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酰亚胺

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A photoresist composition including a polymer is disclosed, wherein the polymer includes at least one monomer having the formula: wherein, R1 is selected from H, linear, branched or circular alkyl with 1-20 carton atoms, linear, branched or circular alkyl with 1-20 C atom, which is perfluorinated or semi-perfluorinated; and CN; R2 is alicyclic group with 5 or more carbon atoms; X is selected from methylene, aether, ester, amide and the connecting part of the carbonate; R3 is linear or branched alkylene with one or more carbon atoms or perfluorinated or semi-perfluorinated linear or branched alkylene; R4 is selected from H, CH3, CF3, CHF2, CH2F and perfluorinated or semi-perfluorinated aliphatic group; R5 is selected from the CF3, CHF2, CH2F and perfluorinated or semi-perfluorinated substituted and unsubstituted aliphatic group; n is 1 or higher integer; OR12 is OH or at least an acid unstable group selected from the tert-alkyl carbonate, tert-alkyl ester, tert-alkyl aether, acetal and ketal.

本发明公开了一种包含一种聚合物的光刻胶组合物,该聚合物包括至少一种具有下列结构的单体:其中,R 1 选自氢、具有1~20个碳原子的线形、支化或环状烷基、半氟化或全氟化的具有1~20个碳原子的线形、支化或环状烷基、以及CN;R 2 为具有5个或更多个碳原子的脂环基团;X为选自亚甲基、醚、酯、酰胺和碳酸酯的连接部分;R 3 为具有1个或多个碳原子的线形或支化亚烷基或者半氟化或全氟化的线形或支化亚烷基;R 4 选自氢、甲基(CH 3 )、三氟甲基(CF 3 )、二氟甲基(CHF 2 )、氟代甲基(CH 2 F)、以及半氟化或全氟化的脂族基团;R 5 选自三氟甲基(CF 3 )、二氟甲基(CHF 2 )、氟代甲基(CH 2 F)、以及半氟化或全氟化的取代或未取代的脂族基团;n为1或更大的整数;OR 12 为OH或者选自叔烷基碳酸酯、叔烷基酯、叔烷基醚、缩醛和缩酮的至少一种酸不稳定基团。

Target compounds have been synthesized by condensation of the aromatic nucleus and amino heterocylcle with acyl isocyanates or acylisothiocyanates in absolutely anhydrous and aprotic solvent.

为了寻找高活性的农药品种,利用生物等排原理和亚结构连接法,对脲类化合物的母体结构进行了修饰,将芳氧羧酸类及吡唑环引入酰基脲母体结构中,利用酰基异氰酸酯与杂芳环胺类化合物在无水非质子溶剂中发生亲核加成反应,合成了四个系列21种新的酰基脲类目标化合物。

Benzyloxy benzoyldimethylsulfoxide was prepared by the reaction of ethyl 4-benzyloxybenzoate and dimethyl sulfoxide in the presence of sodium hydride, followed by Pummerer reaction with concentrated hydrochloric acid to afford eo-hydroxy-co-thio-methyl-(4/-benzyloxy) acetophenone, which reacted with urea, thiosemicarbazide, semicarbazide hydrochloride and o-phenylenediamine to give imidazolidine-2,4-dione, l,2,4-triazine-3- one and quinoxaline derivatives, respectively.

本文用4-苄氧基苯甲酸乙酯和二甲亚砜为原料,在氢化钠存在下反应,合成了(4′-苄氧基)-苯甲酰基-二甲亚砜。研究了该亚砜在浓盐酸的存在下发生的Pummerer重排反应,用重排产物ω-羟基-ω-甲硫基-(4′-苄氧基)-苯乙酮分别与尿素、氨基脲、氨基硫脲和邻苯二胺反应合成了2,4-咪唑啉-二酮、1,2,4-三嗪-3-酮、喹喔啉等含氮杂环化合物。

The increase in the methylene resonance signal intensity which reflects the alterations in membrane lipids and accordingly in the biophysical and biochemical characteristics of cell membrane during apoptosis was found to be closely associated with nuclear changes as detected by DNA laddering assay and the TUNEL procedure.

在用烟酰胺处理的烟草细胞中,亚甲基信号强度的增加与DNA Ladder几乎同时出现,随诱导时间的延长,亚甲基信号强度也逐渐增大,在24 h亚甲基信号强度增加约2倍。

Originally limited to dialkylamino methylenation, the application of Mannich reaction has been expanded much further in recent years to a wide variety of monosubstituted amines, amine equivalents and amides. In addition, a variety of Aza-Mannich and Mannich-Michael methodologies have emerged.

最初该反应的应用范围仅局限于二烷基胺亚甲基化反应,近年来才得到了长足的发展,其研究范围扩展到单取代的胺、胺的类似物以及酰胺等化合物,并发展形成Aza-Mannich和Mannich-Michael等复合Mannich反应。

In the last part we first synthesized the propargylic amines though several methods and then developed a new methodology for the synthesis of -α-chloroalkylidene-β-lactams via the catalysis of PdCl〓 with CuCl〓 and BQ with moderate to good yields and good generality.

论文的第三部分工作是我们首先通过几种方法合成了炔丙基胺化合物,接着对PdCl〓催化的炔丙基胺的羰基插入环化反应进行了研究,以中等收率得到-α-氯代亚烷基-β-内酰胺化合物,反应的普适性良好。

They are insoluble in water, ethanol, methanol, acetone, chloroform and benzene, but soluble in DMA, DMF and DMSO.

它们溶于N,N-二甲基甲酰胺、N,N-二甲基乙酰胺和二甲基亚矾等溶剂,但不溶于水、乙醇、甲醇、丙酮、氯仿和苯。

The results suggested that the reaction temperature, the ratio of oil to water, the amount of ethyl cellulose as dispersant, initial monomers composition, the drop manner and the amount of initiator, the stirring speed, the pH of the buffer and the elution process have great influence on the morphology such as diameter of the hydrogel beads.

研究结果表明,采用反相悬浮聚合法,以丙烯酰胺和N-乙烯基吡咯烷酮为共聚单体,N,N'-亚甲基双丙烯酰胺为交联剂,牛血清白蛋白为模板,可以制备BSA印迹共聚物微球;反应温度、水油比、乙基纤维素分散剂用量、初始共聚单体配比、引发剂用量和加入方式、搅拌速度、水相pH值以及后续洗脱条件等均对粒径等微球结构和形态产生明显影响。

The application of perfluoroalkanesulfinyl chlorides and chiral perfluoroalkanesulfinamines in organic synthesis was studied in this dissertation.

中文摘要本论文对全氟烷基亚磺酰氯在含氟化合物合成中的应用进行了研究,并对它的衍生物手性全氟烷基亚磺酰胺的制备和应用进行了初步探索。

With the aid of 〓P NMR examination for the process and ESI-MS/MS analysis of the derivatized products from the reaction intermediate, it is found that the corresponding phosphoryl chloride is generated after mixing the hydrogen phosphonate derivative with chlorodiisopropylamine, and they react with amino acid, amino acid methyl ester, dipeptide methyl ester or N-methyl imidazole carboxyl alkyl diamine respectively to form the desired products.

利用〓P NMR对反应过程监测以及对反应中间体衍生化后产物的ESI-MS/MS检测分析发现,氢亚磷酸二酯与氯代二异丙胺反应首先生成了磷酰氯中间产物,它继续与氨基酸、氨基酸甲酯、二肽甲酯、1-甲基咪唑-2-酰基烷基二胺等反应生成了目标产物。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

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这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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