进行实验

In this study, the following studies have been carried out(1)Test on a typical MR damper employed in this study was carried out, Neural network model based a direct model and a inverse model were established. The performance of the models were cpmpared with the Bingham model and the hyperbolic tangent model. Results show that ANN model can describe the mechanical behavior of MR damper perfectly as a nonparmetric model.

本文主要进行了以下三个方面的工作：(1)对一种典型的磁流变阻尼器进行了性能试验，利用实验实测数据建立了阻尼器的Bingham模型、双曲正切模型两种参数模型以及基于神经网络的正向和逆向模型，对三种计算模型进行了仿真分析，并与试验结果进行对比研究，结果表明，神经网络模型比两种参数模型能更好地模拟阻尼器的动态性能。

Main contents and conclusions are: 1 The ionization current was measured continuously by a charge-integration method with a computer after the introduction of radon into the chamber.

主要内容及结论：1充氡后利用计算机连续进行电离电流累积测量，得到了精细的电流随时间的变化曲线，可清楚看出氡及其子体的生成衰变造成的电离电流的生长—稳定—衰减过程，与理论计算值进行了比较，由电离电流衰减速度的变化得出氡吸附作用的影响，并测量到电离室冲洗后氡的反扩散现象；2由已知活度的标准源定出相对测量的刻度系数K值，K=24.62 Bq／pA，对同一个监测源以半年为周期进行多次测量后得出稳定性符合要求；3通过测量电离电流和气压的关系曲线以及不同气压下的饱和曲线，确定了常规的工作条件；4测量了盐酸清洗电离室内表面降低本底的效果；5不确定度分析表明相对测氡的扩展不确定度(k=2)小于5％，由本底涨落得出探测下限为0.5 Bq；6理论上对壁损失修正进行了计算，实验上保持电离室工作在饱和区的情况下，测量了不同气压下电离电流的变化，从中得出了壁损失随气压变化的规律，可以看出，电离电流的实测值和计算值随气压变化规律基本一致；当气压大于125 kPa时，端效应等其它因素造成的影响不大于2％，因而在此工作条件下，测量电离电流后通过计算修正壁损失可以实现近似的绝对测氡，提出了进一步提高绝对测量准确度的方法。

The fluid film bearing-flexible rotor nonlinear system with squeeze film damper is modeled practically using the finite element method and the Hamilton principle.(3) The film forces produced by fluid film bearing and squeeze film damper are determined by finite element method at any moment, and the Jacobian matrix is also determined.(4) A method for analyzing the dynamics of a large system with local nonlinearities is presented. The stability and bifurcation of the equilibrium position and the unbalance responce of a fluid film bearing-flexible rotor system with squeeze film damper are investigated based on the assumption of an incompressible lubricant together with the long bearing approximation for fluid film bearing, short bearing approximation for squeeze film damper and the"π"film cavitation model.

主要研究内容包括下面几个方面：（1）对挤压油膜阻尼器-滑动轴承-转子非线性动力系统中的非线性现象进行了机理方面的研究；（2）应用有限元方法及Hamilton原理对复杂的挤压油膜阻尼器-滑动轴承-转子非线性动力系统进行了建模分析；（3）对滑动轴承及挤压油膜阻尼器中任一时刻的油膜力及相应的Ja-cobi矩阵的确定进行了分析；（4）对一类具有局部非线性的多自由度动力系统，提出了一种可以有效地分析其动力特性的方法；（5）采用实验与理论分析相结合的方法，对挤压油膜阻尼器-滑动轴承-转子非线性动力系统的动力特性进行了分析。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小，进行综合分析，确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量，测定条件：加入100ml浓度为8.0±0.1％的氢氧化钠，在恒温水浴中煮沸回流6h；采用溶剂萃取法测定JOB-1C中TATB的含量，选择TATB饱和的二甲基甲酰胺为萃取溶剂，用G4坩埚式过虑器进行萃取分离；采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量，通过实验确定了多波长组合：λ=267nm，275nm，283nm，291nm，299nm；朗波—比耳定律的适用范围为PNP浓度：0.005～0.025mg/ml，HMX浓度：0.06～0.30mg/ml；在测定波长下，对PNP、HMX标准溶液的吸光度—浓度进行线性回归，由回归曲线的斜率得出PNP、HMX的吸收系数；根据朗波—比耳定律和吸光度加和性原理，在测定波长下，对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归，回归曲线的斜率即为混合溶液中PNP的浓度。

According to the theory of Sagnac FourierTransform spectrometer, the method which we used to reconstruct the spectrum correctly from the captured interferogram was developed. With the steps of trend term correction, apodisation, phase correction and conjugate symmetrization applied to the interferogram captured and then reconstructed it, the error was avoid.The experiment to reconstruct the spectrum of monochromatic light source such as Helium lamp used in the developed prototype was carried out. The results agree with the nominal spectrum distibutions of the sources with the accuracy of 4nm.

