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Amounts of 2 furaldehyde and 5 hydroxymethyl 2 furaldehyde in wood vinegar from the treated wood were increased,but amounts of carboxylic acids,phenols,pyrocatechol,guaiacols,and maltol were almost constant.

与未处理材相比,处理材木醋液中糠醛及5 羟甲基糠醛的收量增加,而羧酸类、苯类、邻苯二、愈创木类及麦芽的收量几乎不变。

The effect of aqueous ethanol (50% v/v) on the activity of purified mushroom polyphenol oxidase has been found to be as follows:(1)The oxidation of catechol or pyrogallol is greatly stimulated,an increase in the rate of oxygen uptake of over 100% having been invariably observed with catechol as the substrate,whereas the oxidation of other substituted o-dihydric phenols is inhibited in 50% ethanol.

三无论有无抗坏血酸的存在,50%乙醇对多氧化酶活力的提高程度是一样的,在有一定量的抗坏血酸的存在下,多氧化酶对儿茶的 Michaelis 常数(25℃)在水溶液及50%乙醇溶液中各为0.072×10~(-3)M 及0.49×10~(-3)M。

The result shows that MWNT complex filtering membranes have 13.5% and 42.8% adsorptions for resorcin and alizarin red respectively. And, c-MWNT complex filtering membranes have 33.2% and 80.3% adsorptions for resorcin and alizarin red respectively. Comples filtering membrane have a great affinity for resorcin and alizarin red molecules. The membran been easily renewable, can be used repeatedly.

结果表明:制得的MWNT复合膜分别吸附了13.5%的间苯二和42.8%的茜素红;c-MWNT复合膜则分别吸附了33.2%的间苯二和80.3%的茜素红,复合膜对间苯二和茜素红表现出良好的吸附性,而且制得的复合膜极易再生,可重复使用。

Producted RF and CRF aerogels by process of sol-gel technics, dynamic-exchange, CO2 supercritical drying, and procedural increase in temperature carbonization methods, which have eximious capability and nanometer network structure; Systemic analysis various factors which effect gel course, such as ratio of reactants and the dosage of catalyst, and probed into the better experiments conditions(the concentration of resorcinol and formaldehyde is more than 2% and the value of R/C is between 50 and 300); During gel course , primary investigated the viscosity curve and particle size distribution of sol-solution, and analyzed the reason of catalyst dosage effects particle size of gel, and confirmed that the up-growth of gel follows the theory of " polymerize increase ".The experiment results indicated that ultrasonic with unvarying temperature disposal shortened gel time and optimized quality of gels, and the factors of ultrasonic effect gel reaction velocity were analyzed; Prepared organic aerogels using compounds of resorcin and hydroquinone substitute resorcinol reacts with formaldehyde the first time, and also optimized the proportion of resorcinol and hydroquinone (the proportion of hydroquinone in 10%~40%).

采用溶胶-凝胶工艺结合动态溶剂交换、CO2超临界流体干燥与程序升温碳化方法制备出性能优良、具有纳米网络结构的RF与CRF气凝胶;深入研究了反应物配比催化剂用量等条件对凝胶过程的影响,得到了较佳的RF凝胶制备条件(RF浓度应大于2%,R/C值取50~300);初步研究了凝胶过程中的粘度、粒径变化情况,分析了催化剂用量影响凝胶中粒子尺度的原因,在实验上印证了凝胶生长遵循"聚增长"的理论;通过引入超声波改进了RF气凝胶的制备工艺,缩短了凝胶反应时间,提高了凝胶品质,并探讨了超声波促进RF凝胶反应作用的原因;首次用对苯二与间苯二复配制备了混合有机气凝胶,优化出复配比(对苯二含量为10%~40%)。2。

Analysis of the treated aqueous solution was conducted with GC-MS,and the main intermediates during phenol degradation were isobutyric acid,malonic acid,benzoquinone,butenoic acid,oxalic acid,maleic acid,succinic acid,hydroquinone,catechol and resorcin.

利用GC-MS分析了苯降解主要中间产物为异丁酸、丙二酸、对苯醌、丁烯酸、乙二酸、顺丁烯二酸、丁二酸、邻苯二、对苯二及间苯二等,并据此推测了苯电催化氧化的可能反应途径。

Based on the β-cyclodextrins' fluorescence enhancement to resorcinol, a new way of fluorescence analysis for resorcinol is presented in this paper.

利用β-环糊精对间苯二的包络作用,增敏间苯二的荧光强度,提出一种测定环境中间苯二的荧光检测新技术。

The application fields and market situation of resorcinol in the United State, west Europe and Japan were narrated in detail. Meanwhile, the domestic consumption of resorcinol in different fields, its import and export situation were analyzed. And the expansion, newly construction of resorcinol units in China were summarized.

详细概述了美国、西欧和日本间苯二的应用领域及市场现状;同时还分析了国内间苯二在各领域的消耗和近几年的进出口情况,并对国内扩建以及新建的间苯二装置情况进行了全面的总结。

Inhibition to activated sludge process by 2-naphthol was also investigated by Warburg respirometer to verify the conclusion drawn from Rank Cell respirometer test. 2-Naphthol in low concentration was biodegradable, hence resulted in the acceleration of respiration, while in higher concentration 2-naphthol would dramatically inhibit microorganisms respiration on account of high K〓 and electron density.

用Warburg呼吸仪研究了2-萘对活性污泥过程的抑制作用,验证了RankCell呼吸仪的研究结论,发现低浓度下2-萘自身能被生物降解而使活性污泥中微生物呼吸速率升高;浓度增加后2-萘因良好的脂溶性和强亲核能力而对活性污泥过程产生强抑制。

Methods The effects of various concentrations of tea polyphenols on proliferation, invasion and apoptosis of CGTH W-3 cells were observed by MTF assay, plate scarification assay and flow cytometer, respectively.

方法用MTT法检测细胞增殖活性,观察不同浓度茶多对CGTH W-3细胞增殖活性的影响;并通过培养板划痕法观察茶多对CGTH W-3细胞侵袭能力的影响;应用流式细胞仪检测各浓度茶多诱导CGTH W-3细胞凋亡的作用。

Results show that the antibacterial component belongs to volatile oil、sesquiterpene、phenols and organic acids. The antibacterial part of the broth was isolated by silica gel column and 6 fractions of obviously antibacterial activity were obtained .By further study Fractions 1、2、3 contain sesquiterpene and fractions 8、9 contain phenols and fraction 10 contains phenolic organic acid.

对发酵液抑菌成分的研究表明,抑菌活性成分组成为挥发油倍半萜、和有机酸等类化合物,采用硅胶柱层析对发酵液抑菌活性部位进行分离实验,得到了6个具有明显抑菌活性的粗组分(组分1、2、3、8、9、10),其中组分1、2、3含有倍半萜类物质,组分8、9含有类物质,组分10中有含羟基的羧酸类物质。

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