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DL-Asparagine was produced by ammonolysis of maleic anhydride in the presence of N catalyst in a stainless steel autoclave.

在一内衬钛材的不锈钢高压釜中,采用自制的N催化剂,通过马来酸酐氨解反应合成了DL-天冬酰胺。

METHODS:This compound was synthesize by steps of ammonolysis,hydrogenize,diazotization and coupling from 4-nitrobenzoyl chloride.

以对-硝基苯甲酰氯为原料,经氨解、氢化、重氮化及偶合四步反应得到了巴柳氮。

This paper advances the preparation method of erucamide by direct ammonolysis .

本研究提出菜籽油直接氨解、溶剂脱脂、蒸馏预分离、溶剂结晶提纯制取芥酸酰胺的方法。

The results indicate that the optimized sulfonylation reaction time is 4 h, the materiel rate of chlorosulfonic acid and 2-chloroimidazo[1,2-α]pyridine is 1.2 : 1, with ethylamine the yield increasing from 15.4% to above 70%; the optimized ammonolysis reaction time is 3 h and the reaction temperature is 27℃, with the acetonitrile yield increasing from 60.1% to above 79.6%.

实验结果表明,磺酰化反应的最佳反应时间为4 h,氯磺酸与2-氯咪唑并[1,-α]吡啶的用量比为1.2:1,加入三乙胺可将收率由15.4%提高到70%以上;氨解反应的最佳反应时间为3 h,反应温度为27 ℃,加入乙腈可将收率由60.1%提高到79.6%;方案经改进后,总反应时间缩短3 h,收率提高了5.5%。

Waste minimization in ammonolysis process of O,O-dimethylphosphorochloridothioate;2. An Investigation on the Micelle-Catalytic Hydrolysis and Ammonolysis of Carboxylic Acid Esters;3. The final product is generated by ammonolysis of the compound under high pressure.

以4-溴-1,8-萘酐为原料,用2,4-二甲基苯胺在醋酸中与之反应得到N-2′,4′-二甲基苯基-4-溴-1,8-萘酰亚胺,然后将NDNA在高压下用氨水进行氨解得到最终产品。

In the first step of thedouble annulation route, 2-amino-3-carbamoyl-5,6-dihydro-4-pyridones 2 werecreated in high to excellent yields by a formal [5C + 1N] annulation reaction ofketene--acetals 1 with ammonia.

第一步,二硫缩烯酮1和氨源通过[5C + 1N]加成反应产率极高的得到了2-氨基-3-氨基甲酰基-5,6-二氢-4-吡啶酮2。

Objective To explore and discuss the effect and mechanism of N-acetylcysteine combined with ascorbic acid on severe acute pancreatitis.

目的 探讨N-乙酰半胱氨酸联合抗坏血酸对大鼠重症急性胰腺炎(severe acute pancreatitis,SAP)的作用及其机制。

Only the mutation from G to A at site 1135 changed glycin of the 355th amino acid to asparagine.

只有1135位的G变为A,使编码蛋白的第355个甘氨酸变成了天冬酰胺。

The aspartic acid of aspartame could be replaced by asparagine as reported in the literature.

文献已报道甜味肽的天冬氨酸可被天冬酰胺替换,仍保持甜味。

Studies with labelled aspartate demonstrate its ready conversion into asparagine.

用标记的天门冬氨酸研究证明,它迅速地转变为天门冬酰胺。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力