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Objective To Optimize the extraction process of Salvia acid from Salvia miltiorrhiza.

目的 优化丹酚酸的提取工艺,提高丹酚酸B的提取率。

To avoid the influence of ammonolysis, alcoholysis and hydrolysis on molecular structure identification, in this paper, derivational estimation is utilized to confirm molecular structures ofβ-naphthol-containing sulfonyl chloride intermediates. Then the structures of corresponding sulfonamide dyes are also confirmed by FTIR,~1H NMR and mass spectrometry.

为了避免磺酰氯化合物发生水解、醇解和胺解等衍生化反应影响磺酰氯化合物分子结构表征,本文采用衍生化反推法证明了β-萘酚结构磺酰氯化合物的分子结构,并利用红外光谱、核磁共振氢谱、质谱表征了含β-萘酚结构磺酰胺染料的分子结构。

Some new lignans of dibenzocycloheptadiene and benzofuran analogues were first synthesized successfully by intramolecular nonphenolic oxidative coupling and rearrangement of the 1,4-biaryl-2,3-dimethyl-2,3epoxide substituted butanes with DDQ in TFA.

以DDQ为非酚氧化偶合试剂与1,4-二芳基-2,3-环氧类化合物进行分子内的非酚氧化偶合反应,首次合成了二苯骈环庚二烯类和苯骈呋喃类的新型木脂素,其结构由不同光谱和X-单晶衍射所确证。

All the experimental operations were carried out under the conditions of water-free and oxygen-free in nitrogen stream. The synthesis and characterization of novel enantiopure {[2Na]3[Sm3]}(1) and {[2Na]3[Gd3]}(2) were described.

在无水无氧条件下,以氯化钐、氯化钆和R-联萘酚为原料室温合成了手性联萘酚稀土配合物{[2Na]3[Sm3]}(1)和{[2Na]3[Gd3]}(2),对所合成的配合物进行了荧光性能研究。

It can be concluded that polyphenol tablet from Chinese green tea has evident anti-plaque effect.

茶多酚含片具有明显的抗牙菌斑作用。茶;牙菌斑;茶多酚

Both black and green tea contain polyphenols substances thought to block cell damage that can lead to cancer.

红茶和绿茶都含有茶多酚,茶多酚被认为可以阻断对细胞的损伤,细胞损伤会引发癌症。

Pentachlorophenol is one of the most toxic organic pollutants that are difficult to degrade in chloropenoxies.

五氯酚是氯酚族中最具毒性和最难降解的有机污染物。

Using N,N′-dimethy-p-toluidineas the catalyst,bisphenol A-glycidyl methacrylate,the resin matrix in most dental composite restorative materials,was synthesized by the reaction of bisphenol A and glycidyl methacrylate,and characterized by FTIR,~1HNMR and M S.

以N,N-二甲基对甲苯胺为催化剂,双酚A和甲基丙烯酸缩水甘油酯为原料合成了一种常用的口腔修复材料树脂基质———双酚A双甲基丙烯酸缩水甘油酯,并用FTIR1、HNMR和质谱对其结构进行表征。

With TEMPO(5 mol%) as the catalyst,N-methyl-N-phenyl-hydrazine(1.2 equiv.) as the amine source,the direct ortho-amination of 2-naphthols could be easily achieved.The reaction was carried out at room temperature under air atmosphere.

以5 mol%TEMPO为催化剂,1.2当量N-甲基-N-苯基肼作氨源,二氯甲烷为溶剂,空气中,室温下,实现了对2-萘酚邻位氨基化,可以高效的合成1-氨基-2-萘酚类化合物。

With TEMPO(5 mol%) as the catalyst,N-methyl-N-phenyl-hydrazine(1.2 equiv.) as the amine source,the direct ortho-amination of 2-naphthols could be easily achieved.

以5 mol%TEMPO为催化剂,1.2当量N-甲基-N-苯基肼作氨源,二氯甲烷为溶剂,空气中,室温下,实现了对2-萘酚邻位氨基化,可以高效的合成1-氨基-2-萘酚类化合物。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

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