酸值

Combining the performance evaluation (activity, selectivity and stability) and the characterization of the catalysts (XRD, TPD, FTIR and the pore structure measure), it can be concluded that :(1)The activity of modified β is higher than MCM-22, but the selectivity of ethylbenzene is lower about 3% than that of MCM-22;(2)The mounts of diethylbenzene and the other by-products are higher 1.7 times and 1.5 times than these of MCM-22 respectively;(3)The catalytic performance of zeolite mixture is nearly equal to modified β, but the selectivity of ethylbenzene is higher about 0.5% than that of modified β;(4)The catalytic activity of zeolite is mainly correlated with the number of acid sites, strength and distribution, and the distribution of products is determined by the binding energy of ethylbenzene and the pore structure, while the stability of catalyst is affected by the amount of poly-ring aromatic alkylate and the pore structure.

以性能评价和特性表征（XRD、TPD、FTIR和孔结构测定）相结合的方式，对上述三种催化剂性能比较的结果表明：（1）改性的活性明显高于MCM-22，但乙苯选择性却低于MCM-22绝对差约3%；（2）改性(上二乙苯和其他副产物的生成量分别约为MCM-22上对应值的1.7和1.5倍左右；（3）混合型催化剂的性能与改性相仿，但乙苯选择性提高0.5%左右；（4）对乙苯合成，沸石催化剂的活性主要取决于其B酸中心数、酸强度及酸分布，产物分布则取决于催化剂表面的乙苯脱附能垒值和孔道结构，而稠环芳烃的生成量和催化剂孔道结构是影响催化剂稳定性的主要因素。

Glycine receptor competitive antagonist partially reversed the effects of propofol. When slices were preincubated with GABA〓 receptor and glycine receptor competitive antagonists collaterally or preincubated with GABA〓 receptor incompetitive antagonist and glycine receptor competitive antagonist collaterally, 100μM propofol still decreased the amplitude of EPSCs.

2在膜钳制电压为-70mV条件下，100M丙泊酚明显降低合用GABA〓受体和甘氨酸受体竞争性拮抗剂预孵的大鼠海马脑片CA1区电刺激诱发的EPSC幅值，下降程度小于单纯甘氨酸受体竞争性拮抗剂预孵组，大于单纯GABA〓受体竞争性拮抗剂预孵组；而且，100M丙泊酚更是明显降低合用GABA〓受体非竞争性拮抗剂和甘氨酸受体竞争性拮抗剂预孵的大鼠海马脑片CA1区电刺激诱发的EPSC幅值，下降程度甚至大于单纯甘氨酸受体竞争性拮抗剂预孵组。

The effect of reaction time, leaching times and solvent PH, ratio of raw material and solvent, PH of phytin, settling time on phytin yield and quality, extracted from tikitiki , were studied.

对米糠中提取菲丁的工艺条件进行了优化，考察了酸浸时间、酸浸次数、酸浸pH值、液料比、中和pH值、静止时间等因素对产品的产量和质量的影响，得出了优化的工艺条件。

This article that focuses on the systematic and in-depth research in the current primal problem about abnormal burst pressure reservoir depress burst pressure has procured following main fruits:1 It forms the method which could obtain massive vertical static state mechanics parameters.2 In a foundation of acquisition of rock mechanics parameters,apply bent lamella that as mechanical model along with characteristic of actual geologic characteristics to analysis curvature for anticlinal strcture, get homologous tectonic stress value throug relation between the curvature and stress and different principal curvature in anticlinal structure,consequently set up laminational stress model for anticline reservoir. The block lamination for existed fracturing date has formed method of setting up mechanical model of lamination terrestrial stress by abtaining the block tectonic stress coefficients which are got by complex utilization test, laboratory test and fracturing date playback.3 Analysesing the main reason which lead to high burst pressure by considering the characteristic of reservoir geology,reservoir,and rock mechanics and reservoir damage,etc.Establishing burst pressure quantitative prediction model which provide gist for depressing construction risk and optimizing construction craft under the condition of open hole completion ,gun-perforated completion and damaged reservoir.4 Provding theoretical basis for interpreting acidification pretreatment which could depress busrt pressure by finding the relation between the influencing factors and rock machanics parameters and analysing the factors that have effect on rock mechanics parameters. Expounding the mechanism of reaction of mixed monomineral and acid from the angle of microcosmic element, evaluating quantitatively acid sensilility of different kinds of mineral effectively, and determing the first-order reaction dynamical equation of each mineral.5 Revealing rock mechanics property chage as a result of acid flooding in different condition by sandstone traumata experiment in different temperatures which combined with rock mechanics triaxial stress experiment.6 Associating damage mechanics with sandstone acidizing, established sandstone damage mechanics model in the foundation of the recognition on the rock mechanics parametric variation which is caused by acid-rock reaction in both macroscopic view and microscopic view ,also demonstrated those processes and quantitative estimated the acid busrt pressure to direct the site operation.

