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Oral doses of 150-200 mg of plant indican were given to human subjects, including normal man and hepatitis patients, as well as dogs and rabbits.

此外在所有尿液中省检出不同的极性大的未知吲酚类化合物。在人尿中检出二个未知吲酚类化合物A和B。

The main results were as follows. The main nutrition bioactive components in Opuntia Milpa Alta were analyzed using chemical and instrumental analytical methods. The results showed that the content of crude protein and fat was 0.65%~0.68% and 0.30%~0.31% respectively. The total content of the amino acids was 6.81%~7.38%, and Glu was 1.08%~1.52%.The contents of pectin and cellulose was 1.47%~1.68%, 0.87%~1.22% respectively. They were oxalate free and rich in Ca 5.6%, Fe 8.06mg/100g, Zn 3.30mg/100g, VB6 5.62mg/100g, low in tannin 0.02%~0.04%.The bioactive matter content such as polysaccharide, polyphenol, and flavone were high, about 1.27%, 63.14mg/100g, 36.21mg/100g respectively.

主要研究内容如下:采用化学和仪器分析方法,对米邦塔仙人掌中的主要营养和生理活性成分进行分析,结果表明,粗蛋白含量为0.65%~0.68%,脂肪含量为0.30%~0.31%;氨基酸总量为6.81%~7.38%,其中谷氨酸含量达1.08%~1.52%;果胶、膳食纤维分别为1.47%~1.68%和0.87%~1.22%;干样钙含量5.6%,铁8.06mg/100g,锌3.30mg/100g;B族维生素丰富,其中干样VB6含量5.62mg/100g;单宁0.02%~0.04%;不含草酸;生理活性物质如粗多糖、多酚、黄酮类物质分别约为1.27%、63.14mg/100g、36.21mg/100g,半乳糖约占多糖中单糖总量的80%;HPLC检测出8种酚类物质,绿原酸含量最多达42.40μg/g,其次是芦丁和槲皮素,其含量分别为25.02μg/g和10.91μg/g。

Both of anti-oxidative activity and contents of polyphenol and pigment of Japanese red Perilla are higher than that of local Perilla.

酚类物质和色素物质的含量与紫苏抗氧化活性之间存在显著的相关关系,证明了多酚类物质在紫苏抗氧化活性中的作用。

Analytical results showed that the upper clear liquid of pyrolysis oils was mainly consisted of water-soluble substances,such as phenol,cresol,xylenol,sugars,hydantoins,morpholines,pyranones and pyridine derivatives compounds,etc.,while the lower sediment was mainly insoluble or hardly water-soluble substances,such as the big substituent phenolics(the number of substituent carbon atoms of which is greater than or equal to 2),aryl phosphate esters,fatty acid esters and nitrile compounds,and so on.

研究表明,热解油上层清液主要是一些较易溶于水的物质,如苯酚、甲酚、二甲酚、糖类、乙内酰脲类、吗啉类、吡喃酮类和吡啶类化合物等;而下层沉淀则主要为不溶或难溶于水的物质,如大取代基酚类(取代基碳原子数≥2)、磷酸三芳基酯类、脂肪酸酯类和腈类化合物等。

Some new results are obtained from the studies: 1 a novel thermokinetic research method, the characteristic reduced parameter method, has been proposed, and the kinetics of oxidation of benzoquinone by hydrogen peroxide has also been investigated with this method; 2 the kinetic mathematical models that the metallomicelles made from the mono-nuclear or dinuclear complexes and surfactants catalyze the phenolic derivant oxidation have been established respectively; 3 the feasibility and mechanism that the metallomicelle, a mimetic model of peroxidase, catalyzes the phenolic derivant oxidation has been discussed.

研究得到如下新的结果:(1)提出了一种新的热动力学研究法——特征对比参量法,用该法研究了过氧化氢氧化苯醌反应动力学;(2)分别建立了由单核和双核金属配合物与表面活性剂形成的金属胶束催化酚类氧化反应的动力学数学模型;(3)探讨了金属胶束模拟过氧化物酶催化酚类氧化反应的可行性及其机理。

Raeusch fruit. Total phenolic content and phenolic compositions of Canarium album Raeusch fruit from Fujian area were analyzed by Folin-Ciocalteu colorimetry, UV spectrum and HPLC method.

方法]采用Folin-Ciocalteu比色法、紫外吸收光谱法和HPLC色谱法分别对福建檀香橄榄果实中的酚类含量和酚类化合物组成进行了分析测定。

The Spectrophotometry method was used in experiment, the results is that the content of polyphenol is 14.8 mg/g in Jianshui's Elsholtzia bodineri Vaniot., which was higher than Shiping. The content of total flavones in the tea is 52.8 mg/g in Shiping, 43.9 mg/g in Jianshui.

通过分光光度法检测红河州两个县市野山茶茶水中的多酚类物质及总黄酮的含量,结果表明建水野山茶多酚类物质含量较高,为14.8 mg/g;石屏野山茶总黄酮较高,为52.8 mg/g。

After 3 months storage, our result showed that (1) color a value of rose liqueur with sucrose treatment had a slower decreased than with fructose treatment,(2) the sample added with caffeic acid or ferulic acid or tea polyphenol showed no significant difference in the color, anthocyanins content, and antioxidant capacity during storage as compared to control, and (3) the total amount of volatile compounds of rose liqueur decreased gradually, however there was one ester volatile formed, hexadecanoic ethyl ester, during storage.

贮藏三个月发现,(1)以果糖勾兑者在储藏试验中,其红色度下降速度较以蔗糖处理者快,建议仍以非还原糖进行勾兑对日后酒液保存较易,且酒液最好能予以避光包装,以避免颜色品质的下降;(2)添加不同之多酚类化合物时发现,添加caffeic acid、ferulic acid和茶多酚对酒液色泽、花青素含量、以及抗氧化能力之降低速度与控制组并无显著性的差异。(3)酒液储藏三个月后,其香气高级醇均有减少之趋势;但有hexadecanoic acid, ethyl ester酯类出现。

It was found that the more easily systhesized and stable N, N-acetal or N, Ohemiacetal can replace N-tosyl imino ester to react with phenols in the presence of TiCl〓, and α-arylglycine derivatives were also obtained in high yields and high regioselectivity.

进一步研究发现,更易合成的N,N-或N,O-缩醛可以作为亚胺酯的替代物和酚类化合物发生傅克反应。路易酸TiCl〓能有效地促进酚类化合物和亚胺酯的傅克反应较高产率、较高区域选择性的得到2-羟基α-芳香甘氨酸衍生物。

It is shown that the of the porous carbon towards (I_2) depends on the pore volume of the porous carbon; the adsorption of the porous carbon towards phenolic compounds depends on the density of carboxylic and lactonic groups on the surface of the porous carbon; the adsorption of the porous carbon towards Cr d...

发现多孔炭对酚类化合物及Cr的吸附以化学吸附为主,其中对酚类化合物的吸附由羧基与内酯基的表面密度合量决定,对Cr的吸附由表面官能团中羧基和内脂基含量的合量决定;多孔炭对I2的吸附以物理吸附为主,由孔容决定。

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