介绍了Sagnac型干涉成像光谱仪基本原理，针对上述问题得到一套对采集得到的干涉图进行光谱重构的方法，通过对所采集干涉图进行消趋势项、切趾、相位校正、共轭对称化等步骤的处理，再进行重构，即可有效避免直接重构所带来的误差，使用所研制的原理样机对氦灯等单色光源进行光谱曲线重构实验，得到的光谱强度分布曲线与标称曲线基本吻合，光谱复原精度达到了4nm，具有较好的重构效果。

In this paper, a thermal simulation model of a LED driver was established. The thermal field and thermal stress analysis of the driver was done by using the software EFD Pro 8.2, and the temperature rise from various parts and the temperature field distribution of the PCB were obtained. By analyzing the reasons leading to overheating and unideal heat distribution, corresponding thermal simulation using an improved model was carried out. Finally, the comparison and analysis of experimental measurement results and simulation results were given.

本文基于计算流体力学中的有限体积法，建立了该变换器的热仿真模型，利用EFD Pro 8.2软件，对驱动电源内部进行了热场及热应力分析，得到了各部分的温升情况和整个电源温度场的分布情况，分析导致PCB局部过热的原因，然后针对热仿真得出的不理想的热分布情况提出了改进的方法，进行了模型改进，对PCB板上的各部分进行合理的重新布局，并再次进行了热仿真，最终得到了较为理想的结果，最后给出了实验测量结果与仿真结果的对比及分析。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应，以光学纯酒石酸为原料，研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性，全文共分三部分十个章节：第一部分对当前手性药物和手性技术进行了概述，并由此展开了本文的研究背景和任务；第二部分为有机合成部分，对醛的不对称烯丙基化反应进行了深入探讨，以苯甲醛为原料对反应条件进行优化，在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选，优化配体回收实验条件，最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性，结晶回收的手性配体光学纯度保持不变。

During using anaerobic fermentation slurry as insecticide, there had many problems that are random using, non-strictly prevention and curing time, non-suitable temperature and consistency mixture ratio ctc. In this research, fristly the different mixtures are made according to the different ratio of slurry to additive. Then the insecticidal effects of the mixture are tested in different conditions so as to find the good matches of slurry and additive in laboratory. According to the up result of the good matches extents of mixture, the field experiment is made to test the mixture's insecticidal chraricter and is further found new dosage form which has many good indexes such as good insecticidal effectiveness, little additive dosis ctc. So as to looking for the dosage form's synergism, the significant analysis is done and the characters of the dosages are tested which are ecological and environmental and the new types of dosage are determined. At last, for proving the dosage's field insecticidal potency, the wide field area experiments are done and four new style dosages are triturated which adapt ecological agriculture development. Aadditionally the effective period of the mixtures are tested when other experiments are done.

本文针对厌氧发酵液作为杀虫剂施用时，随用即配和无严格的增效剂种类、喷施时间及温度、浓度配比等现象，首先对各添加剂与厌氧发酵液配成的不同浓度的混和剂在不同条件下进行实验室测试，确定杀虫率高的浓度范围，进一步细化各混和剂浓度范围作田间试验，选出杀虫效果好，添加剂量少等各项指标都好的剂型并进行显著测定，确定出各剂型的增效情况；然后对选出的剂型进行生态和环保特性测定，以便确定新剂型，最后对选定剂型作大区试验来验证田间杀虫药效，最终研制出了4种适合生态农业发展的新型无污染药肥，并对选出的混合剂进行了有效期实验测定。

The main purpose of this thesis was the chemistry composition analysis and research of Sorbus tianschanica . This thesis first made preparation of an experiment in detail to the fruit of the sorbus tianschanica to Xinjiang ,then mainly aimed to research flavonoid compounds of the sorbus tianschanica.

本论文主要对新疆天山花楸的黄酮类化合物进行了研究，首先对天山花楸的果实进行了预实验，然后对天山花楸枝叶的黄酮类化合物进行了定性研究及对其不同有效部位的黄酮类化合物进行了较为详细的定量研究。

In the method, camera was calibrated according to linear model, then its nonlinear parameters were modified based on considering lens aberration, at last image was emendated according to new parameters, full camera calibrated steps and procedure were...

在扩展两步标定方法中，首先对相机进行线性标定，然后进行非线性修正，最后进行图像校正，并提出了完整的标定步骤和程序，进行了相机标定实验。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。