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The thermal inactivation of penicillin amidase entrapped in AOT/isooctane reversed micelles was studied in detail.

研究了青霉素酰化酶在二-(2-乙基己基)琥珀酸双酯磺酸钠/异辛烷反胶团中的稳定特性。

In the precence of the base catalyst KF/Al2O3, the one - pot reaction of 2 -hydroxybenzaldehyde or 2 - hydroxynaphthaldehyde with ethyl α- bromoacetate,α-bromoacetophenone , 1,4 - dichloromethylbenzene , 4,4'- dichloromethylbiphenyl and 1,5 -dichloromethylnaphthalene gave the benzofuran compounds in 38-89% yield.

本文报道用 KF/Al_2O_3作为碱催化剂,由水杨醛或2-羟基-1-萘醛分别和α-溴代乙酸酯、α-溴代苯乙酮、苄基氯、4,4'-二氯甲基联苯和1,5-二氯甲基萘等进行一锅化缩合反应,以38~89%的产率合成了14种芳并呋喃化合物。

The electrochemical reduction and carboxylation of ethyl cinnamate have been carried out in an undivided cell equipped with a Mg sacrificial anode using MeCN as solvent.

在一室型电解池中,以MeCN为溶剂,Mg为牺牲阳极,成功地实现了肉桂酸乙酯的电化学还原和羧化。

Effects of 1 2-benzenedicarboxylic acid dibutyl phthalate and diphenylamine on mineral elements absorption of young tomato root system were studied in this paper.

以番茄为试材,研究了邻苯二甲酸、邻苯二甲酸二丁酯和二苯胺3种化感物质对番茄幼苗根系吸收矿质元素的影响。

The method to calculate the rate constant of the acetic ether saponification is in this way improved in this paper.

对乙酸乙酯皂化反应实验数据处理方法进行了改进,该方法无须测定初始电导,避免了初始电导的测定误差给计算结果带来的影响对两组实验数据进行了计算,结果表明,该方法简单、易操作,并有较高的精

The chemical constituents of extracts of Tamarindus indica L were determined by GC-MS. The relative contents of constitutes were determined by area normalizing method. 48 compounds were identified, amounting to total mass fraction 98.5%. The main compounds were 5-methyl-2(3H)-furanone, diethyl succinate, furfural, hexadecanoic acid, linolenic acid, 5-methylfurfural, oleic acid, linoleic acid, etc.

并利用气相色谱仪-质谱仪对罗望子萃取物的化学组成进行了分析鉴定,并用面积归一化法测定了各种成分的质量分数,共鉴定了48种成分,占总质量分数为98.35%,其中主要成分为:5-甲基-2(3H)-呋喃酮、丁二酸二乙酯、糠醛、十六酸、亚麻酸、5-甲基糠醛、油酸、亚油酸等。

The results showed polymeric diaryliodonium salts were effective aryl ion transfer reagents. Thirdly, a new type polymer supported hypervalent iodine reagents poly { [4-Hydroxy iodo] styrene} has been developed. It was an effective oxidative reagent, and could be applied to the one pot synthesis of 4-arylthiazoles.

然后,我们以聚苯乙烯羟基对甲苯磺酰氧基碘苯为原料,成功制备了一类新型聚合物高碘试剂—聚苯乙烯负载的炔基碘盐,并研究了其作为炔基转移试剂的有效性:(1)该试剂可对硫、氮、硒等负离子进行亲电炔基化反应,合成炔基亚砜、0,0-二烃基二硫代磷酸炔基酯、1-苯乙炔基苯并噻唑以及炔基硒醚。

At the same time,we have tried the precess for the preparation of 3-exomethylene cepham sulfoxide ester by the improved ring-expanding method over Kukolja, in which the different acid scavengers are employed in the presence of tolune, NCP and stannic chloride.

同时尝试了改进的Kukolja扩环法合成3—环外亚甲基头孢亚砜酯。以甲苯为溶剂,NCP为卤化试剂,无水SnCl_4为路易斯酸,通过选用了不同的酸清除剂,以制备闭环产物。

In chapter 3, 83 volatile chemical constituents have been identified from the petroleum ether extracted part of ethanol extract of Debregeasia longifolia Wedd., and the relative percentages of the compounds are determined by GC method. From the extract of trichloromethane and ethyl acetate, 8 compounds have been isolated.

第三章首次对长叶水麻乙醇提取物的石油醚萃取部分分离并鉴定出83种成分,并用毛细管气相色谱面积归一化法测定了各组分的相对百分含量;从氯仿和乙酸乙酯萃取部分分离得到了8种化合物,用波谱学方法鉴定了其中2种成分。

The experimental condition of acetylating method for determining priminary alcohol and secondary alcohol catalyzed by perchloric acid in the medium of analytically pure ethylacetate is proposed.

提出了以高氯酸为催化剂,分析纯乙酸乙酯为介质,乙酰化法测定伯、仲醇的实验条件,实现了对经典方法的改进,简化了操作程

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。