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Methods Diethyl phthalate and diethyl succinate were used for raw material to synthesize the Rubidate.

方法以邻苯二甲酸二乙和丁二酸二乙为原料合成茜草双

The method comprises: utilizing arctiin as the precursor compound, and converting arctiin into 4, 4'-dihydroxy enterolactone by intestinal bacteria in an anaerobic condition. 4, 4'-dihydroxy enterolactone is lignin compound, and can be converted into phytoestrogen in human intestinal canals.

本发明是以牛蒡苷为先导化合物,在厌氧条件下,以肠道细菌将牛蒡苷转化为4,4′-二羟基肠内。4,4′-二羟基肠内为木脂素类化合物,在人的肠道中能被转化为植物雌激素―肠内而发挥药理作用。

The anion UV cured water soluble prepolymer was synthesized with toluene diisocyanate, dihydroxy compound, dihydroxyalkyl carboxylic acid, and polyurethane acrylate. The structure of the prepolymer was characterized by infrared spectroscopy.

采用甲苯二异氰酸、聚二元醇、二羟甲基丙酸和丙烯酸羟乙合成水性阴离子型聚氨丙烯酸,用傅立叶红外光谱证实了该聚合物的结构。

Spiral Spirobifluorene acetylated is oxidated by m-chloroperoxybenzoic acid and hydrolyzed by sodium hydroxide ,obtaining 2,2 '- dihydroxy -9,9'- spiral Spirobifluorene .Through nitrification,Reduced by hydrazine hydrate, we may get the 2,2 '- diamino -9,9'- spiral Spirobifluorene which are characterizated by IR, 1H-NMR !

L-酒石酸和乙醇化得到酒石酸二乙,将保护羧基保护起来,然后用碘甲烷在2,3-位上两个甲基,得到2,3-二甲氧基-酒石酸二乙,再用氢氧化钠将其水解,得到2,3-二甲氧基-酒石酸,用五氯化磷将羧基酰化,得到2,3-二甲氧基- 1,4-丁二酰氯,经过与二环己胺反应,得到拆分配体2,3-二甲氧基–N,N,N',N'-四环己丁二酰胺。

The paint includes liquid A, which consists of acrylic resin, mixed solvent of xylene, acetone and isophorone, organic silicone solution, superfine silica powder, titanium dioxide powder, methyl-(N-beta-amino ethyl gamma-amino propyl)-dimethoxy siloxane solution, gamma-methyl acrylyloxy propyl tromethoxy siloxane solution and fluorocarbon modified siloxane; and liquid B, which consists of hexamethylene diisocyanate, polydiisocyanate, xylene, and methoxy propyl acetate. When the paint is used, two components are mixed together.

由丙烯酸树脂、二甲苯和丙酮及异佛尔酮混合溶剂、有机硅酮溶液、超细二氧化硅粉、钛白粉、甲基(N-β-氨乙基γ-氨丙基)二甲氧基硅烷溶液、γ-甲基丙烯酰氧基丙基三甲氧基硅烷溶液、氟碳改性硅氧烷溶液组成A液,由六亚甲基二异氰酸聚异氰酸、二甲苯和甲氧基乙酸丙混合溶液组成B液,使用时将两组分混合。

A method for the preparation of microcellular elastomeric polyurethane foams from a reaction mixture comprising a polyisocyanate component containing at least 85% by weight of 4,4'-diphenylmethane diisocyanate or a variant thereof, a polyol composition comprising at least one polyoxyalkylene polyol having an average nominal hydroxyl functionality of from 2 to 6, an average hydroxyl equivalent weight of at least 1300 and an average oxyethylene content of between 50 and 85% by weight, water, a chain extender having an average hydroxyl equivalent weight of from 15 to 250 and optionally a crosslinking agent, the hardblock-content being more than 45% by weight.

本发明是有关一种制备微孔弹性聚氨基甲酸泡沫体的方法,其反应混合物包括:一种含至少85重量%的4,4′-二苯甲烷二异氰酸或其变体的聚异氰酸组分,一种多元醇组合物,其包含至少一种平均标称羟基官能度从2至6、平均羟基当量至少1300且平均氧乙烯含量介于50至85重量%之间的聚氧亚烷基多元醇,水,一种平均羟基当量为15至250之增链剂,以及视需要使用的交联剂,该硬性嵌段-含量(hardblock-content)大于45重量%。

The thermal decomposition yielded unsaturated compound and dithiobenzoic acid, leading to some loss of living character of the polymerization, such as retarded reaction rate and broadened molecular weight distribution.

我们根据合成双硫的经验和实验中的观察发现,双硫的热稳定性对RAFT聚合影响很大,在较高的温度下双硫会发生一定程度的热分解,生成的双硫酸会对聚合有一定的阻聚和延迟作用。

The title nano-sized polymeric microgels were synthesized by emulsion polymerization method,using divinyl benzene as crosslinking agent and methyl methacrylate,hydroxyl ethyl methacrylate,butyl acrylate as monomers.

通过乳液聚合的方法,以二乙烯基苯为交联剂,用甲基丙烯酸甲、甲基丙烯酸-β-羟乙、丙烯酸丁等丙烯酸类单体合成纳米尺寸的聚合物微凝胶粒子。

It showed that the ammonium ferric sulfate dodecahydrate was an excellent catalyst,the yield of the n-butyl lactate could reach over 95.0% under molar ratio of n-butyl alcohol and lactic acid 2.25∶1,the reaction temperature of 110~125℃,reaction time of 1.5 h and amount of the ammonium ferric sulfate dodecahydrate catalyst of 2.5%.

实验表明:NH4Fe(SO4)212H2O是合成乳酸正丁的良好催化剂。最佳反应条件为:醇酸物质的量比2.25∶1,催化剂的用量为反应物料总量的2.5%,化反应时间为1.5 h,反应温度110~125℃,化率可达95.0%。

Homology modeling of 3-D structure of two AChE from L.entomophila were constructed using H.sapiens(1p0i:A) native BuChE structure and Drosophila melanogaster(1d×4:A) native AChE structure as templates,respectively,by SWISS-MODEL.The catalytic triad were found and denoted in the 3-D structure of AChE from L. entomophila referring to T.californica.2.2 Gene cloning ofβ-actin and mRNA expression levels of two AChE genes from L. entomophilaBecause no reference gene has ever been used in Real Time PCR for L.entomophila in GeneBank,a fragment ofβ-actin gene was cloned from L.entomophila(GenBank Accession No.: FJ041117).It consists of 822 bp encoding a protein of 273 amino acids residues.

利用蛋白质结构同源建模工具,分别以人丁酰胆碱酶(1p0i:A)和果蝇乙酰胆碱酶(1d×4:A)的蛋白晶体结构为模板,对嗜虫书虱2个AChE的三维结构进行同源建模,并在三维结构中发现了AChE的酶解活性位点,证明嗜虫书虱体内也存在2个AChE基因。2.2嗜虫书虱β-actin基因克隆及乙酰胆碱酶基因mRNA表达水平研究目前关于嗜虫书虱的分子生物学研究较少,在GenBank中没有可用作内参基因的序列,因此本研究从嗜虫书虱体内克隆获得β—actin基因片段(GenBank登录号:FJ041117),该片段长度为822 bp,编码273个氨基酸残基,同源性比对分析表明该片段与其它昆虫的β—actin基因具有很高的同源性。

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