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Therefore this research is to synthesize alkyl dialkyl o-hydroxyphenyl phosphate (8) as new lubricant additives.

所以本研究希望能结合磷酸酯与儿茶二者的优点以开发出新型态的润滑油添加剂---儿茶磷酸酯衍生物。

Two monomers,bispmpargyl ether of bisphenol-Aand 4,4'-biphenyl dibenzyl azide were synthesized and characterized with FT-IR,1H-NMR and elementary analysis.

合成了两种单体双A二炔丙基醚与4,4′-联苯二苄叠氮,研究了一种新的低温聚合体系——双A二炔丙基醚与4,4′-联苯二苄叠氮在烘箱中的本体聚合行为。

The experimental group(28 cases) was injected Tc-MDP 5mg/days by vein and received Diclofenac Diethylamine Emulgel drug .

对照组(26例)常规采用非甾体抗炎药物双氯酸治疗,治疗组(28例)在服用双氯酸的同时静注 Tc-MDP(5mg/d)。40d后获取两组静脉抗凝血(3ml),分离出红细胞与血浆。

Experimental results indicate that the reduction of chemical oxygen demand were 40%, 38%, 12%, 50%, and 73% for β-naphtho1, salt R, dihydroxy salt R, acid red, and wastewater, respectively when the reactions had run for 4 h at a pH of 1.7. In comparison, the COD reduction of-naphtho1 and salt R were 10.2% and 16.2%, lower than 23.4% and 18.1% with H2O2, while the Fenton reaction time was 1 h.

当pH=1.7、反应4h时,β-萘、R盐、二羟基R盐、酸性红、实际废水的化学需氧量去除率分别可达40%、38%、12%、50%和73%;对比实验显示,反应时间为1h时,β-萘和R盐的COD去除率分别为10.2%和16.2%,而用H2O2则分别为23.4%和18.1%。

The method comprises following steps: taking diphenol and 3- trifluoromethyl- 4- chloronitrobenzene as raw material, salt precipitating for diphenol and potash, refluxing with water- containing toluene, reacting with 3- trifluoromethyl- 4- chloronitrobenzene and getting dinitro monomer; taking dinitro monomer, ferro powder and HCl as raw material, ethanol and water as disslovant for refluxing and ethanol recrystallization, getting fluorine- containing aromatic diamido monomer.

合成方法是以二与3-三氟甲基-4-氯硝基苯作原料,先将二与碳酸钾成盐,甲苯带水回流反应,然后与3-三氟甲基-4-氯硝基苯反应制得二硝基单体;再以二硝基单体,铁粉,HCl为原料,乙醇和水做溶剂,回流反应、乙醇重结晶,得到含氟芳香二胺基单体。

Specificity studies on the substrate revealed that the HdPO was capable of oxidizing not only the o-diphenol, but also tyrosine. The apparent Km value on tyrosine was about 9.52 mmol/L. As shown in the experiments, HdPO behaved oxidizing activities both on diphenol and monophenol, which implies that the HdPO was probably not only a type of tyrosinase-type PO but also a catechol-type.

底物特异性研究还发现此HdPO不仅对邻苯二具有氧化活性,对酪氨酸底物也具有氧化活性,且对酪氨酸的Km值约为9.52mmol/L,说明该酶既具有酪氨酸酶活性,又具有儿茶酶活性。

Wood Vinegar is a natural material that is distilled from wood. It is compose of organic acid and hydroxybenzene , Various dosage of wood vinegars, pyrolignerous acid and guaiacol were mixed into organic manure firstly in this experiment, and then, the above said organic manure are separately added into soil. Under the analysis of the amount of the edaphon, adding 10g wood vinegar to 1kg organic manure and 30kg soil can much active the edaphon effectively in a short term and make a maximum rising extent of edaphon numbers.

木醋液是从多年生柞木中经过高温蒸馏出来的纯天然物质,其主要成分是有机酸和类物质,为了明确木醋液和主要成分对土壤微生物的作用,将加入不同剂量的木醋液、愈创木、醋酸的有机肥施入土壤,观察土壤中微生物数量的变化,结果表明:在1kg有机肥中加入10g木醋液,施入30kg土壤中,土壤微生物数量增加幅度最大,土壤微生物10d内被有效地激活;同时,当在1kg有机肥中木醋液的添加量高达50g时,对土壤微生物有一定的抑制作用。

The Spectrophotometry method was used in experiment, the results is that the content of polyphenol is 14.8 mg/g in Jianshui's Elsholtzia bodineri Vaniot., which was higher than Shiping. The content of total flavones in the tea is 52.8 mg/g in Shiping, 43.9 mg/g in Jianshui.

通过分光光度法检测红河州两个县市野山茶茶水中的多类物质及总黄酮的含量,结果表明建水野山茶多类物质含量较高,为14.8 mg/g;石屏野山茶总黄酮较高,为52.8 mg/g。

All the complex series based on 4',4''-dicarboxy-1,6-diphenoxyhex- ane (C6-2COOH) and 4',4''-dicarboxy-1,10-diphenoxydecane (C10-2COOH) possessed higher melting and clearing points, usually showed soft crystal or crystalline smectic phases and crystal polymorphs except C10-2COOH/ p -PhBPy complex displaying also an enantiotropic nematic phase, while the complexes based on 4,4'-dicarboxy-α,ω-diphenoxy tetraethyleneglycol ether (C8O4-2COOH) with a longer flexible spacer exhibited monotropic fluidic smectic SmA and/or nematic phases.

研究表明,分别具有较短的6或10个亚甲基的烷烃间隔基的双苯甲酸衍生物4',4''-二羧酸-1,6-二氧基己烷(C6-2COOH)和4',4''-二羧酸-1,10-二氧基癸烷(C10-2COOH)的系列复合物具有较高的熔点和清亮点,一般都只出现结晶近晶相和多晶型转变现象。

Objective:To establish a method for determining the contents of total phenolic acid in Evodia rutaecarpaJuss.

目的:建立吴茱萸中总酸含量的测定方法,测定吴茱萸及其炮制品中总酸的含量。

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