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The results showed that the addition of alcoholate increased the elution recovery of phenolic acids on resins in supercritical CO2. The infrared spectroscopy was used to study the interaction between solute and solvent molecules in supercritical fluid. The hydrogen bond between alcoholate entrainer and phenolic acid was the main factor to increase the ability of supercritical elution. The results appeared that salvianolic acids could be extracted by supercritical carbon dioxide with ethanol as entrainer.

结果表明:醇类夹带剂的加入能大大提高树脂上酸类化合物的超临界洗脱率;通过红外光谱技术研究了超临界流体中分子间的相互作用与超临界洗脱过程的关系,认为醇类夹带剂与酸类化合物的氢键作用是提高酸类化合物洗脱率的主要因素;以乙醇为夹带剂的超临界CO2洗脱可应用于丹参酸的提取。

The method, which is capable of effecting very good separation of phenol and the 3 cresol isomers under the same chromatographic conditions, can be used to determine phenolic compounds in phenolic tar by external standard, and to analyze these compounds in the toxic leaching solution of the tar.

摘 要:建立了焦油中类物质质量分数测定和浸取毒性测定的气相色谱法,此法可以在同一色谱条件下对焦油中的苯及邻、间、对甲实现很好的分离,利用外标法分别进行定量分析,并对焦油浸取液中相应组份进行测量。

They have close relationship as the former may provide new ideas and approaches for the later, while the later may be the simulation for the former and gives it helps in degradation products identification and mechanism explanation. It is necessary to choose a suitable system, which has high potential of treating EDs and close relationship to the natural environment, to combine the researches in the two aspects. Our group has been engaged in researches on the photochemical properties and application to water pollution control of different ferric species including Fe -OH complexes, Fe -polycarboxylate complexes, Ferric oxides and Fe -humic acid complexes. Fe -oxalate complexes system has higher efficiency than the other ferric species systems in photooxidation and degradation of organic compounds. This thesis is focused on the photodegradation of nine EDs estradiol (E2), estrone (E1), 17α-ethynyl estradiol (EE2), diethylstilbestrol , bisphenol-A , 4-Nonylphenol , 4-Octylphenol , di-n-butyl phthalate , and di (2-ethylhexyl) phthalate .

因此从处理效率和环境化学意义两方面考虑,结合本课题组在不同铁形态(包括Fe-OH配合物、Fe-多羧酸配合物、Fe氧化物、Fe-腐殖酸配合物等)的光化学特性及其在水污染控制中的应用方面较系统的研究工作基础,本论文选择了四类共9种典型的内分泌干扰物(雌二醇(E2)、雌酮(E1)、17α-乙炔基雌二醇(EE2)己雌、双A、壬基、辛基、酞酸二丁酯和酞酸二乙基己基酯),研究了它们在Fe-草酸盐配合物体系中的光降解效果,推测其降解机理,探索环境内分泌干扰物光氧化处理的新体系,同时为预测其在环境中的光降解行为提供了依据。

96H LC 0,96 h LC 50 ,and 96 h LC 100 of twelve chemicals of phenol ,alkyl benzene and nitrobenzene,and three water samples to sword fish(\%Xiphophorus helleri)\% and rare minnow(\%Gobiocypris rarus\%) were tested.3. The phenol ic waste water was purified through the absorption of polyvingl pyridine.

介绍了含废水与聚乙烯基吡啶类树脂接触,类会吸附在树脂上,使废水得到净化,然后将吸附了类的树脂加热处理回收,与此同时,对树脂也进行了再生处理,再生后的树脂可循环使

The reactions of several phenols and 2, 2, 6, 6-tetramethyl-4-substituted piperidine oxoammonium salt have been studied. It was found that these oxoammonium salts are new facile reagents for phenolic coupling.

应用2,2,6,6-四甲基哌啶氧铵盐实现了类的氧化偶联反应:对位取代的类底物得到邻位-邻位偶联产物;2,6-二取代的类底物得到对位-对位偶联产物;2,4,6-三取代的阻碍类底物得到苄位氧化偶联产物。

Using tea polyphenol and Vc as the control, the effect of lotus seed polyphenol on scavenging OH and O2(superscript -) was studied with Fenton reaction and pyrogallol autoxidation methods.

以茶多和Vc为对照,采用Fenton反应法研究莲子多对羟自由基的清除作用;采用邻苯三自氧化法研究莲子多对超氧阴离子自由基O2

But urushiol has a poor resistance to alkali because phenol hydroxyl of urushiol shows weak acidity. Meanwhile, inherent brittleness of urushiol has limited its development and application.

但是,由于漆羟基显弱酸性,使得漆耐碱性较差;同时,漆清漆固有的脆性等也限制了其发展和应用。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多,用显色反应检识羟基;采用紫外分光光度法对多粗体物进行总多含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

Compared with pearled grain, whole grain has higher concentration of oil and tocol, showing that seed coat may be one of the major tissue accumulating oil and tocol.

大麦油的母育组成成分主要为α-生育(占总生育的65.4%)和α-生育三烯(占总生育三烯的70.7%)。

Methods: A total of 21 young swines were randomly divided into untreated group, low-dose salvianolate group and high-dose salvianolate group (7 in each group). AMI was induced by ligaturing left anterior descending coronary artery. After the operation, 400 or 200 mg salvianolate dissolved in 250 mL 5% glucose saline was administered by intravenous drip to swines in the HS group and the LS group respectively for 7 days. The swines in the untreated group were administered with 250 mL 5% glucose saline.

苏中幼猪21只,随机分为模型组和低、高剂量丹参多酸盐组。3组均经开胸结扎冠状动脉左前降支制作心肌梗死模型,造模成功后当日,高剂量丹参多酸盐组给予400mg丹参多酸盐加250mL 5%写葡萄糖生理盐水静脉滴注;低剂量丹参多酸盐组给予200mg丹参多酸盐加250mL 5%葡萄糖生理盐水静脉滴注;模型组给予等体积的5%葡萄糖生理盐水静脉滴注。1次/d,连续给药7d。

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Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势,并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。

This dramatic range, steeper than the Himalayas, is the upturned rim of the eastern edge of Tibet, a plateau that has risen to 5 km in response to the slow but un stoppable collision of India with Asia that began about 55 million years ago and which continues unabated today.

这一引人注目的地域范围,比喜马拉雅山更加陡峭,是处于西藏东部边缘的朝上翻的边框地带。响应启始于约5500万年前的、缓慢的但却不可阻挡的印度与亚洲地壳板块碰撞,高原已上升至五千米,这种碰撞持续至今,毫无衰退。