酯化了的

The route include three steps: etherification, ammoniation and then oxidation. Factors such as chloracetate, reaction temperature on process were studied. And discussed the ionic liquid was recovered.

讨论了不同的氯乙酸酯和反应温度对醚化反应收率的影响，讨论了不同的二苯甲硫乙酸酯对氨解反应收率的影响，及离子液体的回收使用。

The affections on the yield of DLLA caused by catalyst, temperature and time etc. were studied. By using ethylene glycol as diluent, the distillate temperature of DLLA was lowed and the carbonization phenomenon could be avoided, which caused the yield of DLLA increasing from 36.8% to 51.3%. The molecular weight of PDLLA prepared by this method could reach 184,000. DLLA and PDLLA was characterized and analyzed by DSC, XRD and IR.The key of direct method to synthesize PDLLA is the exclusion of H2O from reaction system.

丙交酯开环聚合制备PDLLA的关键在于中间体D，L-丙交酯的制备，研究了催化剂、反应温度、反应时间等因素对DLLA产率的影响，通过在反应体系中加入稀释剂乙二醇，DLLA的馏出温度明显降低，避免了DLLA在蒸馏过程中产生碳化现象，并使DLLA的平均产率由36.8％提高至51.3％，制备的PDLLA分子量最大值达18.4万。

From the reaction mechanism, which involved formation of benzodiazepinium ethoxycarbonylmethylate, the reaction mechanism, which involved formation of benzodiazepinium ethoxycarbonyl- methylate followed by cycloaddition reaction, was tentatively proposed.

通过研究反应过程中分离出的副产物反丁烯酸二乙酯III和4，5-二氢吡唑-3，4，5-三羧酸乙酯IV，初步提出了反应经过乙氧羰基甲基化苯并二氮杂卓翁中间体V再发生环加成反应的机制。

The catalysts such as tetraphenyl tin,aluminium isopropoxide and boron trifluoride etherate complex were used to catalyze the copolymerization.In addition,the copolyester can be given by copolycondensation after monomers were hydrolyzed by phosphoric acid.Boron trifluoride etherate complex was chosen as the catalyst because the catalytic activity was the best among the catalysts.

由于γ-戊内酯为五元环结构，难以进行开环聚合，因此分别考察了四苯基锡、异丙醇铝、三氟化硼乙醚络合物等催化剂，以及以磷酸为催化剂的水解缩聚反应，结果发现三氟化硼乙醚络合物的催化活性最高，因此选择三氟化硼乙醚为本体开环聚合的催化剂。

And thus, either one of the two geometrical isomers can be obtainedat will in high yield with high stercoselectivity,Two different stereoselectivities are displayed in thereactions of arsonium and telluronium benzylides with α,β-unsaturated esters and amides.

发现了苄基胂、碲叶立德在与α，β-不饱和酯、酰胺的环丙烷化反应中表现出不同的立体选择性，肉桂基胂、碲叶立德与α，β-不饱和酯反应时亦是如此。

The synthesis, characterization and polymerization of a new cyclic 6-(N-isopropyl acylamine ethylidene)-ε-caprolactone were reported.

研究了官能团化新型己内酯单体的合成及其与丙交酯无规共聚物的降解性能。

Factors influencing TiO_2-PILC photocatalystic properties were discussed, including the ratio of CH3COOH and Ti, the temperature and aging time of pillaring agents, pH value of reaction solution, the temperature of calcined, etc.

以钛酸四丁酯为前驱物，冰醋酸为鳌合剂，重点考察了[CH3COOH]/比、柱化剂制备温度和陈化时间、催化剂煅烧温度等对TiO_2柱撑蒙脱土结构的影响。

Polyimide/silica (PI/SiO2) nano-hybrid films of different solid content were prepared based on pyromellitic dianhydride and 4, 4'-oxydianiline using tetraethoxysilane as the inorganic precursors.

以均苯四甲酸二酐和4，4'-二氨基二苯醚为有机单体，正硅酸乙酯为无机前驱体，制备了SiO2含量一定，PAA杂化胶液固体含量不同的PI/SiO2纳米杂化薄膜。

A series of polyimide/SiO2-TiO2 hybrid films with different contents and weight ratio of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor by situ method .

以正硅酸乙酯和钛酸四丁酯为前驱体，采用两相原位同步法制备一系列不同含量及重量比的聚酰亚胺/SiO2-TiO2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性。

In the reaction, industrial chlorinating agent and brominating agent with low cost and easy acquisition are used as oxidants to oxidize the ethyl lactate into the ethyl pyruvate.

反应中使用了廉价易得的工业用氯化剂、溴化剂作为氧化剂，将乳酸乙酯氧化为丙酮酸乙酯。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。