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逐渐变化

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In order to disclosure the reason why the electrocatalysis activeness and selectivity droped after being used several hundred hours continuously, the x-ray diffraction, scanning electron microscopy and energy dispersive spectroscope have been used to characterize the surface condition variations of Monel metal. The results indicated: Monel metal belongs to the Cu-Ni alloy around the electrolysis experiment.And after being used for 600hr, the surface layer element composition and geometry distribution of the alloy changed, namely in the alloy the Cu element /which superficial free enthalpy was smaller,"concentrated" to the alloy surface,and formed one kind of marble structure microcrystallite.Thus the electrode surface becamed rough a

为了揭示蒙乃尔合金阴极在连续使用数百个小时后电催化活性剂选择性下降的原因,采用X射线衍射仪、电子扫描电镜和电子能谱分析仪对电解实验所用的蒙乃尔阴极材料在电解实验前后的表面状态进行了表征,结果表明:所使用的蒙乃尔合金阴极材料在电解实验前后均属于Cu-Ni合金,使用600hr后,由于表面层元素组成和几何排布发生了变化,即合金中表面自由焓较小的Cu元素向合金表面&富集&,形成一种大理石结构的微晶,表面粗糙、不均一,这是造成其对硝基苯电还原的催化活性及选择性随着使用时间延长而逐渐下降的主要原因,同时也为此类电极的修饰改进提供了方向。

The snails used for this study, measuring within the range of 7.1 to 3.0mm., were collected from the banks of Ching-San River, Chungking, Kiangsu.

从11月到第二年5月,卵巢呈丰满而多卵的状态;6月卵巢趋向萎缩;7、8月卵巢萎缩,内仅含有少量的幼稚卵细胞;9月卵巢开始趋向丰满;10月卵巢逐渐恢复丰满的状态。卵巢全年周期变化的过程与镇江地区钉螺的产卵情况基本上相符合。

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