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The change of remaining litter weight was the largest in the earlier 30 days during 60-day litter decomposition, and there was no significant difference in subsequent 30 days. The phenolic acid content of litter was significantly reduced with the decomposition time prolonging, and the releasing quantity of phenolic acid was the highest at the tenth day. The amounts of soil Aerobic azotobacter, Ammonifier and Aerobic cellulose-decomposer and the soil chemical properties such as pH, phenolic acid content, NH+4-N and available phosphorus were significantly affected by the litter aqueous extract of four decomposition stages.

凋落物分解的60d中,凋落物残留量在前30d内变化最大,30d后无显著变化;凋落物中酚酸含量随分解时间的延长,呈显著降低的趋势,且在分解10d时,酚酸释放量最大。4个分解动态的凋落物浸提液显著地改变了土壤好气性自生固氮菌、氨化细菌、好气性纤维素分解菌的数量和土壤pH值、酚酸含量、铵态氮、有效磷等化学性质。

The phenolic acid content of litter was significantly reduced with the decomposition time prolonging, and the releasing quantity of phenolic acid was the highest at the tenth day. The amounts of soil Aerobic azotobacter, Ammonifier and Aerobic cellulose-decomposer and the soil chemical properties such as pH, phenolic acid content, NH+4-N and available phosphorus were significantly affected by the litter aqueous extract of four decomposition stages.

凋落物分解的60 d中,凋落物残留量在前30 d内变化最大,30 d后无显著变化;凋落物中酚酸含量随分解时间的延长,呈显著降低的趋势,且在分解10 d时,酚酸释放量最大。4个分解动态的凋落物浸提液显著地改变了土壤好气性自生固氮菌、氨化细菌、好气性纤维素分解菌的数量和土壤pH值、酚酸含量、铵态氮、有效磷等化学性质。

There are other metal arsenates, such as those of Fe,Zn,Cu, and Pb, which are less soluble and more stable in the neutral pH region than calcium arsenates or ferric arsenate, but these have not been seriously considered as disposal forms.

还有其他金属砷酸盐,例如那些 Fe、 Zn、 Cu和 Pb,比起砷酸钙或者砷酸铁来,这些物质在中性的 pH 值范围内很少是可溶并且更稳定的,但是这些物质没被以处理的形式认真慎重地考虑过。

The influences of different surfactants (sodium dodecyl sulfate, sodium cholate and sodium deoxycholate), different electrolytes (sodium phosphate monobasic, sodium tetraborate and 3-cyclohexylamino-1-propane sulfonic acid), buffer pH and organic modifiers on the determination of sialic acid were studied.

其次建立了一种测定唾液酸的在线富集CZE法,该方法用40 mM磷酸二氢钠为缓冲溶液电解质,通过将样品溶解在乙腈:水=2:1的样品基体中,进样时间增加到100 s来达到样品富集的效果,并考察了样品基体中乙腈浓度和进样时间对富集效果的影响,研究了用硼砂或3-环己胺-1-丙烷磺酸作为电解质、缓冲溶液pH值和有机修饰剂的加入对唾液酸检测的影响。

Potassium ferricyanide and dithiothreitol were used to control redox potential from -100 mV to -450 mV in 3 L fermenter.

在3 L发酵罐上利用铁氰化钾和二硫苏糖醇调节发酵体系氧化还原电位值在-100~-450 mV,结果表明-350 mV为菌体生长和产丁二酸的最佳电位,丁二酸生产速率由0.75 g/提高到1.18 g/,产物丁二酸与副产物乙酸的质量浓度比由2.5提高到3.9。

With the extension of fertilization with organic , especially with the combination with organic and inorganic fertilizer,the soil readily oxidizable organic matter increased, while Kos decreased ; The soil active humus content, humus acid and E4/ E6 value were increased , while molecular weight and aromaticity of humus acid were decreased , thus progress to humus formation and quality of organic matter were enhanced.

