酸催化下,合成了香料糠酸甲酯,并用IR、1HNMR、GC等进行了表征;探讨了包括高纯度糠酸的制备在内的反应影响因素,在醇酸物质的量之比为 5∶1、催化剂体积占甲醇体积 13.0 %、反应时间 3h的最佳工艺条件下,酯化收率为81 0 %,收率比硫酸法、某些固体超强酸法

By means of molecular designing, a series of sodium branched-alkyl benzene sulfonates weresynthesized through seven process, involving Frieded-Crafts reaction, Grignard reaction, sulfonationand neutralization. Those isomers have similar structure, carbons of same quantity, but the position ofalkylaryl dissimilarity. Liner fat acid, metaxylene and halogenated hydrocarbon of different carbonnumber were used as the starting materials. Optimum processing condition was confirmed consideringinfluence of a series of reaction factors such as feed proportioning, quantity of catalysts, quantitysolvent, reaction time, temperature and pressure. Eight kinds of isomers of sodium hexadecylxylolsulfonates were finally synthesized, and characterized by FT-IR.

本文通过分子设计,以不同碳数直链脂肪酸、间二甲苯以及不同碳数的卤代烷为原料,经酰基化、格氏反应、加氢还原、磺化及中和等反应,合成了结构相似、烷烃链碳数一定、芳基在烷烃链不同位置的烷基芳基磺酸盐同分异构体;并考察了原料配比、催化剂用量、反应时间、反应温度、溶剂用量、反应压力等一系列因素对各反应的影响,进而确定最佳工艺条件,最终合成出十六烷基二甲苯磺酸钠的八种同分异构体,利用 FT-IR 对产物结构进行了分析。

Four phenylalanine derivatives were synthesized with this approach. The condition of the condensation reaction was optimized. The side reaction of the Curtius reaction was studied and a urine by-product was isolated and characterized.b. Through the detailed study of the behavior of various N-acetyl phenylalanine methyl esters under the condition of the Bischler-Napieralski reaction, it was found for the first time that the formation of benzyl oxazole derivatives was a competitive approach with the normal B-N reaction.

一、基于Bischler-Napieralski反应设计了以苯丙氨酸衍生物为原料的路线,在这条路线的研究中,主要取得了以下结果:、建立了一条以芳香醛和丙二酸单甲酯为原料,通过缩合、氢化、Curtius等反应制备苯丙氨酸甲酯的通用合成路线,对其中的缩合反应条件及Curtius反应中的副反应进行了深入的研究,利用这条路线合成了四个芳环取代的苯丙氨酸单甲酯衍生物。

The side reaction of the Curtius reaction was studied and a urine by-product was isolated and characterized.b. Through the detailed study of the behavior of various N-acetyl phenylalanine methyl esters under the condition of the Bischler-Napieralski reaction, it was found for the first time that the formation of benzyl oxazole derivatives was a competitive approach with the normal B-N reaction. A convincing mechanism was suggested and a rule governing the reaction was summarized.c.

一、基于Bischler-Napieralski反应设计了以苯丙氨酸衍生物为原料的路线,在这条路线的研究中,主要取得了以下结果:、建立了一条以芳香醛和丙二酸单甲酯为原料,通过缩合、氢化、Curtius等反应制备苯丙氨酸甲酯的通用合成路线,对其中的缩合反应条件及Curtius反应中的副反应进行了深入的研究,利用这条路线合成了四个芳环取代的苯丙氨酸单甲酯衍生物。

Kinetics characteristics of α- pinene isomerization catalyzed by activated carbon supported phosphotungstic acid was studied .

研究了活性炭固载磷钨酸催化α-蒎烯的异构化反应的动力学特征,研究表明,以环己烷作溶剂,α-蒎烯在活性炭固载磷钨酸上的异构化服从准一级动力学模型,其反应的表观活化能为100。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。