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酸化剂

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The synthetic method for nickel borate acylate, a kind of rubber-steel c ord adhesion promoter, through nickelous carbonate borate and mixed carboxylic a cids was studied, and many factors influencing the synthesis of NBA were investi gate d systematically.

研究了以碳酸镍、硼酸酯和混合羧酸合成新的金属橡胶粘合促进剂硼酰化镍的新方法。系统地考察了各种因素对合成硼酰化镍的影响。

Corrosion resistance and adhesive force to coating of works could increase strongly by seal treatment to bluing works in silane coupling agent.

用该封闭剂对发蓝工件进行封闭处理后,能明显提高工件的抗蚀性和对涂层的附着力,解决了因皂化和铬酸盐钝化而带来的涂层附着力较差和环境污染等问题。

Factors of esterfication of mixed dibasic acid were studied: alcohol acid mol ratios, the content of the catalysts, the reaction time and the content of water carrier.

实验考察了混合二元酸酯化的影响因素:醇酸摩尔比、催化剂用量、反应时间以及带水剂的种类和用量对酯化率的影响。

Hybrid mesoporous molecular sieve materials with hexagonal mesoporous structure and covalent bonded polyoxometalates were synthesized based on tetraethoxysilane anti lacunary polyoxometalate, SiW11, via sol-gel method in the presence of triblock copolymers P123 as the structure-directing agent. The influences of molar ratio of inorganic precursors and aging temperature on the structure and the loadings of SiW11 in the hybrid materials were investigated. Some reaction details in the synthesis were revealed.

用嵌段共聚物P123为模板剂,正硅酸乙酯和缺位结构的多金属氧酸盐SiW11为无机前驱体,由溶胶-凝胶法合成了具有六方结构和SiW11共价键联的介孔分子筛杂化材料SiW11/SBA-15,着重考察了无机前驱的配比和老化温度对杂化材料结构及SiW11负载量的影响。

METHODS: The spiral modiolar artery in guinea pig cochlea was exposed by microsurgery, then the fluorogold or horseradish peroxidase was given around the SMA for retrograde tracing.

在正常豚鼠单侧耳蜗螺旋蜗轴动脉局部滴加逆行追踪剂辣根过氧化物酶或荧光金,观察双侧交感颈上神经节、星状神经节内HRP或FG逆标神经元的分布;采用逆标与免疫组化相结合的双重标记方法观察追踪阳性神经元是否表达酪氨酸羟化酶、神经肽Y、钙基因相关肽或P物质。

Methods: the spiral modiolar artery in guinea pig cochlea was exposed by microsurgery, then the fluorogold or horseradish peroxidase was given around the sma for retrograde tracing. the bilateral superior cervical ganglia and stellate ganglia were observed to find retrogradely labeled neurons. the neurotransmitters of these sympathetic fibers around sma were ascertained by using retrograde tracing combined with immunohistochemical double labeled technique.

在正常豚鼠单侧耳蜗螺旋蜗轴动脉局部滴加逆行追踪剂辣根过氧化物酶或荧光金,观察双侧交感颈上神经节、星状神经节内hrp或fg逆标神经元的分布;采用逆标与免疫组化相结合的双重标记方法观察追踪阳性神经元是否表达酪氨酸羟化酶、神经肽y、钙基因相关肽或p物质。

The graft polymerization of acrylonitrile on Crosslinked polyvinyl alcohol microspheres CPVA microspheres was performed by using cerium ammonium sulfate as initiator, and grafted microspheres CPVA-g-PAN were prepared. Subsequently, the grafted PAN was converted into poly via amidoximation reaction with hydroxylamine hydrochloride as reagent, resulting in the functional microspheres CPVA-g-PAO. The chemical structure and physicochemistry characters were adequately characterized with infrared spectrum, scanning electron microscope and determining Zeta potential. The effects of main factors on the amidoximation transform reaction of the grafted PAN were researched with emphasis, and the adsorption property of the functional microspheres CPVA-g-PAO for some biomolecules was examined preliminarily with uric acid as a model biomolecule.

以硫酸铈铵为引发剂,实施了丙烯腈在交联聚乙烯醇微球表面的接枝聚合,制备了接枝微球CPVA-g-PAN,然后以盐酸羟胺为试剂,通过偕胺肟化转变,将接枝的PAN转变为聚偕胺肟,制得了接枝有聚偕胺肟的功能微球CPVA-g-PAO,采用红外光谱法、扫描电子显微镜及Zeta电位测定等法,对功能微球CPVA-g-PAO的化学结构及物理化学特性进行了表征,重点考察了各主要因素对接枝PAN的偕胺肟化转变反应的影响,也以脲酸为模型分子,初探了功能微球CPVA-g-PAO对生物分子的吸附性能。

To elucidate the possible mechanism of differentiation and /or apoptosis in NB4, K562 cells induced by tributyrin, a histone deacetylase inhibitor, the level of acetylated histone H3 was detected by Western blot, p21~ WAF1expression was detected by semi-quantitative RT-PCR.

为了探讨组蛋白去乙酰化酶抑制剂三丁酸甘油酯(tributyrin,TB)诱导NB4、K562白血病细胞分化和凋亡的作用机制,利用Westernblot方法及逆转录聚合酶链反应检测TB作用前后NB4、K562细胞组蛋白H3乙酰化水平以及p21WAF1表达量的改变。

To elucidate the possible mechanism of differentiation and/or apoptosis in NB4, K562 cells induced by tributyrin, a histone deacetylase inhibitor , the level of acetylated histone H3 was detected by Western blot, p21(superscript WAF1) expression was detected by semi-quantitative RT-PCR.

为了探讨组蛋白去乙酰化酶抑制剂三丁酸甘油酯(tributyrin, TB)诱导NB4、K562白血病细胞分化和凋亡的作用机制,利用Western blot方法及逆转录聚合酶链反应检测TB作用前后NB4、K562细胞组蛋白H3乙酰化水平以及p21(上标 WAF1)表达量的改变。

Thirdly, the mechanism of extractant and diluent loss in aqueous phase was studied in both saponified organophosphorus acids and naphthenic acid extraction systems.

本文通过研究皂化有机磷酸、环烷酸从有机相到水相的转移及水相中胶团或o/w型微乳状液的形成,证明了皂化酸性萃取剂和有机溶剂的水相流失与水相聚集体的形成有关。

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