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The catalytic effect of different modified molecular si eves were studied for synthesis amyl acetate, the results indicate that SO 2- 4 /FeZSM have go od catalysis activity to esterification .The effect of the ratio of reactants, the amoun t of the catalyst and the reaction time were also investigated.

考察不同改性分子筛催化合成乙酸戊酯的催化活性,结果表明:改性SO2 - 4/FeZSM对合成酯的催化作用较好,并讨论了以该催化剂催化酯化时原料配比、催化剂用量、反应时间等因素与酯化反应的关系。

Amyl cinnamate was synthesized from cinnamic acid and amyl alchol using tungstosilicic acid as catalyst.

以钨硅杂多酸为催化剂,通过桂皮酸和正戊醇酯化反应合成桂皮酸正戊酯,研究了各有关因素对桂皮酸酯化率的影响。

In this paper, the direct esterification of carboxylic acid and alcohol by using dealuminated USY as catalyst was studied.

研究脱铝USY 催化羧酸与醇的直接酯化反应,考察了催化剂硅铝比对酯化反应的影响及不同类型酸酶酯化的一般规律。

Using tapioca starch as raw material to prepare oxidized starch is better if we need the oxidized starch with low viscosity,can be used with high concentration starch slurry, and good transparency, good whiteness, low retrogradation and syneresis. Then, the research of using oxidization technology to improve the properties of tapioca crossed-linked and esterified starch was also researched: under the conditions of

然后,研究了应用氧化技术来改善木薯交联酯化淀粉的性能,在次氯酸钠用量为0.2%, pH8.5恒定反应,室温反应,反应过程不控温的反应条件下对木薯交联酯化淀粉进行氧化,可以在保持其交联酯化淀粉的应用性能不改变的前提下,大幅度提高产品的透明度,改善了产品应用性能。

As compared with traditional esterification, the cost of dehydrogenation was lower than that in process of esterification, and the actual yield reached 82% over 76.9% in esterification.

并将脱氢法与传统的酯化法进行了比较,脱氢法的成本要低于酯化法,且其实际收率达到了82%,超过酯化法的76.9%。

The n-butyl lactate was synthesied by the esterification of lactic acid and n-butyl alcohol in presence of ammonium ferric sulfate dodecahydrate NH4Fe(SO4)212H2O,and the factor influencing on the yield of reaction were discussed.

摘 要:在十二水合硫酸铁铵催化下,由乳酸和正丁醇发生酯化反应合成了乳酸正丁酯。实验考察了该催化剂催化酯化合成乳酸正丁酯的醇酸比、催化剂用量、反应时间、反应温度诸因素对酯化率的影响。

Isoamyl isovalerate was synthesized through esterification reaction by using isovaleric acid and isoamyl alcohol as raw materials and nano-H4SiW12O40/SiO2 as catalyst, the influencing factors in the reaction were studied, and the results showed that the esterification rate could reach 98.6 % under the conditions of the ratio of alcohol-acid 1.4∶1, the use level of catalyst 5 %, and the reaction time 1.5 h.

以纳米复合钨硅杂多酸为催化剂,异戊酸和异戊醇为原料,通过酯化反应合成苹果油,对酯化反应的影响因素进行了研究,结果表明,在醇酸物质的量比为1.4∶1,催化剂用量5%,反应时间1.5h的条件下,酯化率可达98.6%。

The results show that the optimal parameters of esterification are as follows: 4% of SO42-/ZrO2, molar ratio of methanol to litsea cubeba kernel oil 101, 68 ℃ of reaction temperature and 4 h of reaction time, the acid value decreases to 2.52 mg/g. Compared with the traditional acidic-catalyzed method, this method has the advantages of no acid proof equipment, easy to recycle catalyst and no acidic waste water emission. The optimal parameters of transesterification are as follows: 25 ℃ of reaction temperature, 0.5% of hexadecyl-trimethyl-ammonium bromide, 1% of NaOH, molar ratio of methanol to the oil 61 and 15 min of reaction time. The ester exchanging rate is 97.6%. This method adopts phase transfer catalyst and produces industry prospect, which has many advantages such as energy-saving and time-saving under room temperature.

研究结果表明,固体酸SO42-/ZrO2催化酯化反应的最佳条件为:油重4%的SO42-/ZrO2,醇油摩尔比为101,温度为68 ℃,反应时间为4 h,原油酸值降到2.52 mg/g;该法相对浓硫酸催化酯化法具有不需耐酸设备、催化剂易回收、无废水排放等优点;相转移催化酯交换反应的最佳条件为:温度为 25 ℃,0.5%的十六烷基三甲基溴化铵,油重1%的NaOH,醇油摩尔比为61,反应15 min,原油酯交换率达到97.6%;采用相转移催化技术,反应在常温下进行,大大减少了能耗,缩短了反应时间,具有的产业化前景。

The esterifying conditions of starch phosphate monoester of potato are investigated and analyzed in order to discuss the effects of esterification on granule diameter and gelatinization temperature of potato starch.

通过对磷酸单酯淀粉酯化条件的研究和分析,探讨了不同酯化条件对马铃薯淀粉磷酸单酯粒径和糊化温度的影响。

By esterification, saponification, doubledecomposition and formulation, liquid rare earth of monoisooctyl phthalate complex heat stabilizer was prepared with phthalic anhydride, isooctyl alcohol, sodium hydrate, rare earth chloride, mixed solvent and other reagents. The optimum conditions are: the temperature of esterfication is 130~140℃,and the reaction time is 1h. The temperature and time of saponification is 60℃ and 10min respectively. The temperature of double decomposition is 60~70℃,and the reaction ti...

摘 要:以邻苯二甲酸酐、异辛醇、氢氧化钠、氯化稀土、混合溶剂、助剂为原料,通过酯化反应、皂化反应、复分解反应以及复配制备了以邻苯二甲酸单异辛酯稀土为主要成分的液态稀土复合热稳定剂,其工艺条件为:酯化反应的温度控制在 130~ 14 0℃,反应时间为 1h ;皂化反应的温度为 6 0℃,反应时间为 5min ;复分解反应的温度在 6 0~ 70℃,反应时间为 1h ;水洗温度控制在 6 0~ 6 5℃;混合溶剂的用量为 5 0 %,稀土含量为 6 0 3%;在复配过程中,采用亚磷酸酯作为辅助热稳定剂,其用量为 5 %~ 7%,PVC中加入 2 %的这种稀土复合热稳定剂,在185℃下,其热稳定时间为 4 5min。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。