酒石酸

The auxiliary can be recovered in high yield (81%) only by filtering and recrystallization. Besides, some other aldehydes have been chosen to test the enantioselectivity of N,N\'-dibenzyl tartamide, in comparison with two other allylaborates reagents developed previously by Roush and Brown, respectively. The results show that %e.e. of homoallylic alcohol is superior to that of the former, and approaches the Brown reagent.

产物经S_N2反应得瑞格列萘中间体-甲基烯丙基-2-氯苯基-叠氮甲烷(17)；同时，将筛选出的新型手性配体N-苄基酒石酸二酰胺用于其他几种醛(正丁醛，异戊醛和环己醛)的不对称烯丙基化反应，并与广泛应用的Roush配体(22)和Brown配体(27)相比较，发现其立体选择性优于Roush配体，并接近Brown配体，但明显具有可回收利用的优势。

This invention is directed to the-tartaric acid salt of 2-amino-N-{1-(2,4-difluoro-benzyloxymethyl)-2-oxo-2-3-oxo-3a-pyridin-2-ylmethyl-2-(2,2,2-trifluoroethyl-2,3,3a, 4,6,7-hexahydro-pyrazolo(4,3-c) pyridin-5-yl-ethyl}-2-methyl-propionamide which is a growth hormone secretagogue and as such is useful for increasing the level of endogenous growth hormone.

本发明涉及2－氨基－N－{1－－(2，4－二氟－卞氧甲基)－2－氧代－2－3－氧代－3a－(R－吡啶－2－基甲基－2－(2，2，2－三氟－乙基)－2，3，3a，4，6，7－六氢化－吡唑子基(4，3－c)吡啶－5－基－乙基}－2－甲基－丙酰胺的－－酒石酸盐，它是一种生长激素促分泌素，并且可用于提高内源性生长激素水平。

Controlled porosity osmotic pump tablets of sodium salicylate was prepared and the release profile was determined in vitro.

结果 最佳处方为：酒石酸用量30 mg，DEP用量23%，PEG用量3%，包衣增重4%，3批样品在12 h内体外释放符合零级过程。

The antimony doped tin oxide nanoparticles were synthesized at 240℃for 17 h by the complexing hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

摘 要：以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimony-doped tin oxide nanoparticles were synthesized at 240℃ for 17h by the complexing-hydrothermal oxidation method using stannate, antimony white and sulphuric acid as the starting materials, sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant. The resulting powders were characterized by means of differential thermal analysis, infrared spectrometry, X-ray diffraction and transmission electron microscope. The mechanism of the preparation of ATO powder was investigated as well.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合－水热氧化法在水热氧化温度为240℃和水热保温时间为17h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合－水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexinghydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

The antimonydoped tin oxide nanoparticles were synthesized at 240 ℃ for(17 h) by the complexing hydrothermal oxidation method using stannate,antimony white and sulphuric acid as the starting materials,sodium hydrotartrate as the complexing agent and hydrogen peroxide as the oxidant.

以锡酸钠、锑白和硫酸为原料，酒石酸氢钠为配合剂，双氧水为氧化剂，采用配合水热氧化法在水热氧化温度为240℃和水热保温时间为17 h时，合成单分散性的蓝色锑掺杂二氧化锡粉末，用差热分析、红外光谱、X射线衍射和透射电镜对所制得的粉末进行表征，并对ATO纳米粉体的配合水热氧化合成机理进行探讨。

After it was adjusted with ammonia until the test paper turned purple,in subacid medium of pH 6～7 ammonium acetate buffered solution,bivalent nickel was precipitated quantificationally by dimethylglyoxime.

试样以稀硝酸溶解高氯酸冒烟后，酒石酸掩蔽剂将铁等干扰元素配位掩蔽，以氨水调节至刚果红试纸呈紫色后，在pH6～7的乙酸铵缓冲溶液微酸性介质中，二价镍定量地被丁二酮肟沉淀。

The sample was dissolved by hydrofluoric acid and hydrogen nitrate, then the tantalite and hydrofluoric acid formed TaF6- in the media of tartaric acid－hydrofluoric acid.

试样以氢氟酸、硝酸溶解后，在酒石酸－氢氟酸介质中，钽酸与氢氟酸形成阴离子TaF6-，与结晶紫生成蓝紫色的络合物，用苯萃取出来采用光度法测定钽量，测定结果均在国标允许误差范围内。

In hot regions, extra tartaric acid is added to 'correct' the acidity.

在热的地区，需加入额外的酒石酸来"纠正"酸度。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失