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In this paper six carbazole oxime ester derivatives were synthesized through Friedel-Crafts acylation, oximation and esterification from N-alkyl-carbazole.

以N-烃基咔唑为原料,经Friedel-Crafts 酰化、成肟和酯化反应,合成了6种咔唑肟酯衍生物。

College of Environment and Energy Engineering, Beijing Polytechnic University, Beijing 100022, China )Abstract The phosphoryl N → O migration reaction and ester exchange reaction on phosphorus of phosphoserine with methyl alcohol involving hexa-coordinate phosphorus intermediate 3 had been studied by MNDO method.

用MNDO方法对磷酰化丝氨酸仿生化反应机理中所形成的六配位磷中间体(3)可能的3个异构体的结构及其反应活性进行了研究。

The phosphoryl N→O migration reaction and ester exchange reaction on phosphorus of phosphoserine with methyl alcohol involving hexa-coordinate phosphorus intermediate 3 had been studied by MNDO method. The three isomers structures of 3 were discussed in detail based on the calculation results.

谭波用MNDO方法对磷酰化丝氨酸仿生化反应机理中所形成的六配位磷中间体(3)可能的3个异构体的结构及其反应活性进行了研究。

The reaction of condensation-cyclization of the two prepared compounds at 100 ℃ in the presence of anhydrous potassium carbonate gave 1,4,7,10-tetrakis(p-toluenesulfonyl)-1,4,7,10-tetraazacyclododecane,with a yield of 71%.

在无水碳酸钾存在下,100℃加热使所得两种磺酰化产物缩合环化得到1,4,7,10-四-1,4,7,10-四氮杂环十二烷,产率71.0%。

METHODS: Fresh bovine tendo calcaneus collagen was dispersed in 0.5 mol/L acetic acid, co-precipitated with chitosan and lyophilized. Dry membranes were cross-linked in 0.05% glutaraldehyde for 24 hours. In vitro its degrading rate was measured by use of collagenase degrading test. The chitosan-collagen membrane was implanted to subcutaneous dorsal sites of SD rats. After implantation, histocompatibility, vascularity and degradation were observed in vivo.

以酸溶法制备胶原溶液,添加一定比例的脱乙酰化几丁质,冻干成膜,0 。0 5 %戊二醛溶液浸泡交联,行体外酶降解实验,检测其耐受酶降解能力;将制备的几丁质-胶原蛋白膜包埋于 36只 SD大鼠皮下,术后 3、5天,1、2、3、4、6、8和 12周取材,检测其组织相容性、血管化能力及材料在体内降解情况。

The synthesis of nalbuphine hydrochloride from thebaine as starting material was through following processes:oxidation,high-pressure hydrogenation,acetylation,removing methyl of 3-methoxy,hydrolysis,condensation,reduction and finial salification.

以蒂巴因为起始原料,经氧化、高压氢化、乙酰化、氰化、脱3-位甲氧基的甲基、水解、缩合、还原、成盐,合成了盐酸纳布啡,总收率达18。

The preparation process includes condensation, acylation and aminization with high yield and low cost.

其合成工艺包括缩合、酰化、胺化,具有工艺路线简单、收率高、成本低的特点。

It is ofreactions of aromatic rings such as acylation, alkylation, etc..

具有芳香性,在环上能进行酰化反应,烷基化反应等芳香环所具有的反应特性。

Which is made up of long carbon chain by N-alkylation or acylation,The surface activity is greatly enhanced because of structure of borate surfactants and the basic property of long carbon chain.

它们将长碳链通过N烷基化和酰化联接在一起的一类含硼表面活性剂,由于是含四配位硼氧杂环结构的表面活性剂和结合长碳链的基本性质从而极大的提高了表面活性。

AVI may be protein matrix and it possesses neither a membrane boundary nor an internal structure,its formation is the result of the anthocyanins transported into the vacuole bind with a protein matrix. In vacuole, AVI is irregular and jelly-like in shape. In AVIs, the attachment of anthocyanins to the matrix protein is likely to be via H-bonds to a sterically restricted site. AVI is suggested to act as vacuolar anthocyanin "trap", preferentially for anthocyanidin 3, 5-diglycosides or acylted anthocyanins. The emergence of AVI can enhance color intensity and results in the "blueness" of color in the vacuole.

花色苷液泡包涵体可能具备蛋白质基质,既无膜包裹又无内部结构,其形成是转运进液泡的花色苷与蛋白质基质结合的结果;液泡里的花色苷液泡包涵体形状不规则,象果冻;在花色苷液泡包涵体中,花色苷可能通过氢键连接于蛋白质基质的一个有限空间位点;花色苷液泡包涵体被认为是液泡中花色苷的&陷阱&,优先摄取花色素3,5-二糖苷或酰化的花色苷;花色苷液泡包涵体的存在可增加液泡色彩的强度并导致&蓝化&。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意,我建议我们在价格上大家各让一半。

After an hour and no pup, look for continued contractions and arching of the back with no pup as a sign of trouble.

一个小时后,并没有任何的PUP ,寻找继续收缩和拱的背面没有任何的PUP作为一个注册的麻烦。