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Deacidification of rice bran oil was studied by using monoglyceride and glycerol blends as an esterification agent and ZnCl2 as a catalyst.

以单甘酯和甘油混合物作酯化剂,ZnCl2为催化剂对米糠油进行化学酯化脱酸研究。

Research and development for fhe production of pyrocatechol and hydroquinone by reaction of phenol with hydrogen peroxide and percarboxylic acid as hydroxylating reagent are introduced.

着重介绍用过氧化氢和过氧化羧酸作羟基化剂,使苯酚羟基化生成邻苯二酚和对苯二酚的研究开发进展。

Two estolide are that the ester melts an agent take amylum as raw material , with smooth butylene , the ester carrying out the solid room's spends reaction under the situation of there being no menstruum,ester composing smooth amylum butylene diacid Shan, and by having optimized reaction condition , having improved reaction efficiency.

以淀粉为原料,以顺丁烯二酸酐为酯化剂,在无溶剂的情况下,进行固体间的酯化反应,合成淀粉顺丁烯二酸单酯,并通过优化反应条件,提高了反应效率。

Factors influencing TiO_2-PILC photocatalystic properties were discussed, including the ratio of CH3COOH and Ti, the temperature and aging time of pillaring agents, pH value of reaction solution, the temperature of calcined, etc.

以钛酸四丁酯为前驱物,冰醋酸为鳌合剂,重点考察了[CH3COOH]/比、柱化剂制备温度和陈化时间、催化剂煅烧温度等对TiO_2柱撑蒙脱土结构的影响。

Based on the above experiments, the author studied the mixed metallic pillared and modified montmorillonites. The experimental result indicated that the microporous structure of Fe-Al-PLMs was affected by the changing of interlayer Fe-Al polymer with different Fe/Al ratio. But the presence of Al iron was helpful to incorporate Fe iron into interlayer of montmorillonites.. Introducing Zr helped Al-PLMs getting better larger spacing, thermal stability, surface area and pore volumes. Its successful to apply Zr-Al-PLMs to treat wastewater containing Cr iron. The experiment of modifying Al-PLMs by PVA showed that the order of adding starting materials (Al-pillaring solution, PVA, montmorillonite solution) was related to the property of Al-PLMs. The PVA as precursor was beneficial for Al to go into interlayer of the clay and to form larger basal spacing porous clay. The surface area and pore volumes of Al-PLMs increased mainly because of increasing the external surface area and mesoporous volumes after acid-activating. This conclusion confirmed that the microporous structure of pillaring clay depends upon the interlayer pillar.

实验结果表明:在Al-PLMs中引入Fe离子,不同Fe/Al比制得的Fe-Al-PLMs因层间的Fe-Al聚合离子结构不同而影响其微孔结构,但羟基Al离子的存在有利于Fe离子进入蒙脱石层间;在Al-PLMs中引入Zr离子,有助于其层间距、比表面积、孔体积增大,所得Zr-Al-PLMs应用于含Cr废水处理效果显著;PVA改性后的Al-PLMs其物化性质变化与铝柱化剂、PVA溶液、蒙脱石溶液三者不同添加顺序有关,说明PVA的前撑有利于Al进入蒙脱石层间得到较大层间距的Al-PLMs;经酸化处理得Al-acid-PLMs,其比表面积增大以外表面积为主,孔体积增大以中孔为主,这也证实了柱撑蒙脱石的微孔结构取决于其层间的柱化物。

On the basis of these principles and requirements,in this paper,a new modifier has been synthesized from pyromellitic dianhydride and thiosemicarbazide by the nucleophilic addition of anhydride,the cyclization of acyl thiosemicarbazide in alkaline solution,and the N-hydroxymethylation of the triazole-thione.

本文根据这一思路,以均苯四甲酸二酐和氨基硫脲为起始原料,通过酸酐的亲核加成反应、酰氨基硫脲的碱性环化反应、三唑硫酮环的N-羟甲基化反应合成出了一种新的N-羟甲基三唑硫酮酸改性剂。

A new process for the preparation of 5-bromo-vanillin with vanillic aldehyde as raw material,AlBr3 as activator,HBr and H2O2 as brominating agent and anhydrous alcohol as solvent was developed in this paper.

摘 要:以甲基香兰素为原料,氢溴酸与过氧化氢为溴化剂,溴化铝为催化剂,无水乙醇为溶剂制备5-溴香兰素。

Reasonable acid system is the key factor of eliminating the fracturing fluid damage to fracture surface and proppant, and also the key factor of making the hydraulic fracturing compounding acidifying technology successful.

酸液体系是否合理是能否消除压裂液对裂缝壁面及支撑剂层损害的关键因素,因此也是水力压裂复合酸化技术能否取得成功的关键。

The selected process consists of several steps as follows. Firstly, ammonifying the oily mixture of PXA pyrolysis by ammonia or aqueous ammonia, then adding the organic solvent to extra

实验结果表明,合适的分离提纯工艺为:先将裂解产物用氨水氨化、有机溶剂萃取,然后用硫酸酸化11-CUA铵盐水溶液、再将粗品11-CUA于合适介质中结晶,得到高纯度11-CUA晶体;优化工艺条件为:氨化pH值8.0~10.0、温度25-35℃,甲苯为萃取剂,酸化pH值1.5~2.0、温度55-60℃,环己烷为结晶介质,粗品11-CUA在环己烷中溶解温度50~55℃、与环己烷初始质量比4:100、结晶前沉降分层时间10min、结晶温度20℃。

In the reaction, industrial chlorinating agent and brominating agent with low cost and easy acquisition are used as oxidants to oxidize the ethyl lactate into the ethyl pyruvate.

反应中使用了廉价易得的工业用氯化剂、溴化剂作为氧化剂,将乳酸乙酯氧化为丙酮酸乙酯。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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