酞酰亚胺

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为：以青霉素G钾盐为原料，选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂，氧化得青霉素亚砜；采用对硝基溴苄为酯化试剂，制备青霉素亚砜酯；以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂，酞酰亚胺钾和4A型分子筛为酸清除剂，顺利开环；再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯，最终产率在60%以上。

Surface photovoltaic behavior of titanoxophthalocyanine/N,N-bistolylperylene tetracarboxylic diimide composite films was investigated with surface photovoltaic spectroscopy and field induced surface photovoltaic spectroscopy.

用表面光电压谱和电场诱导表面光电压谱相结合的方法，研究了酞菁氧钛/N，N-二甲苯基苝酰亚胺复合薄膜的表面光伏行为，发现加入N，N-二甲苯基苝酰亚胺使复合薄膜在可见光区和近红外光区均产生负的光伏响应，可归结为光伏极性反转现象。

Photovoltaic Polarity Inversion in Thin Filma of Titanoxophthalocyanine/N,N-Bistolylperylene Tetracarboxylic Dimimide Composite Films

酞菁氧钛/N，N-二甲苯基苝酰亚胺复合薄膜的光伏极性反转

The purpose of this work is to develop new methods for syntheses of polyimides derived from chlorophthalic anhydrides.

本工作的目的是以氯代苯酐和二胺为原料，制备双氯代酞酰亚胺单体，然后进行聚酰亚胺合成方法的研究，以达到减少合成步骤，降低其生产成本的目的，主要内容如下： 1由双氯代酞酰亚胺与双酚A在不同体系中进行聚合反应，发现双酚是否完全成盐和聚合体系含水量是决定聚合物分子量的关键因素。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。