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The addition of puerarin, tea polyphenol and acid compositions in VECO effectively improved the effects on soberness, intoxication avoiding, ataxia correcting and memory barrier eliminating. The tea polyphenol has superior behavior on soberness, intoxication avoiding and memory barrier eliminating than that of puerarin, while puerarin is more effective in the function of ataxia correcting than tea polyphenol.

金葛露中加入葛根素、茶多和酸类物质有助于解酒、防醉、纠正运动失调和改善记忆障碍,其中茶多的解酒、防醉和改善记忆障碍的效果比葛根素明显,葛根素纠正运动失调作用的效果比茶多明显。

The factors relevant to the running buffer and their effects on separation were investigated. The buffer solution composed of 30 mmol/L sodium borate and 2.4 mmol/L β-CD was found to be the most suitable electrolyte for separation. The second order dissociation constant range of honokiol was estimated. The content range of honokiol in Cortex Magnoliae Officinalis and was 3.42-5.98 mg/g, while the mean content of honokiol in its preparation 0.021 mg/mL.

优化了厚朴提取物的分离条件,考察了缓冲溶液浓度、pH 值、β-CD的添加浓度对分离的影响,确定了最佳的分离缓冲溶液组成为30 mmol/L 硼砂和2.4 mmol/L β-CD,pH 值为9.48;推测出和厚朴的二级离解常数pKa2 的范围为9.94-10.83;在优化的分离条件下,测定了厚朴药材和藿香正气口服液中和厚朴的含量分别为3.42-5.98 mg/g、0.021 mg/mL,和厚朴的线性范围是0.020-0.405 mg/mL,其线性相关系数R=0.998(n=5),加样回收率为98.4-103.5%,RSD 为3.2-5.7%(n=3)。

Methods: 50 female patients undergoing induced abortion, received propofol intravenous anaesthesia, induction dose was 2mg~2.2mg/kg, superaddition propofol 30mg~50mg to maintain anaesthesia depth.

50例接受人工流产手术的患者,用丙泊静脉麻醉,诱导剂量为2~2.2mg/kg,用质量分数为2%的丙泊,在20s的时间内均匀注入,术中病人有略微肢动时追加30~50mg丙泊以维持麻醉深度。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下,以异丙醇作溶剂,苯硒与化合物2不反应。在氢氧化钾存在下,以异丙醇/水作溶剂(体积比20:1,在室温下,硒可以有效地进攻中化合物2中1,3,2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件,顺利实现了硒对N^1-(2-呋喃基)-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环,生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

Methods The propofol in blood was extracted with cyclohexane,and thymol was used as the internal standard,determining the concentration of propofol by HPLC fluorescence detector.

用环己烷提取全血中的丙泊,以百里为内标定量,用HPLC 荧光检测器测定丙泊含量。

The detection wavelength was set at 274 nm.Result The linear range of thymol was 0.04~1.23 mg (r=0.9999),and the average recovery was 99.02%(RSD 1.03%).

结果 百里香在0.04~1.23 mg (r=0.9999)有良好的线性关系;平均回收率百里香99.02%(RSD 1.03%),重复性百里香RSD 0.88%。

A hydrolysis approach has been developed to prepare polyurushiol -SnO 2 hybrid film from urushiol-Sn polymer which is synthesized with urushiol and stannic chlorde.

先由漆和四氯化锡合成非螯合型漆锡聚合物,然后采用水解法由该聚合物与NaOH水溶液制得聚合漆-SnO2 杂化材料。

The synthetic organic chemicals, such as phenol, m cresol, phloroglucinol, phenylamine, 3,5 xylenol, p tertiary butyl phenol, nitrobenzene, tert butanol and chloral were oxidized in supercritical water system.

研究了超临界水氧化系统中合成有机化学品,如、间苯三、对叔丁基、间甲、3 ,5-二甲、苯胺、硝基苯、叔丁醇、三氯乙醛等的氧化作用。

ConclusionWhen fentanyl combined with Diprivan is used in supraconduction visible aponia induced abortion, the method that Diprivan isused 3 min after fentanyl is used, can decrease dose of Diprivan and reduce adverse effects, and it may be safe, effective and economic vein anesthesia method.

在芬太尼复合异丙对超导可视无痛人工流产中,使用芬太尼3min后静推异丙可以明显减少异丙的用量,减少不良反应的发生,是安全、有效、经济的静脉麻醉方法。

More and more attention is focusing on the safty of drinking water suply. In this paper, firstly, chloramine formation and the characteristics and kinetics of monochloramine autodecomposition were studied. Secondly, considering the high concentration of ammonia and the complication of organic matters in Shanghai Huangpu River, formation characteristics and rules of disinfection byproducts were reviewed during the breakpoint chlorination process, and on the basis of grading and clssification of organisms, the control effects of chloramination on DBPs formation were studied. Finally, the formation rules of 2-monochlorophenol, 2,4-dichlorophenol and 2,4,6-trichlorophenol from phenol chlorination were investigated, and related influencing factors and kinetics were analysed.

饮用水的安全供给受到越来越多的重视,本文首先进行了氯胺形态以及一氯胺自降解特性及其动力学研究;然后结合上海黄浦江水源氨氮浓度高、有机物成分复杂的特点,研究折点加氯过程中消毒副产物的生成特性和规律,以及在将有机物分级和分类的基础上,研究氯胺消毒对不同类别有机物生成消毒副产物的控制效果;最后考察了氯化苯生成2-一氯(2-MCP)、2,4-二氯(2,4-DCP)及2,4,6-三氯(2,4,6-TCP)的规律,并进行了影响因素和动力学分析。

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