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TrithiocarbonatesS,S\'-bis (α,α′-dimethyl-α-acetic acid) trithiocarbonate (TTC1),3-(2-carboxyethylsulfanylthiocarbonylsulfanyl) propionic acid (TTC3),2-(2-carboxyethylsulfanylthiocarbonylsulfanyl) propionic acid (TTC4) and2-(2-carboxyethylsulfanylthiocarbonylsulfanyl)-2-methylpropionic acid (TTC5) weresynthesized by phase transfer method.

用相转移法合成了S,S′-二(α,α′-甲基-α&-乙酸)三硫代碳酸(TTC1)、S,S′-二丙酸三硫代碳酸(TTC3)、S-丙酸-S′-三硫代碳酸(TTC4)和S-丙酸-S′-(α,α′-甲基-α&-乙酸)三硫代碳酸(TTC5)。

In this article, three representative oil and fat resourse (edible raw oil, unedible linseed oil and waste oil and fat) were used to study the fatty acid methyl ester preparation technology, and the products from different technologies were compared and analysed. For plant oil, ester exchange process was performed immediately after simple decolorating and alkali refining pretreatment.

对于植物油脂,采用简单的脱色、碱炼预处理后,直接进行交换的工艺;对于废油脂,由于其成分变质较严重,预处理也显得相对复杂,采用了先预化再交换的工艺和先皂化酸化后再化的两种工艺。

The optimum reaction condition of NaClO oxidative pretreating and viny acetate acetylating technique has been determined according to sizing property, that further improves the function of acetylated starch size and expands its application in warp sizing .

对醋酸淀粉的变性工艺进行了系统的研究和探讨,以浆纱性能为依据,确定了次氯酸钠氧化预处理工艺和醋酸乙烯乙酰化工艺的最佳反应条件,进一步提高了醋酸淀粉浆料的性能,扩大了醋酸淀粉在纺织经纱上浆中的应用

The results of the effect on HSV-2 virulence experiment and the sample-canceling experiment showed that the four sulfated oligosaccharides had no virucidal activity to HSV-2 but inhibition activity.

初步探讨了低聚糖硫酸的抗病毒作用机制,由不同时间加药实验结果推测四种低聚糖硫酸具有类似的作用机制,可能作用于HSV-2与细胞的吸附阶段,不能抑制病毒在细胞内的复制过程;低聚糖硫酸的作用对象为病毒;对病毒毒力的影响实验和撤药实验说明四种低聚糖硫酸不能杀灭HSV-2,仅起抑制作用。

The esterifying conditions of starch phosphate monoester of potato are investigated and analyzed in order to discuss the effects of esterification on granule diameter and gelatinization temperature of potato starch.

通过对磷酸单淀粉化条件的研究和分析,探讨了不同化条件对马铃薯淀粉磷酸单粒径和糊化温度的影响。

In the step of esterification, dehydration of boric acid and then esterifying with phenol were carried out in order to increase conversion of esterification. Effect of reaction temperature, consumption of boric acid, kinds and consumption of dehydrolating agent on the yield of esterification was studied. The experimental results showed that high conversion of 98% of esterification was obtained.

本实验将化反应分解为脱水反应步骤和化反应步骤,以便提高化反应收率,同时,考察了反应温度、硼酸用量、带水剂种类及用量对化反应收率的影响,实验结果表明,该步反应条件简便易操作,反应转化率达98%。

By studying the influences that pH and SMTP act on the cross- linking reactions of potato starch and sweet potato starch, the cross-linking reaction mechanisms of PSPE and SPSPE were proposed and the chemical reactive velocity equations were determined. The relations between cross-linking reactions and temperatures were studied, meanwhile the activation energy of chemical reactions and apparent frequency efficient of cross-linking reactions were calculated. Technical conditions of preparing PEPS and SPEPS were determined.

3研究了pH值和三偏磷酸钠浓度对马铃薯淀粉和甘薯淀粉交联反应的影响,提出了低交联马铃薯淀粉磷酸和甘薯淀粉磷酸的交联反应机理,确定了化学反应的速率方程式,研究了温度对交联反应的影响,计算了马铃薯淀粉交联反应和甘薯淀粉交联反应的活化能和表观频率因子,确定了制备低交联马铃薯淀粉磷酸和甘薯淀粉磷酸的工艺条件。

A novel method combining a conventional free-radical solution polymerization with a chemical saponification was used to synthesize a, cu-dicarboxyl terminated oligo s with molecular weight below 1500. Here, cn-carboxyl terminated oligo s were firstly synthesized by the free-radical polymerization in THF, where 4,4'-azobis(4-cyanovaleric acid) was used as initiator, thioglycolic acid as chain transfer agent, then CTBMA were transformed into di-CTBMA via saponifying CTBMA in dioxane/H_2O/KOH solution.

利用传统自由基聚合法,在四氢呋喃溶液中自由基引发聚合甲基丙烯酸丁单体而得到w-羧基-甲基丙烯酸丁低聚物(分子量在1500左右);利用CTBMA 末端基的反应特性,在二氧六环/水/KOH混合溶液中皂化CTBMA,使之转化为a ,w-羧基甲基丙烯酸丁低聚物;研究了溶剂的类别、反应时间等反应条件对皂化产物结构的影响;利用MALDI-TOF-MS及LSIMS对皂化各阶段产物进行了分析监测。

The paper mainly refers to the thermal stabilities of three nitrates n-propyl nitrate (NPN, isopropyl nitrate and 2-ethylhexyl nitrate by using Infrared spectrum experiment, ARC and DSC.

本论文主要采用了红外光谱实验,加速度量热仪和差示扫描量热仪等手段研究三种硝酸(硝酸正丙NPN、硝酸异丙IPN、硝酸异辛EHN)的热安定性。

During esterification of benzyl chloride and sodium formate, benzyl formate is esterilysis which is a reversible reaction, and the mole ratio of benzyl formate to benzyl alcohol is 3:7 because of the chemical equilibrium.

在氯化苄与甲酸钠的化反应同时存在甲酸苄的水解反应,并且甲酸苄的水解反应是可逆反应,受化学平衡的限制,在实验条件下的甲酸苄与苯甲醇平衡的摩尔比大致为3:7。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。