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The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.

报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物,邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证

A method for separation and determination of amino acids using pre column derivatization with 6 aminoquinoline N hydroxysuccinimido carbamate AccQ.

对Waters公司采用 6 氨基喹啉 N 羟基琥珀酰亚胺基氨基甲酸酯柱前衍生化测定氨基酸的方法进行了改进。

Flash pyrolysis of carbohydrazide picric acid,semicarbazide picric acid and aminoguanidie picric acid is conducted by using T-jump/Fourier transform infrared spectroscopy.

利用温度跃升傅里叶变换红外原位分析技术(T-jump/FTIR)对苦味酸碳酰肼,苦味酸氨基脲和苦味酸氨基胍的快速热分解过程进行了研究,利用快速扫描傅里叶变换红外光谱在线检测气相产物的种类及浓度变化趋势。

The synthesis of the intermediate amidetriazinone was a crucial step in the synthesis of triazinone. Ethyl acetate was used as the initial material then was carried out for five steps hydrazine hydrate, triphosgene, chloroacetone, hydrazine hydrate respectively with the yield of 59.8%.

三嗪酮类化合物的合成关键是中间体氨基三嗪酮,本文以乙酸乙酯为起始原料,经过酯的肼解、成环反应、胺的烷基化、酮和肼的缩合、酰胺的水解五步反应合成中间体氨基三嗪酮,其收率达59.8%。

Now we don't know how aminoglycoside antibiotics damages hair cells, but there are some theories about it, such as:(1)AmAn affects the transformation among phosphoinositoln, inositol- 3-phophate and glycerine-2-acyl, also, it can cause the change of Ca2+ concentration in endocellular.

氨基糖甙类抗生素(aminoglycoside antibiotics, AmAn)损伤毛细胞的机制尚不清楚,但有以下几种学说:(1)影响了磷酸肌醇、三磷酸肌醇、二脂酰甘油间转化从而导致细胞内钙离子浓度的变化;(2)抑制G蛋白和鸟氨酸脱羧酶活性;(3)氨基糖甙类抗生素能引起内耳毛细胞的凋亡。

Methods: Serum alcohol and ALT、AST、GGT、ALP、CK、LDH、AMY、LIPA measured before and after beer consuming (4ml/kg) in 17volunteers. Meanwhile, the direct inhibitory effects of beer on the serum enzymes were studied by comparing the serum enzyme activities with or without beer.

利用17名健康志愿者,观察口服啤酒(4ml/kg)前后不同时间血液中酒精浓度及丙氨酸氨基转移酶、天冬氨酸氨基转移酶、γ-谷氨酰转肽酶、碱性磷酸酶、肌酸激酶、乳酸脱氢酶、淀粉酶、脂肪酶活性的变化,同时在体外加入血清中与体内浓度相近的啤酒,以观察啤酒对酶活性的直接影响。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下:一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸;蒸馏NMP;干燥增溶剂;二、在氮气气氛下,Py与NMP混匀后加入密封的反应器中,再加入增溶剂,然后加入5-氨基-2-苯并唑,搅拌;三、在氮气气氛下,将步骤二的混合液搅拌并升温至50℃~150℃后加入脂肪族二酸,再加入TPP后缩聚;四、再倾入甲醇析出沉淀,过滤,清洗沉淀,再干燥;即得到含唑环半芳香聚酰胺。

Another method for determining primary structure is to employ Edrnan's , which reacts quantitatively with the free amino group of a peptide to yield the corresponding pheny lthiocarbamoyl peptide, leaving the rest of the peptide chain intact.

另一种可以决定初级结构的方法是用埃德曼降解法,它们能与肽键上的游离氨基定量反应,产生相应的苯氨基硫代甲酰肽,而其余的肽链保持不变。

The shell polyose is glucosamine is composed by the majority of D- glucosamine and few N- the acetyl - D-, gets up the linear chain polysaccharide by β-(1,4) sugar glucoside keying, its structure is similar to the cellulose.

壳聚糖是由大部分D-氨基葡萄糖和少量的N-乙酰-D-氨基葡萄糖组成,以β-(1,4)糖苷键连接起来的直链多糖,其结构类似于纤维素。

The shell polyose is glucosamine is composed by the majority of D- glucosamine and few N- the acetyl - D-, gets up the linear chain polysaccharide by β-(1,4) sugar glucoside keying, its structure is similar to the cellulose.

壳聚糖是由大部分D-氨基葡萄糖和少量的N-乙酰-D-氨基葡萄糖组成,以β-(1,4)糖苷键毗连起来的直链多糖,其结构类似于纤维素。

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但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊!不用提了。提到肉,真是糟透了。

Tristan, I have nowhere to send this letter and no reason to believe you wish to receive it.

Tristan ,我不知道把这信寄到哪里,也不知道你是否想收到它。