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Result The results showed that its components were quite complex, and 89 organic compounds were identified. There were 72 kinds of oxygen-containing organic compounds which included esters, phenols, aethers, ketones and alcohols in the depolymerization product, small amounts of alkanes, alkenes, arenes, thiophenol and nitrogen-containing organic compounds were also detected, which showed that characteristics of the product with high oxygen content, low nitrogen and sulphur content.

结果]超临界乙醇解聚产物成分十分复杂,GC/MS分析鉴定出89种有机化合物,其中72种为含氧化合物,主要有酯、酚、醚、酮和醇等,还检测出少量烷烃、烯烃、芳烃、苯硫酚和含氮化合物,反映了解聚产物的高含氧量和低含氮硫量的特性。

High content α-tocopherol was prepared from tocopherol mixture (tocopherol content 52.3%).

以含量为52.3%的混合生育酚作原料制备高含量的α-生育酚。

Rational reaction condition is that ratio of the Cu(superscript 2+) schiff base complex of disproportionated rosin amine is 3%, urushiol concentration is 68.8 g/L, the system of reaction reacts 36 h at 30℃ in alcohol dissolvent.

结果表明,氧化聚合反应的理想条件是以乙醇为溶剂,加入3%歧化松香胺席夫碱-铜配合物催化剂,漆酚浓度为0.0688g/ml,在30℃下反应36h后,漆酚聚合物的沉淀得率为51.3%。

A colorless to yellowish oily liquid containing phenols and creosols, obtained by the destructive distillation of wood tar, especially from the wood of a beech, and formerly used as an expectorant in treating chronic bronchitis.

杂酚一种含有酚混合物的无色到黄色油状液体,可由木焦油干馏而得,以前被用作治疗慢性支气管炎的祛痰剂

A colorless to yellowish oily liquid containing phenol s and creosols,obtained by the destructive distillation of wood tar,especially from the wood of a beech,and formerly used as an expectorant in treating chronic bronchitis.

杂酚一种含有酚混合物的无色到黄色油状液体,可由木焦油干馏而得,以前被用作治疗慢性支气管炎的祛痰剂

After the diazotization ,2-aminophenol-4-(2-'carboxy)sulfanil phenylamine was coupled with acetoacetanilide,2-naphthol,1-phenyl-3-methyl-5-pyrazolone,1-naphthol-4-sulfonic acid,separately to get the different diazotized compounds,then complexed with potassium chromium sulfate or cobaltous chloride to obtain the yellow,orange,red,purple,blue and other colour dyestuffs.

2-氨基苯酚-4-(2'-羧基)磺酰苯胺重氮化,分别与乙酰乙酰苯胺、2—萘酚、1-苯基-3-甲基-5-吡唑啉酮、尼文酸、1-乙酰氨基-7-萘酚等偶合,得到不同的偶氮化合物,然后分别与硫酸铬或氯化钴进行络合反应,得到黄、橙、红、紫、蓝多种颜色染料,并进行了毛织品的染色实验。

Early stage of infection by alginic acid decomposing bacteria, the contents of polyphenol compound increased quickly,but the activities of polyphenol oxidase were stabilized.

在褐藻酸降解菌感染海带的初期,多酚类化合物含量骤然升高,而多酚氧化酶的活性却没有明显变化。

Under the selected chromatographic operation conditions, the 2,2'-Dihydroxy-1,1'-binaphthyl, 2-Naphthol and other impurities could be separated efficiently.

在选定的色谱条件下,1,1'-联-2-萘酚和2-萘酚等杂质之间具有较好的分离效果。

Based on the associated reactions of bromothymol blue with cationic surface- active agent when put in phosphate buffer solution of pH7.5~8.5 and fades, a new way for determination of cationic surfactant by Spectrophotometric methods was established.

摘 要:基于溴百里酚蓝在 pH7.5~ 8 5的磷酸盐缓冲介质中,与阳离子表面活性剂发生离子缔合反应,而使溴百里酚蓝褪色这一现象,建立了分光光度测定阳离子表面活性剂的新方法。

Metabolites, including 1 phenolic diterpene, 2 phenolic acids (rosmarinic acid and caffeic acid), 2 flavonoids (6-methoxyluteolin-7-glucoside and homoplantaginin) and 1 coumaric acid ( cis-4-glucosyloxycinnamic acid), were successfully identified from two rosemary extracts with chloroform-methanol ( v / v , 3/1) and 50% aqueous methanol on the basis of HPLC, UV, NMR and MS data.

基于高效液相色谱、紫外吸收、核磁共振波谱及质谱数据,具有代表性的6个迷迭香代谢物的结构得到了确定,它们分别为1个酚类二萜、2个酚酸、2个黄酮(6-甲氧基木樨草素-7-葡萄糖苷和高车前甙)和1个香豆酸(顺-4-香豆酸葡萄糖苷)。

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