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The adsorption orientations of benzene derivatives, thiophenol, 4-aminothiophenol and 1,4-dithiobenzene, were investigated on the surfaces of roughened Ag electrodes by using surface-enhanced Raman spectroscopy.

采用表面增强拉曼光谱技术研究了苯硫酚及其功能衍生物,对巯基苯胺和对苯硫酚在粗糙银电极上的吸附取向特征。

METHODS With thymol and bupivacaine as the internal standards for propofol and lidocaine respectively,the extraction was performed with cyclohexane.

以麝香草酚和布比卡因分别为异丙酚和利多卡因的内标,样品用环己烷提取。

The absorption of NH + 4 was lowered by t he i ndophenol method because of the similar structure of thymol and phenol.

由于百里酚与苯酚结构相似,造成靛酚法的铵离子分析中吸光度有所降低。

Objective To investigate the effect of remifentanil combined with propofol in totally intravenous anesthesia on children undergoing tonsillectomy.

目的 探讨瑞芬太尼、丙泊酚全凭静脉麻醉与芬太尼、丙泊酚和异氟烷静吸复合麻醉在小儿扁桃体摘除术中应用的比较。

The results showed that the phenolics in cranberry would reduced. The free quercetin showed the best stability. And the flavonoids and proanthocyanidins were the second. The total phenolics showed the worst stability.

结果显示,蔓越莓中的酚类化合物含量会随储存时间而下降,其中以游离态quercetin之安定性最佳,总类黄酮及前花青素则其次,在总酚类化合物之安定性最差。

The result shows that catalyst concentration, reaction time, urushiol concentration and temperatures affect the polymer yield in oxypolymerization of urushiol system.

讨论了该配合物作为催化剂,催化漆酚氧化聚合反应时,催化剂浓度、时间、底物浓度以及温度对漆酚氧化聚合反应的影响。

DISCUSSION Using both propofol and fentanyl together for induced abortion opration has kinds of excellencis,such as quick rising effects,clam inducement and convalescence,expeditious vivification,and that is safety and effective measure for anaesthesia.

病例报告]给200例ASA分级Ⅰ级早期妊娠患者在丙泊酚复合小剂量芬太尼麻醉下施行人工流产术,未出现疼痛及人工流产综合征等并发症。[讨论]丙泊酚及芬太尼联合应用于人工流产手术具有起效快,诱导和恢复期平稳,苏醒迅速等特点,是安全且有效的麻醉方法。

Extracting Tea Polyphenolswith acetoacetic ester is a Key technique in TP indus- trial production.

乙酸乙酯萃取茶多酚是茶多酚工业生产中的关键技术。

Novel organic silane of 3,3′-dihydroxyldiphenoxydimethyl alkoxy silane and 3,3′,3-trihydroxyldiphenoxydimethylalkoxy silane triglycidyl ether for epoxy resin modification were synthesized.

研究了含酚羟基有机烷氧基硅烷及3,3′,3-三羟基苯氧基硅烷三缩水甘油醚两种新型有机硅改性剂对双酚F环氧树脂力学性能及热性能的影响。

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物,利用理化性质和波谱技术(UV、IR、EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构,分别为9种蒽醌类化合物:大黄酚,大黄素甲醚,大黄素,芦荟大黄素,大黄酸,番泻苷A或B,ω-羟基大黄素(ω-hydroxylemodin),大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside),芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside);3种菲醌类化合物:丹参酮ⅡA(tanshinoneⅡA),隐丹参酮,丹参酮Ⅰ(tanshinone Ⅰ);1种异黄酮:7,3'-二羟基-5'-甲氧基异黄酮(7,3'-dihydroxy-5' methoxyisofla-vone)以及原儿茶醛,原儿茶酸,黄芪甲苷(astragaloside Ⅳ),苦杏仁苷,2,3,5,4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷(2,3,5,4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside),Z—儿茶素,桂皮酸。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

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