本文针对目前异常破裂压力储层降低破裂压力的主要问题展开较为系统和深入的研究，取得了以下主要成果：1形成了利用测井资料，结合室内岩芯测试结果，获取静动岩石力学参数的相关性特征，从而获得纵向上大量静态力学参数的方法。2在获取了岩石力学参数的此基础上，利用弯曲薄板作为力学模型，结合区块实际地质特征对背斜构造进行曲率分析，通过曲率与应力的关系，利用背斜构造不同部位的主曲率求得相应的构造应力值，从而建立起背斜储层的分层应力模型；对已有压裂资料的区块分层，形成了综合利用测试、室内实验、压裂资料反演获得该区块构造应力系数，建立起分层地应力的力学模型的方法。3综合考虑储层地质、油藏、岩石力学特性和储层伤害等因素，分析造成高破裂压力的主要原因，综合利用岩石力学、弹性力学等知识，建立了裸眼完井、射孔完井条件下以及储层受到伤害后的储层破裂压力定量预测模型，为降低施工风险和优化施工工艺提供了依据。4完成了物性、岩性影响岩石力学参数的因素分析，找出了各影响因素和岩石力学参数之间的关系，为从机理上解释酸化预处理降低破裂压力提供了理论基础；从微观元素的角度阐述了单矿物与酸反应的机理；并在此基础上，有效评价了各种矿物的酸敏感性，定量确定了岩石中各矿物的一级反应动力学方程。5完成了不同温度下的酸液类型、酸液浓度、注酸量等一系列砂岩损伤实验，结合岩石力学三轴应力实验，系统揭示了在不同条件下注酸而引起的岩石力学性质变化。6将损伤力学与砂岩酸化相结合，在宏观、微观两个方面认识酸岩反应引起岩石力学参数变化基础上，建立了砂岩损伤力学模型，并对其进行验证，在此基础上定量计算酸化后的破裂压力，有效指导现场施工

Fruit yields, weight of single fruit, per fruit pulp weight, fruit edible ratio, water content of sarcocarp were all increased with the increase of SWC and reached the maximum at SWC75. Soluble brix, soluble suger and titratable acid of fruit had notable or significantly notable negative-linear relations with SWC (R~2 = 0.880 7*; R~2 = 0.717 7* and R~2=0.965 1**) while pH of fruit was increased as SWC did. Brix-acid ratio of fruit was increased linearly with the increase of SWC (R~2=0.908 6*, n=50) and reached the maximum at SWC75. Suger-acid ratio also increased with SWC.

在SWC≤75%时，柑橘产量，单果重，单果果肉重、果实可食率、果肉含水量等随SWC增加而显著增加，在75%时各指标值最高；果实可溶性固形物、可溶性糖和可滴定酸含量分别与SWC呈显著或极显著线性负相关，相关系数分别为R~2=0.880 7~*(n：50)、R~2=0.717 7~*(n=50)和R~2=0.965 1~n=50果实pH值则呈相反趋势，柑橘果实固酸比和糖酸比随SWC的增加而显著增加，果实固酸比与SWC呈显著线性相关(R~2=0.908 6~*，n=50，糖酸比在SWC=75%时达到最大值。

There are some midst matters in wastewater, for removal of these matters the electrolyze time should exceed 30 min. The experimental results show that the bipolar packed bed cell has best treatment efficiency of phenol wastewater under condition that voltage is 10V, electrolyses time is 30 min, and velocity of flow is 1.03 cm/min.Basic on the study on treating of phenol wastewater, this paper carry on a research on treating of circuitry board film wastewater by bipolar packed bed cell.

本文在以上处理苯酚废水研究的基础上，论文研究了BPBC处理两种不同浓度得脱膜废水，试验结果表明，对于浓度较高的酸化气浮-光酚顿的出水，在外加氧化剂双氧水后，最佳处理工艺：槽电压8V，实际电解时间60min，双氧水的投加量为1倍理论药量，pH值为3，COD的去除率达到60%；在酸化气浮过程采用酸铜废液调节pH值将会降低COD的去除率。

The liquid absorption value and growth of the bacillus was measured after 24, 48 and 72 hour. It was showed that the most effective level of maltose in the medium is 5%. The media with pimelic acid was centrifugated 30min at 10000r/min, room temperature

本研究还将添加5%的麦芽糖的生物素培养基分组，分别加入0、0.2、0.4、0.6、0.8、1.0、1.2、1.4、1.6、1.8、2.0g/L的庚二酸，接种，在37℃，220r/min条件下进行振荡培养，然后测定24、48和72h时菌液的吸收值、pH值、生物素和庚二酸含量，确定庚二酸添加量为1.0g/L时，培养液中的生物素产量最大，庚二酸利用率最高。

A new method for the separation and purification of chiral mandelic acid by heated benzene extraction and refrigeration crystal was established. The ionization constant of mandelic acid was mensurated by pH potentiometer titration.

采用pH值电位滴定法测定了扁桃酸的离解常数，采用高效液相色谱法考察了扁桃酸在不同溶剂中的溶解度曲线和在苯-水体系中于不同pH值条件时的分配率，建立了热苯萃取和冷却结晶的扁桃酸纯化工艺。

The solubility curve of mandelic acid in different solvent and the distribute ratio of mandelic acid in benzene-water system in different pH condition were determine by HPLC. The results showed that the ionization constant pK_a of mandelic acid was 5.28, the solubility of mandeli...

研究结果显示，扁桃酸的离解常数pKa值为5.28；扁桃酸在水和苯中的溶解度曲线可分别表示为：S=38.756e0.0354t和S=0.2746e0.0649t；扁桃酸在水和苯中的溶解度差值曲线可分别表示为：ΔS/S1=0.1196t-2.712和ΔS/S1=0.3688e0.0723t；苯是最适合用于冷却结晶的溶剂；热苯萃取扁桃酸的苯水比例可选为1∶1；降低pH值有利于扁桃酸在苯中的分配。

Moreover, the physiochemical properties of CLA-SL were determined: color Y20R2.2, acid value 0.23mgKOH/g, peroxide value 3.15mmol/kg, iodine value 131gI/100g and saponification value 192mgKOH/g.

经过两级分子蒸馏后，重相酸价由98.5mgKOH/g降低至0.23mgKOH/g，CLA-SL产品的得率为43.5%，收率为91.0%。分子蒸馏CLA-SL产品的理化指标：色泽Y20R2.2，酸价0.23mgKOH/g，过氧化值3.15mmol/kg，碘值131gI/100g，皂化值192mgKOH/g。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。