随着有机肥特别是有机无机氮肥配施的年限延长,土壤易氧化有机质的含量逐渐增加, Kos 下降;提高了土壤松结态腐殖质含量,提高胡敏酸的比例;提高胡敏酸的E4/ E6值,降低土壤胡敏酸的分子量及芳构化程度;从而促进土壤腐殖化进程,改善有机质的品质。

The acidic composition can be prepared by mixing a monovalent or polyvalent cation and an organic acid in the presence of a strong oxyacid, wherein the resultant acidic composition is less corrosive to a ferrous metal than a solution of a mineral acid having the same acidic pH value as that of the acidic composition, and where in the acid composition is more biocidal than a mixture of the organic acid and a metal salt of the organic acid which mixture has the same acid normality value as that of the acidic composition.

所述酸性组合物可以在一种强羟基酸存在时,通过混合单价或多价阳离子和有机酸来制备,其中与具有相同的酸性pH值的无机酸溶液相比,所形成的酸性组合物对含铁金属的腐蚀性更小,并且与具有相同酸当量值的有机酸与有机酸金属盐的混合物相比,所述的酸组合物具有更强的杀生物作用。

As a result, both the detection limit of the sensor decreased by 2~3 magnitudes and the signal magnitude increased about ten times than that of fly labellar single hairs. The sensitivity to many stimulants from simple molecules such as NaCl, KCl, sucrose, glycine, proline, glutamic acid and aspatic acid to macromolecule such as bovine surem albumin was lower than 10〓mol L〓. For this reason, the maxillary palp of cockroach is reveled as an important candidate for construction of a new type of intact-receptor biosensors.

这种协同作用导致下颚须感觉区对有些刺激物如NaCl,KCl,蔗糖,甘氨酸,脯氨酸,谷氨酸,天冬氨酸,牛血清白蛋白的响应阈值比一般单根感觉毛至少低2-3个数量级,达10〓molL〓以下;信号幅度提高约十倍,是一种新型的适合用作传感器的敏感材料。

Results With different concentration of sodium arsenite 0.5 ~ 5.0 μmol/L, the skin fibroblasts were markedly stimulated, and a dose effect relationship was observed.

结果与对照组比较,皮肤成纤维细胞经不同剂量的亚砷酸钠诱导后,吸光度值均有改变,存在剂量效应关系(P〈0.01)。0.5~5.0μmol/L浓度的亚砷酸钠对皮肤成纤维细胞有明显的增殖作用,而10μmol/L浓度的亚砷酸钠产生明显的毒性作用。

The invention relates to a preparation process for synthesizing polyethylene terephthalate 1, 3- terephthalate catalyst, which comprises adding titanic acid ester, germanium compounds and cobalt compound into liquid dispersed phase of organic solution, wherein the total weight concentration is 4-10%, and preparing the catalyst through mechanical stirring or ultrasonic wave mixed ligand for 10-60 minutes in 0-120 DEG C, wherein the adding content of titanic acid ester, germanium compounds and cobalt compound are respectively 200-500ppm, 50-300ppm and 100-400ppm of reaction monomer mass of terephthalic acid or dimethyl terephthalate.

本发明涉及一种合成聚对苯二甲酸1,3-丙二醇酯催化剂的制备方法,将钛酸酯、锗化合物和钴化合物加入到有机溶剂的液体分散相中,总重量浓度为4~10%,在0-120℃通过机械搅拌或超声波混配10-60min制得;钛酸酯、锗化合物和钴化合物加入量分别是对苯二甲酸或对苯二甲酸二甲酯反应单体质量的200-500ppm、50-300ppm、100-400ppm;用此催化剂制备PTT产品,酯化和缩聚反应时间相对于单独使用钛酸四丁酯缩短了30-60min,产品特性粘数0.70-1.05dL/g,色相b值在2-6之间,切片可用于加工新型合成纤维及工程塑料产品。

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