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All the complex series based on 4',4''-dicarboxy-1,6-diphenoxyhex- ane (C6-2COOH) and 4',4''-dicarboxy-1,10-diphenoxydecane (C10-2COOH) possessed higher melting and clearing points, usually showed soft crystal or crystalline smectic phases and crystal polymorphs except C10-2COOH/ p -PhBPy complex displaying also an enantiotropic nematic phase, while the complexes based on 4,4'-dicarboxy-α,ω-diphenoxy tetraethyleneglycol ether (C8O4-2COOH) with a longer flexible spacer exhibited monotropic fluidic smectic SmA and/or nematic phases.

研究表明,分别具有较短的6或10个亚甲基的烷烃间隔基的双苯甲酸衍生物4',4''-二羧酸-1,6-二酚氧基己烷(C6-2COOH)和4',4''-二羧酸-1,10-二酚氧基癸烷(C10-2COOH)的系列复合物具有较高的熔点和清亮点,一般都只出现结晶近晶相和多晶型转变现象。

Condition optimization for its efficient fermentation was also carried out. The reaction and separation system with the addition of resin HD-8 and the isoeugenol/aquoeus biphasic system of the biotransformation of isoeugenol to vanillin by Bacillus fusiformis CGMCC1347 were set up. The isolation and purification of isoeugenol and vanillin in both systems were studied. The reuse of the immobilized cells in biphasic system was successfully applied.

SW-B9的基础上,对该菌株进行了生理生化特性鉴定以及16S rDNA序列分析,命名为纺锤芽孢杆菌CGMCC1347;继而对该菌株的发酵条件进行了研究,首次建立了纺锤芽孢杆菌CGMCC1347转化异丁香酚生成香草醛的树脂分离耦合体系和异丁香酚—水两相体系,同时对此二体系的底物和产物的分离提取进行了研究,成功实现了两相体系中固定化细胞的反复利用。

The comparison studies on gossypol of different genetic types of pigment gland in the seeds of cotton newly bred, including the special and common glandless and glanded ones, was conducted through highperformance liquid chromatography on a C18 Column with methanol 0.5% acetic acid aqueous solution, 90∶10 as mobile phase at a flow rate of 0.8mL·min-1 and UV detection at 254 nm.

运用高效液相方法对新近育成的特殊和普通的无腺体陆地棉及特殊和普通的有腺体陆地棉及海岛棉等多种遗传类型品种材料的棉酚含量进行了比较研究。实验以一反向C18色谱柱为固定相,甲醇 0.5%的醋酸90∶10为流动相,流速为0.8mL·min-1,建立了分离度好、准确而快速的棉酚HPLC测定方法:其最低检测限量3×10-6g/mL-1,精密度和准确度均小于10%,回收率为100.4%~103.2%。

The enzyme amplified lanthanide luminescent spectrometry of horseradish peroxidase was developed and applied to the analyse of HRP and tuberculosis. The deconvolution curve method was used for synchronous fluorimetric determination of two component systems of highly overlapped spectra, such as phenol and p-dihydroxybenzene, phenol and o-dihydroxybenzene, and tyrosine and tryptophan. A novel mathematical method, combining Gorry's deconvolution method, was presented to remedy data loosing of SavitzkyGolay's deconvolution method and applied to dealing with fluorescent signal.

建立了辣根过氧化物酶的酶联放大镧系发光法,并应用于结核抗体的测定;成功地应用褶合曲线分析法并进行了改进,结合同步荧光光谱法用于苯酚/对苯二酚、苯酚/邻苯二酚和酪氨酸/色氨酸等光谱重叠较严重的双组份体系的同时测定;结合Gorry提出的卷积法,提出一种解决Savitzky-Golay卷积法中两端信息丢失问题的快捷方法。

It is shown that the of the porous carbon towards (I_2) depends on the pore volume of the porous carbon; the adsorption of the porous carbon towards phenolic compounds depends on the density of carboxylic and lactonic groups on the surface of the porous carbon; the adsorption of the porous carbon towards Cr d...

