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酰亚胺

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The graft copolymer has an optimum effect of pour point depressing for the Daqing crude oil when it was synthesized under the conditions of that the mole ratio of EVA and octadecyl maleimide was 1:20, mass fraction peroxidation benzoin formyl was 2.5%, polymerization time was 6h, and the polymerization temperature was 90℃.

以目标物的降凝幅度为评价指标,优选出适合的合成条件为:EVA与十八烷基马来酰亚胺的摩尔比为1:20,引发剂过氧化二苯甲酰的量为2.5%,聚合时间6h,聚合温度为90℃。

All products are characterized with 1H-NMR. The products are used as PTC in the fluoridation of p-chloronitrobenzene, tetrachloroterephthaloyl chloride and N-benzyltetrachloridephthalimide to detect the performance of the different PTCs.

分别将上述化合物作为相转移催化剂应用于对硝基氯苯、四氯对苯二甲酰氯和N-苯基四氯邻苯二甲酰亚胺等化合物的氟化反应中,以检测各催化剂的催化性能。

Market sales of goods is actually soluble saccharin of the sodium o-benzoyl imide salt, Shaodai colorless crystal or white crystalline powder, odorless or slight odor, known saccharin sodium.

商品市场销售实际上是可溶性糖精的钠邻苯甲酰磺酰亚胺盐,Shaodai无色结晶或白色结晶性粉末,无臭或稍有气味,已知的糖精钠。

They are 4-(2- hydroxy-3-butynlenoxy) benzoic acid (1, WA), 5-chloro-7, 8-dihydroxy-7-methyl- 6-oxo-3- [ -3, 4-dihydroxy-3, 5-dimethyl-l-heptylene] -1H-8, 8a-dihydrobenzo [2, 3-c] pyran (2, WB),-2-(2-methyl-2-dibutene diamido)-2-butenoic acid (3, B5262), 3, 4-dihydro-9, 10-dihydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3- c] pyran-1-one (4, A73 semi-Vioxanthin), 8, 8'-bis (6, 9-dioxo-3,4-dihydro-10- hydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3-c] pyran-1-one)(5, A122 Xanthomegnin), 2, 5-dioxo-3a-hydroxymethyl-3, 3a, 6, 6a-tetrahydro-furo [2, 3-b] furan (6, 1003-2), 7-acety1-5-chloro-6, 8-dioxo-7-methyl-3- [ -3, 5-dimethyl-1, 3- diheptylene] -4aH-benzo [2, 3-c] pyran (7, M2-2 sclerotiorin), respectively.

它们分别被命名为4-(2-羟基-3-丁炔氧基)苯甲酸(1,WA)、5-氯-7,8-二羟基-7-甲基-6-氧代-3-[-3,4-二羟基-3,5-二甲基-1-庚烯基]-1H-8,8a-二氢苯并[2,3-c]吡喃(2,WB)、-2-(2-甲基-2-丁烯二酰亚胺基)-2-丁烯酸(3,B5262)、3,4-氢-9,10-二羟基-7-甲氧基-3-甲基-1H-萘并[2,3-c]吡喃-1-酮(semi-Vioxanthin,4,A73)、8,8'-双(6,9-二氧代-3,4-二氢-10-羟基-7-甲氧基-3-甲基-1H-萘并[2,3-c]吡喃-1-酮)(Xanthomegnin,5,A122)、2,5-二氧代-3a-羟甲基-3,3a,6,6a-四氢-呋喃并[2,3-b]呋喃(6,1003-2),7-乙酰基-5-氯-6,8-二氧代-7-甲基-3-[-3,5-二甲基-1,3-庚二烯基]-4aH-苯并2,3-c]吡喃(Sclerotiorin,7,M2-2)。

The effect of N-bromosuccinimide on the activity of Escherichia coli arginyltRNA synthetase was studied.

用N-溴代丁二酰亚胺对大肠杆菌精氨酰tRNA合成酶中的五个色氨酸残基进行化学修饰研究,发现酶分子所含的五个色氨酸残基中有一个可以被。。。

IR analysis indicated that both of the results were accorded with their standards IR spectrum and that the products of alkylation and animation were polyisobutylene succinic anhydride and ashless dispersant TEPA.

通过烃化产物和胺化产物的红外光谱分析,并分别与其标准谱图对照比较,看出产物红外谱图与标准谱图相符,可以确认烃化产物和胺化产物即为聚异丁烯丁二酸酐和聚异丁烯丁二酰亚胺无灰分散剂。

Afterwards, N-(6-chloro-3-pyridinemethyl) phthalimide is prepared by using potassium phthalimide, as nucleophilic reagent, condensation reacting with 2-chloro-5-methylpyridine at a temperature of 70℃.

然后在70℃条件下,以邻苯二甲酸亚胺钾作为亲核试剂,与2-氯-5-氯甲基吡啶发生缩合反应,制备了N-(6-氯-3-吡啶甲基)邻苯二甲酰亚胺

In the third chapter, the synthesis of5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde oxime(2) from5-[(1"S)-1",2"-diacetyl-oxyethyl]-1-phenylpyrazol-3-carboxaldehyde(1) and phenyl-hydrazine were introduced firstly. The synthesis of nine dioxapyrrolino[3,4-c]pyrazoles containing chiral pyrazolyl moiety(6a-i) from 2 with N-substituted-phenylmaleimide by nonmetal oxidant IBD-initiated intermolecular 1,3-dipolarcycloaddition was described in detail.

第三章首先以5-[(1′S)-1′,2′-二乙酰氧基乙基]-1-苯基吡唑-3-醛(1)和苯肼为原料,合成了化合物5-(1′S)-1′,2′-二乙酰氧基乙基1-1-苯基吡唑-3-醛-苯腙(2);再用化合物(2)与N-取代苯基马来酰亚胺反应,利用无金属氧化剂—IBD引发1,3-偶极反应,发生分子间的环加成,合成了9种新型手性吡唑连二氧代吡咯啉并

In order to improve the stability and mechanical properties in moist state,the gelatin nanofibrous membranes were chemically crosslinked by 1-ethyl-3-dimethyl-aminopropyl carbo-diimide hydrochloride and N-hydroxyl succinimide.

采用1-乙基-(3-二甲基氨基丙基)碳二亚胺和N-羟基琥珀酰亚胺对明胶纳米纤维膜材料进行化学交联处理,改善了材料的耐水性、热稳定性和力学抗拉性能。

The hydrophobic core serves as a reservoir for water-insoluble drugs.Hence,these nanoparticles can be used as carriers for hydrophobic drugs.For the synthesis of cholesterol-modified glycol chitosan conjugates,a carboxyl group was initially introduced to cholesterol molecule using succinic anhydride,and then covalently coupled with the primary amino group of glycol chitosan in the presence of 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide hydrochloride and N-hydroxyl succinimide.

本文采用二步反应将胆固醇接枝到乙二醇壳聚糖,首先将胆固醇进行羧基化,将胆固醇与琥珀酸酐反应生成胆固醇半琥珀酸酯,然后用1-乙基-3-(3-二甲基氨丙基)碳二亚胺盐酸盐与N-羟基琥珀酰亚胺作为偶联剂,将胆固醇半琥珀酸酯的羧基与乙二醇壳聚糖主链的氨基进行反应,得到胆固醇疏水改性乙二醇壳聚糖共聚物。

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