酯化了的

Dendritic p-t-butylcalix arene amide derivatives with terminal amino groups of the first and second generations were synthesized from the ammonolysis of ethyl calixylacetate with 1, 6-diaminohexane and Michael addition of methyl acrylate. Their structures were confirmed by IR, 1H NMR.

通过扩散法，采用氨基对丙烯酸甲酯的Michael加成反应和酯基的酰胺化反应交替进行，合成了4种树枝型对叔丁基杯芳烃酰胺衍生物(n=6，8)。

The Pt/FDU-14 catalysts can be effectively applied in the asymmetric hydrogenation of ethyl pyruvate after chirally modified with cinchonidine.

考察了经过手性分子辛可尼定修饰后的Pt/FDU-14催化剂在丙酮酸乙酯不对称氢化反应中的催化性能。

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

In addition, the new phosphine-catalyzed cyclization reactions of dimethylacetylenedicarboxylate and methyl propiolate with N-tosylimines are also described.

发展了膦催化下丁炔二酸二甲酯和丙炔酸甲酯与贫电子亚胺的环化反应，这对2-炔酸酯的反应又是一个补充，进一步丰富了膦催化下贫电子炔烃的反应化学。

The structure of the product was characterized by IR and 1H NMR.It indicated that the double bonds in ester were sulphonated and then converted into the corresponding saturated hydrocarbon ester sulphonate after hydrolysis.

对产物用红外光谱和核磁共振 1H谱进行的结构分析结果显示，油酯的不饱和双键发生了磺化反应，生成了饱和的羟基磺酸盐。

A series of UV curable waterborne hyperbranched polyester s with different acid/amine terminal rate,which contained -OH?-COOH and methacrylic chain end groups,and were partly neutralized with thertiary amine,were synthesized from trimellitic anhydride,epichlorohydrin,glycidyl methacrylate and triethylamine.

以偏苯三酸酐、环氧氯丙烷、甲基丙烯酸缩水甘油酯、三乙胺合成了末端羧基与氨基不同比例的一系列可UV固化的高支化聚酯，研究了末端官能团对合成产物水溶性、粘度以及凝胶转化率的影响。

All process factors that influence the composite thermochomic materials including the molar ratio of ester to water, pH value, reaction temperature, aging temperature, the dosage of thermochomic materials were carefully researched to have successfully acquired the optimal formulation.

重点研究了制备工艺各因素如酯水摩尔比、pH值、反应温度、陈化温度和变色材料用量等对热敏变色复合材料的影响，得出最佳工艺。

A variety of aldehydes were converted into acylals in good yields with anhydride in the presence of a catalytic amount of zinc bromide under solvent-free conditions.

以醛和酸酐为原料，溴化锌为催化剂，无溶剂条件下高产率地合成了偕二酸酯（其中醛与苯甲酸酐的反应是首次报道）。

The non-isothermal decomposition kinetics of nylon 1010 and nylon 1010/POSS composites in nitrogen were investigated. POSS significantly increased the activation energy but had little effect on the reaction order.(5) Exploring research was carried out on the reaction between EVM and nylon 1010. The reaction between EVM and TsOH during melt mixing was also invesigated, and related reaction mechanisms were studied in terms of NMR, TGA-FTIR and etc.

五初步研究了乙烯-醋酸乙烯酯橡胶和尼龙1010在高温下的反应性，报道了EVM和TsOH在高温条件下的反应性，通过核磁共振、热重-红外联用等分析表征方法探索了相关的反应机理，EVM和TsOH反应后，EVM的耐溶剂性、玻璃化转变温度和力学性能均有所提高，而体积电阻率则显著下降。

Then dendrimer-like polyamidoamine s based on the silica gel surface were prepared using Micheal addition of the amino and methyl acrylate,and ester-exchange of ethylene diamine and the ester group.

用硅烷偶联剂对硅胶表面进行氨基功能化，利用氨基与丙烯酸甲酯发生的Michael加成反应和乙二胺与酯进行的交换反应在硅胶表面合成了聚酰胺-胺树状大分子；利用红外光谱对PAMAM-SG的结构进行了表征，研究了溶液pH值、ρ(Ni2+)和温度对PAMAM-SG吸附Ni2+能力的影响。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。