发现多孔炭对酚类化合物及Cr的吸附以化学吸附为主,其中对酚类化合物的吸附由羧基与内酯基的表面密度合量决定,对Cr的吸附由表面官能团中羧基和内脂基含量的合量决定;多孔炭对I2的吸附以物理吸附为主,由孔容决定。

Image recording medium comprising a substrateand an imaging layer containing binder, developer, dye, stabilizer against oil exposure (e.g. Calcium salt of organic acid); method for preparing a recording medium comprising binder, radiation absorber, phenolic compound, calcium salt of organic acid, and leuco dye, said radiation absorber initiating reaction between phenolic compound, calcium salt of organic acid and leuco dye.

图像记录介质,其包含衬底和成像层,所述成像层包含粘合剂、显色剂、染料、抵抗油暴露的稳定剂;制备包含粘合剂、辐射吸收剂、酚类化合物、有机酸的钙盐和无色染料的记录介质的方法,所述辐射吸收剂引发酚类化合物、有机酸的钙盐和无色染料之间的反应。

Compared with pearled grain, whole grain has higher concentration of oil and tocol, showing that seed coat may be one of the major tissue accumulating oil and tocol.

试验表明,大麦油及其母育酚含量既受基因型的控制,又受生长环境条件的影响;大麦种皮部分可能是大麦油的主要储存组织之一,制啤后的大麦原料有可能作为母育酚提取的资源加以利用,从而提高大麦的附加值。

In order to investigate the relationship between the open-chain ligands and metal ions, and the possibility of the metal complexes used as electroluminescent materials, a new naphthol schiff base ligand which is a open-chain crown and its four transition metal complexes, a new amide type tripodal ligand containing heterocyclic ring, two tripodal ligands (H〓L〓 and H〓L〓) containing phenol schiff bases and their rare earth complexes were synthesized and characterized.

为了进一步研究和探讨开链配体与金属离子的配位作用,以及金属配合物作为电致发光材料的可能性,我们设计合成了含萘酚环的Schiff碱开链冠醚H〓L〓及四种过渡金属(Zn、Ni、Co、Cu)配合物,两个含酚羟基的Schiff碱三足配体H〓L〓和H〓L〓及稀土配合物,一个含杂环的酰胺型三足配体L〓,培养了配体L〓的单晶,确定了其晶体结构。

The research suggested that American white oak is the best choice for the production of grape wine with strong oak aroma and European oak is the best choice for the production of grape wine with harmonious oak aroma, fruit aroma and wine aroma; air drying process of barrel plates would influence the content of total phenol, tannin and volatile substances including vanillin and MOL; and baking intensity will change original content of chemical compositions in oak and make oak barrel possess different aroma characteristics and phenol substance content.

研究表明,酿制橡木香较浓郁的葡萄酒选用美国白栎较好,酿造像木香、果香、酒香协调的葡萄酒则选择欧洲橡木较适宜;板材风干过程对橡木板材中的总酚、单宁含量及挥发性香气物质香兰素和橡木内酯的含量均有影响;烘烤强度可改变橡木木材原有的化学组分含量,使橡木桶具有不同的呈香特性和酚类物质含量。

The research suggested that American white oak is the best choice for the production of grape wine with strong oak aroma and European oak is the best choice for the production of grape wine with harmonious oak aroma, fruit aroma and wine aroma; air drying process of barrel plates would influence the content of total phenol, tannin and volatile substances including vanillin and MOL; and baking intensity will change original content of chemical compositions in oak and make oak barrel possess different aroma characteristics and phenol substance content.

研究表明,酿制橡木香较浓郁的葡萄酒选用美国白栎较好,酿造橡木香、果香、酒香协调的葡萄酒则选择欧洲橡木较适宜;板材风干过程对橡木板材中的总酚、单宁含量及挥发性香气物质香兰素和橡木内酯的含量均有影响;烘烤强度可改变橡木木材原有的化学组分含量,使橡木桶具有不同的呈香特性和酚类物质含量。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。