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Linear and star-shaped hydroxy-terminated polys were synthesized by reacting L-lactide with co-initiators such as poly,hydroxyethyl methycrylate,trimethylolpropane,mannitol and sorbierite in the presence of stannous octoate as catalyst.

以辛酸亚锡为催化剂,分别以聚乙二醇、甲基丙烯酸羟乙、三羟甲基丙烷、季戊四醇、甘露醇和山梨醇等和L-丙交反应,得到末端为羟基的线形和星形聚L-丙交

Ling Sheng, Guangzhou Chemical Trading Co., Ltd. is a franchise-n-butyl, octyl ester, diethylene glycol, butyl acetate, such as plasticizers, solvents products trading company.

广州市凌升化工贸易有限公司是一家以专营二丁、二辛、二甘醇、醋酸丁等增塑剂、溶剂产品的生产贸易公司。

Diethylene glycol dibenzoate octyl is the latest developed high-performance PVC plasticizers, can effectively substitute for DOP ester, dibutyl.

二甘醇二苯甲酸辛是最新研制出的PVC高效增塑剂,能够有效替代邻苯二甲酸二辛、二丁

Ethyl alcohol, 3-methyl-4-oxo- pentanoic acid, acetic acid butyl ester, 2-methyl-butanoic acid ethyl ester, diethyl phthalate,-2,4-Decadienal were the same volatiles d from the 10 cultivars.

其中共有组6种,为乙醇、3-甲基-4-羰基戊酸、乙酸丁、2-甲基丁酸乙、邻苯二甲酸二乙、-2,4-癸二烯醛。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法,以钛酸丁和乙酸锌为前驱物,冰乙酸为催化剂和胶溶剂,水为溶剂,无水乙醇为钛酸丁的溶剂,乙醇胺为沉淀剂并提供OH -,经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂,其组分和重量百分比含量如下:钛酸丁占1~15%;二水乙酸锌占1~12%;无水乙醇占1%~20%;冰乙酸占5%~15%;乙醇胺占0.1%~5%;水余量,具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点,可实现对对织物的抗紫外、抗菌、抗静电功能整理。

Synthesis of the phenylhydrazone, oxime and semicarbazonederivatives of calix[4]arenesThe reaction of p-formylcalix[4]arenes with phenyl hydrazine,hydroxylamine hydrochloride or semicarbazide hydrochloride afforded thephenylhydrazone, oxime or semicarbazone derivatives of calix[4]arenes,respectively.

型杯[4]冠醚的全醚化及性能研究利用氢化钠作为碱,对型杯[4]冠醚剩余酚羟基进行烷基化,合成中性杯芳烃型冠醚,初步研究了其对金属离子、有机阳离子和中性分子的识别情况,发现其对这些底物缺乏有效作用能力。

Poly/montmorillonite/2-Carboxyethyl phosphinic acid (PET/MMT/CEPP) nanocomposites were prepared through direct-esterification process by adding reactive flame retardant before esterification, and organic MMT was added before polycondensation.

采用直接化法,将共聚型阻燃剂羧乙基苯基次磷酸和对苯二甲酸以及乙二醇混合后化,在化产物中加入经过有机改性的蒙脱土,缩聚制备了阻燃聚/蒙脱土纳米复合材料(PET/MMT/CEPP)。

In this paper, the synthesies and applications of phophonate esters, specially the syntheses and applications of a-aminoalkyl phosphonate esters have been re-viewed.

有机膦酸由于结构与性质的特殊性及广阔的应用前景,正在成为化学研究的热点。本文对有机膦酸及其衍生物,特别是α-氨基烷基膦酸的合成方法与应用做了介绍

Monododecylphosphate was prepared by esterification of lauryl alcohol with phosphoric acid(mass fraction 85%) on cesium phosphotungstate catalyst.

以磷钨酸铯盐为催化剂,由月桂醇和85%的磷酸直接化合成单十二烷基磷酸,考察了带水剂种类、反应时间、磷钨酸铯盐催化剂中的铯取代数、催化剂用量和月桂醇与磷酸摩尔比等条件对磷酸转化率及单十二烷基磷酸选择性的影响。

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为:以青霉素G钾盐为原料,选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂,氧化得青霉素亚砜;采用对硝基溴苄为化试剂,制备青霉素亚砜;以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂,酞酰亚胺钾和4A型分子筛为酸清除剂,顺利开环;再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜,最终产率在60%以上。

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