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Nitrate contents of main vegetables and fruits in Yaan city's markets were determined by disulfonic acid colorimetry method. Nitrate pollution levels were evaluated by evaluation criteria of nitrate content classification in China.

方法]采用酚二磺酸比色法对雅安市城区市售主要蔬菜和水果硝酸盐含量进行了测定,并参照我国硝酸盐含量分级评价标准对其硝酸盐污染状况进行了评价。

The comparison analysis of nitrate nitrogen determination is conducted with the same standard solution and natural water samples by two methods of spectrophotometric method with phenol disulfonic acid and ultraviolet spectrophotometer.

采用同一标准液和天然水样用酚二磺酸光度法和紫外分光光度法测定硝酸盐氮,进行比对分析,同时调查云南省内用此两种方法密码样考核的情况。

The comparison analysis of nitrate nitrogen determination is conducted with the same standard solution and natural water samples by two methods of spectrophotometric method with phenol disulfonic acid and ultraviolet spectrophotometer.

测定水中硝酸盐氮含量有多种方法,主要包括酚二磺酸光度法、锅柱还原法、戴氏合金还原法、离子色谱法、紫外分光光度法和电极法等。

The optimum reaction conditions were that the molar ratio of maleic anhydride and p-nitroaniline was 1.2:1, the volume ratio of toluene and DMF was 10:1, the amination temperature was 20~30℃ the cyclization temperature was 145~150℃ and the cyclization time was 6 h over; the amount of p-toluene sulfonic acid was 12% of total reactant mass, the amount of copper sulfate was 0.1~0.5% of total reactant mass, the amount of hydroquinol was 0.1% of total reactant mass.

得到的最佳工艺条件是:n:n为1.2:1,V:V为10:1;胺化反应温度为20~30℃,环化反应温度为140~150℃,环化反应时间为6h以上;对甲基苯磺酸用量为反应物总质量的1%~2%;硫酸铜用量为反应物总质量的0.1%~0.5%;对苯二酚用量为反应物总质量的0.1%。

Based on the laminar diffusion model, the micro-mixing in a rotating packed bed was discussed by taking the competitive and consecutive azobenzene reaction between 1-naphthol and diazotised sulphanilic acid as reaction system.

在层状扩散模型的基础上,以1萘酚与对氨基苯磺酸重氮盐在旋转填充床内发生的竞争串联偶氮化合反应为例,探讨了填充床内的微观混合情况。

A new mathematical model is built based on the laminar flow model and coalescence and redispersion model. Taking the competitive and consecutitive azobenzene reaction between 1-naphthol and diazotised sulphanilic acid as an example calculated segregation index.

在层状扩散模型和聚并分散模型的基础上,建立了一个新的数学模型,以1—萘酚与对氨基苯磺酸重氮盐这一竞争串联偶氮化合反应体系为例,计算了反映微观混合状态的离集指数。

The conversion of product reaches 98% under the optimal experiment condition: the molar rate of acrylic acid and tetradecyl alcohol is 1.1; the amount of p-methyl benzene sulfuric acid is 0.8%; the amount of p-benzened...

得出合成丙烯酸十四酯的最佳合成条件:丙烯酸与十四醇摩尔比为1 1,对甲苯磺酸用量为0 8%,对苯二酚用量为0 6%,反应温度为120℃,反应时间为4h。

The micelle shape transformation of tert-octylpheny phenol polyethylene glycol ether (TX-100), sodium dodecyl benzene sulfonate and tetradecyl trimethyl ammonium bromide in heavy water solutions was studied by 1H nuclear magnetic resonance spectroscopy, including an NMR self-diffusion experiment. These experiments showed that the surfactants formed several shapes of micelles (spherical, ellipsoidal, and rodlike) at the respective concentrations which were far above their critical micelle concentration.

运用核磁共振一维氢谱和自扩散实验方法研究了聚乙烯乙二醇异辛酚醚(TX-100)、十二烷基苯磺酸钠和十四烷基三甲基溴化铵三种不同类型的表面活性剂在重水溶液中的胶束形状转变,发现它们在临界胶束浓度以上的各自相应浓度都有胶束形状的变化(由球状转变为椭球状或棒状)。

The watermelon sample was extracted with ultrasound,protein was precipitated with potassium ferrocyanide and zinc acetate,and the pigment was decolored with activated carbon,nitrate would produce yellow compound with phenonldisulponic acid on condition of base.

在超声器中提取西瓜样品,用亚铁氢化钾和乙酸锌沉淀蛋白,活性碳脱色素,酚二磺酸碱性条件下和硝酸盐生成黄色化合物,样品的硝酸盐检测结果有较好的准确度和精密度,能满足样品分析需要。

7-Hydroxy-4-methylcoumarin was synthesized from ethyl acetoacetate and m-dihydroxybenzene by the Pechmann condensation using phenyl sulfonic acid as catalyst under solvent-free conditions.

摘 要:以苯磺酸作催化剂,乙酰乙酸乙酯和间苯二酚为原料,通过Pechmann缩合反应合成7-羟基-4-甲基香豆素。

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